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Synthesis of Pyridine Derivative-based Chemosensor for Formaldehyde Detection Nurul Hidayah; Bambang Purwono; Beta Achromi Nurohmah; Harno Dwi Pranowo
Indonesian Journal of Chemistry Vol 19, No 4 (2019)
Publisher : Universitas Gadjah Mada

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (521.057 KB) | DOI: 10.22146/ijc.44028

Abstract

Compound of 3,3'-(4-(2-amino-4,5-dimethoxyphenyl)pyridine-2,6-diyl)dianiline (CHP) has been synthesized via three-step synthetic procedure from veratraldehyde as starting material and 4-(4,5-dimethoxy-2-nitrophenyl)-2,6-bis(3-nitrophenyl)pyridine (CHP-1) as an intermediate compound. The CHP-1 was reduced using hydrazine hydrate catalyzed by 10% Pd/C to the final target of CHP. The spectroscopic study revealed that CHP in acetonitrile could detect formaldehyde through fluorescence enhancement and showed color change from yellow to blue under the 365 nm portable ultraviolet lamp as a response. Based on the fluorescence spectra, the emission wavelength of CHP in acetonitrile was shifted from 526 to 480 nm after addition of formaldehyde. Limit detection (LOD), selectivity, sensitivity, and computational study geometry of CHP as a chemosensor for formaldehyde has also been investigated. CHP could also be applied as a test paper for the detection of formaldehyde qualitatively.
A Turn-off Fluorescent Chemosensor for Detecting Formaldehyde Based on Pyridine Derivative Nurul Hidayah; Bambang Purwono
al Kimiya: Jurnal Ilmu Kimia dan Terapan Vol 10, No 2 (2023): al Kimiya: Jurnal Ilmu Kimia dan Terapan
Publisher : Department of Chemistry, Faculty of Science and Technology, UIN Sunan Gunung Djati Bandung

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.15575/ak.v10i2.25573

Abstract

Formaldehyde in solution, commonly known as formalin, is often utilized. In Indonesia, there is widespread misuse of formalin as a food preservative. Formaldehyde has been identified as a carcinogenic substance by the International Agency for Research on Cancer (IARC) and the Environmental Protection Agency (EPA). Based on this background, the present study developed a sensor compound capable of detecting formaldehyde obviously. The compound 3'-(4-(3,4-dimethoxyphenyl)pyridine-2,6-diyl)dianiline (ChP-2A) has been successfully synthesized through the reduction reaction of the compound 4-(3,4-dimethoxyphenyl)-2,6-bis(3-nitrophenyl)pyridine (ChP-0A) using 80% hydrazine hydrate and 10% Pd/C as a catalyst. The ChP-2A compound in acetonitrile exhibits a significant decrease in fluorescence intensity (turn-off) after the addition of formaldehyde, and it has been successfully applied in the form of a test paper for the detection of formaldehyde qualitatively
Pelatihan Konselor Sebaya Pada Guru Sekolah Inklusi Muhammad Erwan Syah; Wina Driyan Pradana; Deni Santi Pertiwi; Nurul Hidayah
Gotong Royong : Jurnal Pengabdian, Pemberdayaan Dan Penyuluhan Kepada Masyarakat Vol. 3 No. 2 (2024): Gotong Royong (JP3KM) Juni 2024
Publisher : Mata Pena Madani

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.51849/jp3km.v3i2.46

Abstract

Tujuan dari pengabdian kepada masyarakat ini adalah untuk memberikan pengetahuan serta meningkatkan psychological well being melalui konseling sebaya pada guru di sekolah penyelenggara pendidikan inklusi. Guru di sekolah penyelenggara pendidikan inklusi Kota Yogyakarta jenjang Sekolah Dasar mengalami banyak permasalahan dan beban kerja pada penyelenggara pendidikan inklusi, sedangkan faktor tenaga pendidik memiliki pera penting dalam pencapaian kualitas pendidikan secara umum. Banyaknya tuntutan kerja dan kurangnya dukungan sosial pada guru menjadikan beban guru semakin berat. Dukungan sosial menjadi salah satu faktor yang mempengaruhi psychological well being pada seseorang. Sasaran dalam pengabdian yaitu 45 guru dengan tujuan untuk memberikan pengetahuan serta meningkatkan psychological well being melalui konseling sebaya pada guru di sekolah penyelenggara pendidikan inklusi. Kegiatan ini dilaksanakan pada bulan Mei 2024. Hasil dari pelatihan konselor sebaya ini menunjukan pengaruh yang positif pada psychological well being pada guru di sekolah penyelenggara pendidikan inklusi dilihat dari adanya peningkatan yang baik setelah guru diberikan pelatihan tersebut. Pada akhir sesi dari kegiatan pelatihan ini siswa terlihat lebih bersemangat, gembira, dan antusias hal tersebut menunjukan bahwa siswa merasa lebih baik dari sebelumnya.
Pendampingan Implementasi Effective Communication Training Service pada Kader Posyandu Kelurahan Bener Yogyakarta Sebagai Upaya Menurunkan Stunting Menuju Generasi Emas 2045 Muhammad Erwan Syah; Novita Nirmalasari; Nurul Hidayah
Gotong Royong : Jurnal Pengabdian, Pemberdayaan Dan Penyuluhan Kepada Masyarakat Vol. 4 No. 1 (2024): Gotong Royong (JP3KM) Desember 2024
Publisher : Mata Pena Madani

Show Abstract | Download Original | Original Source | Check in Google Scholar

Abstract

Tujuan kegiatan adalah untuk meningkatkan pengetahuan dan keterampilan komunikasi efektif kader Posyandu Balita. Kegiatan yang dilakukan diantaranya (1) Pelatihan ECTS (Effective Communication Training Service) pada Kader Posyandu bagi kader posyandu; (2) Pendampingan kader posyandu mengimplementasikan ECTS; (3) Psikoedukasi ini bertujuan untuk menyampaikan hasil pemeriksaan saat posyandu, dan kader posyandu menyampaikan informasi tahap tumbuh kembang dan pola asuh kepada anggota posyandu atau ibu dengan balita. Kegiatan pengabdian kepada Masyarakat ini diikuti oleh 65 kader posyandu Kelurahan Bener. Kegiatan ini dilaksnakan pada bulan Juli hingga September 2024. Hasil dari pengabdian ini diantaranya (1) Pengetahuan komunikasi efektif pada kader Posyandu meningkat yang dapat diimplementasikan untuk memperkaya dalam teori dan praktik saat melaksanakan Posyandu; (2) Pengetahuan ketrampilan komunikasi efektif meningkat yang digunakan oleh kader Posyandu kepada ibu dengan balita pada saat posyandu dan psikoedukasi; (3) Mempercepat transfer pengetahuan dan penagalaman kepada kader Posyandu untuk mempersiapkan generasi penerus Posyandu yang terampil dalam berkomunikasi kepada ibu dengan balita saat Posyandu dan psikoedukasi; (4) Kader Posyandu Balita mendapatkan pengetahuan kolektif mengenai komunikasi efektif, tahap tumbuh kembang anak dan pola asuh untuk menurunkan stunting menuju generasi emas 2045; (5) Kader Posyandu Balita memperoleh pengetahuan praktis untuk pengembangan dan peningkatan sarana prasarana pendukung kegiatan pelatihan dan pendampingan implementasi ECTS
Hedonic Test Analysis and Feasibility of The Selling Price of Cocoa Seed Waste Products in PT XYZ Kulon Progo, Yogyakarta Sari, Oktavia Nurmalita; Hidayah, Nurul; Rahayu, Wahidah Mahanani
Journal of Agri-Food Science and Technology Vol. 2 No. 2 (2021): August
Publisher : Universitas Ahmad Dahlan

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.12928/jafost.v2i2.5901

Abstract

Innovative use of waste into herbal beverage products the waste treatment process starts from the stage of roasting cocoa beans, breaking the beans and peeling the skin, sorting, drying, preparation of packaging and materials, filling and mixing, giving silica gel and labelling the expiration date. The raw materials needed are cocoa bean husk, dried cardamom, and cinnamon powder. While the packaging material uses PET plastic bottle packaging. Before the product is marketed, it is necessary to conduct a feasibility analysis of the selling price. The analysis shows that the selling price of chocolate product of Rp. 15,000 is feasible because profit taking is 48% with the selling price per unit more than the cost per unit. The net profit margin of chocolate product of 32.6% means that the company is considered efficient in determining the selling price of its products and successfully controlling costs in it because the NPM figure is > 5%. Hedonic tests were also conducted to determine consumer acceptance of the product through a hedonic test of 20 panelists based on the parameters of color, aroma, taste, and packaging. The hedonic test scale 1 shows that consumers do not like it very much, a scale 2 does not like it, a scale 3 likes it, and a scale 4 likes it very much. The average level of preference for color parameters is 3.58, aroma is 3.31, taste is 3.47, and packaging is 3.84 which indicates that the panelists like these 4 parameters.
Hedonic Test of Pegagan Chocolate Products at PT XYZ Iryani, Dian; Hidayah, Nurul
Journal of Agri-Food Science and Technology Vol. 2 No. 2 (2021): August
Publisher : Universitas Ahmad Dahlan

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.12928/jafost.v2i2.6440

Abstract

Handling of raw materials for cocoa beans is an important process to maintain the quality of the processed chocolate. There are several stages carried out in the post-harvest cocoa process including fruit picking, fruit breaking, cocoa bean fermentation, drying cocoa beans and storage. The purpose of this study was to determine whether or not a sensory assessment of the preference for pegagan chocolate was made, and to analyze the panellists’ level of acceptance of pegagan chocolate. Pegagan leaf chocolate is produced with the aim of providing good nutrition, brain multivitamins and memory enhancers. Sensory assessment of the hedonic test using 20 untrained panellists from the parameters measured were color, taste, texture, aroma and shape. The panellists’ acceptance of chocolate with the addition of pegagan leaves was that the majority liked the chocolate on all parameters.
Chemical Characteristics of Non-Dairy Cheese from Coconut Milk as an Alternative Ingredient for Lactose Intolerance Halim, Judella Kusuma; Hidayah, Nurul; Juwitaningtyas, Titisari; Mutmainah, Mutmainah; Fitriani, Aprilia
Journal of Agri-Food Science and Technology Vol. 4 No. 1 (2023): April
Publisher : Universitas Ahmad Dahlan

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.12928/jafost.v4i1.8724

Abstract

Lactose-intolerant people are unable to ingest cheese since it includes lactose. Lactose-free cheese can be made using coconut milk as an alternative. Coconut milk can substitute milk as a raw material for cheese production because it is rich in proteins such as albumin, globulin, prolamin, and glutelin. This research aims to determine how different proportions of coconut milk and soy extract affect the nutritional value of coconut milk cheese. Cheeses with 80:20, 70:30, and 60:40 ratios of coconut milk to soy extract are made by directly acidifying soy extract with lemon juice. Protein, lipid, and moisture content were all evaluated. At compositions 80:20, 70:30, and 60:40, the protein content of coconut milk cheese was 3.85%; 4.80%; and 5.73%, respectively. Coconut milk cheese had lipid contents of 28%, 27%, and 25.74%, respectively; the moisture contents were 64.93%; 61.92%; and 60.49%. This research contributes to utilizing coconut milk as a milk substitute.
Optimization of lemongrass cultivation into essential oil in Tunggularum, Wonokerto Hidayah, Nurul; Fathurrahman , Haris Imam Karim; Fitriani , Aprilia; Sabila, Liya Yusrina
Jurnal Pemberdayaan: Publikasi Hasil Pengabdian Kepada Masyarakat Vol. 8 No. 3 (2024)
Publisher : Universitas Ahmad Dahlan

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.12928/jpm.v8i3.11601

Abstract

The empowerment of the community in Tunggularum, Wonokerto, aims to optimize lemongrass (Cymbopogon citratus) cultivation into essential oil products through community-based training and practical skills development. Lemongrass is widely cultivated in the area but is underutilized due to limited knowledge of its potential economic value, particularly in essential oil production. This community service project focused on addressing this gap through two primary activities: a socialization session on the essential oil distillation process and hands-on training in the operation of distillation equipment. The project involved 20–25 local participants, predominantly women, who attended both the theoretical and practical sessions. The results showed significant improvements in the participants' knowledge and skills. Over 70% of participants reported feeling more capable of managing the local lemongrass resources and demonstrated an enhanced understanding of the distillation process. The training also fostered new skills in operating distillation equipment, which further encouraged the participants to explore the business potential of lemongrass essential oil production.
The influence of adding red galangal simplicia (Alpinia purpurata K Schum.) on the chemical, organoleptic, and antioxidant activity of soursop leaf tea (Annona muricata L.) Maulidya, Farah Nabila; Hidayah, Nurul
Advances in Food Science, Sustainable Agriculture and Agroindustrial Engineering (AFSSAAE) Vol 8, No 1 (2025)
Publisher : Advances in Food Science, Sustainable Agriculture and Agroindustrial Engineering (AFSSAAE)

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.21776/ub.afssaae.2025.008.01.2

Abstract

Herbal tea imparts health benefits largely due to its polyphenol-based antioxidant activity. Soursop leaves contain compounds including flavonoids, tannins, alkaloids, acetogenins, and saponins. Red galangal contains compounds such as saponins, tannins, flavonoids, and essential oils. The addition of red galangal to soursop leaf tea not only enhances the antioxidant activity of the tea but also improves its flavor. This study investigated the influence of adding red galangal simplicia to soursop leaf tea on its chemical and organoleptic properties, and also its antioxidant activity. The research method was based on varying ratios of the two ingredients (soursop leaves: red galangal simplicia), specifically F1 (100%: 0%), F2 (85%: 15%), F3 (80%: 20%), F4 (75%: 25%), F5 (70%: 30%), with three repetitions. The chemical properties tested included water content, ash content, antioxidant activity, flavonoid content, polyphenol content, and tannin content. The organoleptic tests included assessments of color, aroma, taste, aftertaste, and overall preference. The results demonstrated that soursop leaf tea with the addition of red galangal simplicia had a significant effect on its chemical properties, organoleptic properties, and antioxidant activity. The analysis results showed the lowest water content at 8.51% (F5), the lowest ash content at 7.03% (F5), the highest antioxidant activity at 33.37 ppm (F5), the highest flavonoid content at 95.46 mgQE/g (F5), the highest total phenolic content at 46.10 mgGAE/g (F5), and the highest tannin content at 42.63 mgCE/g (F5). Organoleptic assessment based on color preference scored 3.83 (F1), with the highest aroma score at 3.70 (F5), the highest taste score at 3.51 (F5), the highest aftertaste score at 3.30 (F5), and the highest overall preference score at 3.58 (F5). Based on these results, it can be concluded that the most preferred treatment, with the highest phytochemical contents and antioxidant activity, was treatment F5 with a concentration of 70% soursop leaves and 30% red galangal simplicia.
Pengaruh penambahan simplisia jahe merah (Zingiber Officinale Var Rubrum Rhizoma) terhadap sifat kimia dan organoleptik teh daun kelor (Moringa Oleifera) Riski Bayu Lintang; Nurul Hidayah

Publisher : Program Studi Ilmu dan Teknologi Pangan, Universitas Yudharta, Pasuruan

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.35891/tp.v15i1.4688

Abstract

Tea is a drink that is much sought after by Indonesian people. Moringa leaves have a high antioxidant content, especially flavonoids and polyphenols which can be used as raw materials for tea. Red ginger is a type of rhizome that is rich in phenolic compounds and essential oils. Red ginger in simplicia form is added to tea to improve the organoleptic properties and increase the antioxidant activity of Moringa leaf tea. The aim of this research was to determine the effect of adding red ginger simplicia on the chemical and organoleptic properties of Moringa leaf tea. This research used a Completely Randomized Design (CRD) and was repeated 3 times consisting of 5 treatments with the addition of red ginger simplicia, namely P1 (0%), P2 (10%), P3 (20%), P4 (30%), and P5 (40%). The resulting data was analyzed using One Way ANOVA with a significance level of 5% with the DMRT (Duncan's Multiple Range Test) further test. Test parameters include water content, ash content, flavonoids, antioxidants, polyphenols, tannins and organoleptics. Organoleptic tests with a total of 30 panelists include color, aroma, taste, aftertaste and overall. The highest value is found in P5 with antioxidant activity IC50Â of 33.86 ppm, polyphenols of 59.94 mgGAE/g, flavonoids of 87.14 mgQE/g, P5 tannins of 50.81 mgCE/g, and organoleptic results that are preferred by consumers overall it is P4 with a value of 3.90. The results of this study showed that the addition of red ginger simplicia had an effect on the test parameters for water content, ash content, polyphenols, flavonoids, tannins and organoleptics of Moringa leaf tea.