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All Journal Journal of Materials Exploration and Findings
Gerald Ensang Timuda
Institut Teknologi Bandung

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Characteristics of Sodium Lithium Titanate Synthesized at Different Solid-State Reaction Temperature for Lithium-Ion Battery Anode Yahya, Ilham Nur Dimas; Sofyan, Nofrijon; Khaerudini, Deni Shidqi; Timuda, Gerald Ensang; Priyono, Slamet
Journal of Materials Exploration and Findings Vol. 2, No. 3
Publisher : UI Scholars Hub

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Abstract

The effect of sintering temperature on the characteristics of sodium lithium titanate (NaLiTi3O7/NaLTO) synthesized at different solid-state reaction temperature and its performance as lithium-ion battery anode has been investigated. The precursors for the synthesis consisted of LiOH.H2O, TiO2, and NaHCO3. The synthesis was performed via solid-state reaction method. The precursors were mixed and sintered at variation temperatures of 900oC, 1000oC, and 1100oC for 2 hours under atmosphere condition. The final product was characterized using X-ray diffraction (XRD) and particle size analyzer (PSA). The XRD analysis showed the main phase of NaLTO with some impurities. PSA analysis showed that the sintering temperature has a significant effect on changes in particle size where the sample at a temperature of 1100oC has the largest particle size of 74.62 µm. The battery was fabricated by firstly mixing NaLTO powder with polyvinylidene fluoride (PVDF) and acetylene black (AB) in a ratio of 85:10:5 wt.% and the mix was then deposited onto copper foil to form NaLTO a sheet. The NaLTO sheet was cut into circular discs with a diameter of 14 mm and were arranged in a sequence of separator, metallic lithium, and electrolyte to form a coin cell in a glove box. Characterization using cyclic voltammetry (CV) and charge-discharge (CD) showed that the NaLTO sintered at 1000oC provided good electrochemical performance with the largest diffusion coefficient of 3.948 x 10-10 m2/s, Coulombic efficiency reached 100%, and a high specific capacity of 65.83 mAh/g.
Co-Authors Adnan, Farrah Anis Fazliatun Azizi, Muhammad Chollacoop, Nuwong Dafit Feriyanto Deni Shidqi Khaerudini Dianta Ginting Ilham Nur Dimas Yahya Kurniawan Kurniawan Nofrijon Sofyan, Nofrijon Nono Darsono, Nono Octaviani, Ana Nur Pudjiwati, Sri Putra, Yunata Mandala Sanusi, Yasa Slamet Priyono Tarigan, Kontan