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All Journal Wood Research Journal : Journal of Indonesian Wood Research Society Wood Research Journal : Journal of Indonesian Wood Research Society
Harliando, Bagus Praditya
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Agriculture, Biological Sciences & Forestry

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Inter-tree Variation in Chemical Components of North Sumatra Benzoin Gum (Styrax sp.) Harliando, Bagus Praditya; Sukadaryati, Sukadaryati; Lukmandaru, Ganis
Wood Research Journal Vol 5, No 2 (2014): Wood Research Journal
Publisher : Masyarakat Peneliti Kayu Indonesia

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.51850/wrj.2014.5.2.46-50

Abstract

Benzoin gum, which is known as Sumatra benzoin (Styrax sp), is widely used as an ingredient in the incense. Although these resins are widely used as flavours and fragrances, no studies have been made on inter-tree variation of its chemical composition. Therefore, benzoin gum samples were tapped from the 30 individual trees (age 10 years, 9~35 cm in diameter) grown in the community forest of Polung, Humbang Hasundutan Regency, North Sumatra. The gum chemical components were analyzed by GC-MS and identified by comparing the fragmentation pattern with the standard components and literature studies. It was found that the major compounds detected by GC-MS were cinnamic acid (51.48%), cinnamyl cinnamate (62.56%), benzoic acid (1.94%), chavicol (5.18%), benzyl cinnamic acid (7.8%), atropic acid (9.84%), and vanillin (1.47%). Two main constituents that were always detected from 30 benzoin trees were chavicol and cinnamic acid, followed by cinnamyl cinnamate (28 trees) and benzoic acid (14 trees). By cluster analysis, 30 samples of benzoin gum can be classified into clusters I - III based on the average chemical components. Cluster I consisted of 7 individual trees with a higher percentage of benzoic acid and chavicol but lower concentration of cinnamic acid compared to other clusters. Cluster II consisted of 18 individual trees with a high percentage of cinnamyl cinnamate whereas clusters III consisted of 5 individual trees characterized with a high percentage of cinnamic acid. By Pearson correlation, it was observed that no significant correlation between the values of diameter and the amount of chemical components of benzoin gum.
Inter-tree Variation in Chemical Components of North Sumatra Benzoin Gum (Styrax sp.) Harliando, Bagus Praditya; Sukadaryati, Sukadaryati; Lukmandaru, Ganis
Wood Research Journal Vol 5, No 2 (2014): Wood Research Journal
Publisher : Masyarakat Peneliti Kayu Indonesia

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.51850/wrj.2014.5.2.46-50

Abstract

Benzoin gum, which is known as Sumatra benzoin (Styrax sp), is widely used as an ingredient in the incense. Although these resins are widely used as flavours and fragrances, no studies have been made on inter-tree variation of its chemical composition. Therefore, benzoin gum samples were tapped from the 30 individual trees (age 10 years, 9~35 cm in diameter) grown in the community forest of Polung, Humbang Hasundutan Regency, North Sumatra. The gum chemical components were analyzed by GC-MS and identified by comparing the fragmentation pattern with the standard components and literature studies. It was found that the major compounds detected by GC-MS were cinnamic acid (51.48%), cinnamyl cinnamate (62.56%), benzoic acid (1.94%), chavicol (5.18%), benzyl cinnamic acid (7.8%), atropic acid (9.84%), and vanillin (1.47%). Two main constituents that were always detected from 30 benzoin trees were chavicol and cinnamic acid, followed by cinnamyl cinnamate (28 trees) and benzoic acid (14 trees). By cluster analysis, 30 samples of benzoin gum can be classified into clusters I - III based on the average chemical components. Cluster I consisted of 7 individual trees with a higher percentage of benzoic acid and chavicol but lower concentration of cinnamic acid compared to other clusters. Cluster II consisted of 18 individual trees with a high percentage of cinnamyl cinnamate whereas clusters III consisted of 5 individual trees characterized with a high percentage of cinnamic acid. By Pearson correlation, it was observed that no significant correlation between the values of diameter and the amount of chemical components of benzoin gum.
Extractive Content and Antioxidant Activity of Cajuput Bark (Melaleuca cajuputi Powell) Harliando, Bagus Praditya; Lukmandaru, Ganis; Kartikawati, Noor Khomsah
Wood Research Journal Vol 15, No 2 (2024): WOOD RESEARCH JOURNAL
Publisher : Masyarakat Peneliti Kayu Indonesia

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.51850/wrj.2024.15.2.63-68

Abstract

Both wood and non-wood industries generate large amounts of residues from processes like bark peeling and removal. In the cajuput oil industry, the waste products include distillation residues and cajuput bark. The diverse extractives and chemical components found in cajuput bark have the potential for enhanced value through various applications. This study aimed to determine the chemical components, extractive content (EC), and percentage inhibition of antioxidant activity (%IAA) of cajuput bark extract to explore more effective uses of this byproduct. Cajuput bark (Melaleuca cajuputi Powell) was sourced from a 26-year-old cajuput stand in Paliyan, Gunungkidul. The bark powder was extracted using a methanol-water solvent mixture at concentrations of 40% and 80%. Extraction was conducted in water baths at temperatures of 60°C and 100°C for 120 minutes. GC-MS identified several chemical components in the methanol extract of cajuput bark, including sugars (erythritol, D-arabinose, D-lyxose, adonitol, d-galactose, D-glucitol, and L-rhamnose), fatty acids (lactic acid, glycerol, glyceric acid, malic acid, and palmitic acid), and phenolic derivatives (gallic acid and protocatechuic acid). The average extractive content of the methanol extract of cajuput bark was 4.07%, and the percentage inhibition of antioxidant activity was 40.26%.
Extractive Content and Antioxidant Activity of Cajuput Bark (Melaleuca cajuputi Powell) Harliando, Bagus Praditya; Lukmandaru, Ganis; Kartikawati, Noor Khomsah
Wood Research Journal Vol 15, No 2 (2024): WOOD RESEARCH JOURNAL
Publisher : Masyarakat Peneliti Kayu Indonesia

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.51850/wrj.2024.15.2.63-68

Abstract

Both wood and non-wood industries generate large amounts of residues from processes like bark peeling and removal. In the cajuput oil industry, the waste products include distillation residues and cajuput bark. The diverse extractives and chemical components found in cajuput bark have the potential for enhanced value through various applications. This study aimed to determine the chemical components, extractive content (EC), and percentage inhibition of antioxidant activity (%IAA) of cajuput bark extract to explore more effective uses of this byproduct. Cajuput bark (Melaleuca cajuputi Powell) was sourced from a 26-year-old cajuput stand in Paliyan, Gunungkidul. The bark powder was extracted using a methanol-water solvent mixture at concentrations of 40% and 80%. Extraction was conducted in water baths at temperatures of 60°C and 100°C for 120 minutes. GC-MS identified several chemical components in the methanol extract of cajuput bark, including sugars (erythritol, D-arabinose, D-lyxose, adonitol, d-galactose, D-glucitol, and L-rhamnose), fatty acids (lactic acid, glycerol, glyceric acid, malic acid, and palmitic acid), and phenolic derivatives (gallic acid and protocatechuic acid). The average extractive content of the methanol extract of cajuput bark was 4.07%, and the percentage inhibition of antioxidant activity was 40.26%.
Co-Authors Ganis Lukmandaru Noor Khomsah Kartikawati, Noor Khomsah Sukadaryati Sukadaryati