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All Journal Jurnal Kimia dan Kemasan MESIN International Journal of Renewable Energy Development
Heri Jodi, Heri
Pusat Teknologi Bahan Industri Nuklit-BATAN Kawasan PUSPIPTEK Serpong, Tangerang 15314, Indonesia
Chemistry Control & Systems Engineering Earth & Planetary Sciences Electrical & Electronics Engineering Energy Engineering Mechanical Engineering

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Corrosion Studies On Ss-321 In Natrium-Hydroxide Solution S., Marzuki; Jodi, Heri; Effendi, Nurdin
MESIN Vol 9, No 3 (2007): Ocean Thermal Energy Conversion (OTEC) untuk "Pulau-pulau Kecil"
Publisher : Program Studi Teknik Mesin, Universitas Trisakti

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Abstract

Corrosion Studies On Ss-321 In Natrium-Hydroxide Solution. Experimental corrosionstudies on commercial SS-321 have been carried out. The experiments were carried out in a sodiumhydroxide medium with a concentration variation of 0.4 M. 0.5 M, 0.6 M, and0.7Mcorresponding topHvalues of 13.6, 13.69, 13.78, and 13.84 respectively. The experiments were carried out using a type ofM-273 EG&Gpotentiostat/galvanometer test instrument. The post-corrosion samples microstructure wereanalyzed with the aid of EDS (energy dispersive spectroscopy) equipped SEM instrument to detect thepresence of any viable corrosion byproducts. Forfurther verification x-ray diffraction method was alsoused to detect any possible emerging corrosion byproducts on the samples surfaces correlated to theSEM-EDS result. Experimental results confirm that A1SI-321 commercial alloys immersed in a natriumhydroxide corrosion medium with a variation of concentration experience very little or almost nocorrosion, so that according to the so-called Fontanas criteria these test-materials turn out to have anexcellent resistance toward natrium hydroxide corrosion. This is also evidenced by the very low corrosionrate value measured in this study. EDS study and X-ray diffraction results indicate that the possibleensuing corrosion byproducts are iron oxides, chromeoxides and silicon oxides.
Pembuatan Bahan Polimer Elektrolit Padat Berbasis Nanokomposit Kitosan Montmorillonite Untuk Aplikasi Baterai Yulianti, Evi; Saputri, Rosiana Dwi; Sudaryanto, Sudaryanto; Jodi, Heri; Salam, Rohmad
Jurnal Kimia dan Kemasan Vol. 35 No. 2 Oktober 2013
Publisher : Balai Besar Kimia dan Kemasan

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Telah dilakukan pembuatan bahan polimer elektrolit padat berbasis nanokomposit kitosan montmorillonite yang diaplikasikan dalam sistem baterai. Penelitian ini dilakukan dengan tujuan untuk menentukan komposisi optimal antara kitosan, montmorillonite dan LiClO4 sehingga diperoleh membran dengan karakteristik yang paling baik. Teknik pembuatan membran dilakukan menggunakan metode casting. Terdapat dua seri sampel yang akan di uji, yaitu membran dengan variasi komposisi montmorillonite dan variasi komposisi LiClO4. Komposisi kitosan dan montmorillonite yang digunakan pada sampel seri kedua diperoleh dari komposisi optimal membran kitosan-montmorillonite pada sampel seri pertama. Karakterisasi yang dilakukan meliputi uji tarik, pengukuran konduktivitas ionik dan identifikasi menggunakan difraksi sinar X. Penambahan montmorillonite meningkatkan kuat tarik membran dan konduktivitas ionik setelah ditambah LiClO4. Pada kondisi optimal diperoleh konduktivitas ionik 2,383 x 10-5 S/cm dan kuat tarik 15,19 Mpa pada komposisi montmorillonit 5% b/b dan LiClO4 40%. Hasil analisis difraksi sinar X menunjukkan terjadi proses interkalasi polimer kitosan ke dalam montmorillonite. 
Comparison of lithium sources on the electrochemical performance of LiNi0.5Mn1.5O4 cathode materials for lithium-ion batteries Sudaryanto, Sudaryanto; Salsabila, Nadhifah; Sari, Puspita Ayu Kusuma; Fachrudin, Adinandra Caesar; Salsabila, Adinda Atalya; Nursanto, Eduardus Budi; Priyono, Slamet; Jodi, Heri; Gumelar, Muhammad Dikdik
International Journal of Renewable Energy Development Vol 13, No 3 (2024): May 2024
Publisher : Center of Biomass & Renewable Energy (CBIORE)

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.61435/ijred.2024.59662

Abstract

In order to fulfill the demand for high energy and capacity, an electrode with high-voltage capability, namely LiNi0.5Mn1.5O4 (LNMO) that has an operating potential of up to 4.7 V vs Li/Li+, is currently becoming popular in Li-ion battery chemistries. This research produced LNMO by using a solid-state method with only one-step synthesis route to compare its electrochemical performance with different lithium sources, including hydroxide (LNMO-LiOH), acetate (LNMO-LiAce), and carbonate (LNMO-LiCar) precursors. TGA/DSC was first performed for all three sample precursors to ensure the optimal calcination temperature, while XRD and SEM characterized the physical properties. The electrochemical measurements, including cyclic voltammetry and charge-discharge, were conducted in the half-cell configurations of LNMO//Li-metal using a standard 1 M LiPF6 electrolyte. LNMO-LiOH samples exhibited the highest purity and the smallest particle size, with values of 93.3% and 418 nm, respectively. In contrast, samples with higher impurities, such as LNMO-LiCar, mainly in the form of LixNi1-xO (LiNiO), displayed the largest particle size. The highest working voltage possessed by LNMO-LiOH samples was 4.735 V vs Li/Li+. The results showed that LNMO samples with LiNiO impurities would affect the reaction behavior that occurs at the cathode-electrolyte interface during the release of lithium-ions, resulting in high resistance at the battery operations and decreasing the specific capacity of the LNMO during discharging. The highest value, shown by LNMO-LiOH, was up to 92.75 mAh/g. On the other side, LNMO-LiCar only possessed a specific capacity of 44.57 mAh/g, indicating a significant impact of different lithium sources in the overall performances of LNMO cathode.
Co-Authors Akhmad Herman Yuwono Anne Zulfia Bambang Priyono Eduardus Budi Nursanto Evi Yulianti Evvy Kartini Fachrudin, Adinandra Caesar Gumelar, Muhammad Dikdik johansyah johansyah Marzuki S., Marzuki Nurdin Effendi Rohmad Salam, Rohmad Rosiana Dwi Saputri, Rosiana Dwi Salsabila, Adinda Atalya Salsabila, Nadhifah Sari, Puspita Ayu Kusuma Sembiring, Rinawati Slamet Priyono Zulham Zulham