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DIAMOND LIKE CARBON (DLC) COATING ON CARBON STEEL WITH PLASMA TECHNIQUES FOR GAS PIPES Ilham Nur Dimas Yahya; Djony Izak Rudyardj; Jan Ady
Indonesian Applied Physics Letters Vol. 1 No. 2 (2020): Desember
Publisher : Universitas Airlangga

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.20473/iapl.v1i2.23446

Abstract

A study about coating on carbon steel by plasma technique aims to determine the variation of time and pressure on the hardness and corrosion strength of a material. The material used in this research was carbon steel with carbon chest of 0.245%. This carbon steel was a plasma technique process with a temperature of 300oC and various pressure variations, such as 1.2 mbar; 1.4 mbar; 1.6 mbar; 1.8 mbar; And 2.0 mbar. The highest hardness was found at 1.8 mbar pressure, which was 161.7 VHN. Then set with a temperature of 300oC and a pressure of 1.8 mbar and a time variation, which were 1 hour; 1.5 hours; 2 hours; 2.5 hours; 3 hours. The largest hardness value was obtained at 3 hours with a hardness value of 161.7 VHN. Then the corrosion test obtained the optimum value at 2 hours with a corrosion value of 0.69 mpy. This was because on the surface of carbon steel there was a layer of Diamond Like Carbon (DLC).
Characteristics of Sodium Lithium Titanate Synthesized at Different Solid-State Reaction Temperature for Lithium-Ion Battery Anode Yahya, Ilham Nur Dimas; Sofyan, Nofrijon; Khaerudini, Deni Shidqi; Timuda, Gerald Ensang; Priyono, Slamet
Journal of Materials Exploration and Findings Vol. 2, No. 3
Publisher : UI Scholars Hub

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Abstract

The effect of sintering temperature on the characteristics of sodium lithium titanate (NaLiTi3O7/NaLTO) synthesized at different solid-state reaction temperature and its performance as lithium-ion battery anode has been investigated. The precursors for the synthesis consisted of LiOH.H2O, TiO2, and NaHCO3. The synthesis was performed via solid-state reaction method. The precursors were mixed and sintered at variation temperatures of 900oC, 1000oC, and 1100oC for 2 hours under atmosphere condition. The final product was characterized using X-ray diffraction (XRD) and particle size analyzer (PSA). The XRD analysis showed the main phase of NaLTO with some impurities. PSA analysis showed that the sintering temperature has a significant effect on changes in particle size where the sample at a temperature of 1100oC has the largest particle size of 74.62 µm. The battery was fabricated by firstly mixing NaLTO powder with polyvinylidene fluoride (PVDF) and acetylene black (AB) in a ratio of 85:10:5 wt.% and the mix was then deposited onto copper foil to form NaLTO a sheet. The NaLTO sheet was cut into circular discs with a diameter of 14 mm and were arranged in a sequence of separator, metallic lithium, and electrolyte to form a coin cell in a glove box. Characterization using cyclic voltammetry (CV) and charge-discharge (CD) showed that the NaLTO sintered at 1000oC provided good electrochemical performance with the largest diffusion coefficient of 3.948 x 10-10 m2/s, Coulombic efficiency reached 100%, and a high specific capacity of 65.83 mAh/g.