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All Journal Indonesia Chimica Acta Hydrogen: Jurnal Kependidikan Kimia
Nursaida, Marta Citra
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Chemical Engineering, Chemistry & Bioengineering Chemistry Education

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Synthesis of Colorimetric Sensor for Cyanide Detection with Iron(III) Chloride reagent Using Sol Gel Method with Smarthphone Combination Rohsaita, Amalia; Thohir, Muhammad Bakhru; Surya Efendi, Meilisa Rusdiana; Kusumaning Tiyas, Windi Pangesti; Nursaida, Marta Citra
Hydrogen: Jurnal Kependidikan Kimia Vol 12, No 3 (2024): June-July 2024
Publisher : Universitas Pendidikan Mandalika

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.33394/hjkk.v12i3.11887

Abstract

Sensor untuk mendeteksi ion sianida (CN - ) telah berhasil dilakukan dengan metode sol-gel menggunakan prekursor tetraetil ortosilikat dan pereaksi FeCl3. Penelitian ini bertujuan untuk mengetahui kondisi optimal sintesis, kondisi optimal sensor, menentukan LoD dan LoQ. Sintesis dilakukan dengan mencampurkan prekursor dengan pelarut etanol. Selanjutnya ditambahkan H2O, Triton X-100, reagen dan katalis ke dalam campuran. Variasi yang dilakukan adalah konsentrasi reagen dan waktu penuaan terbaik. Hasil sensor dinyatakan dalam nilai Euclidean Distance (ED) titik Merah-Hijau-Biru (RGB) yang diperoleh. Kondisi optimal untuk penyensoran dilakukan dengan memvariasikan waktu kontak. Pada sintesis sol gel konsentrasi reagen terbaik diperoleh pada konsentrasi 0,1 M dan waktu penuaan terbaik adalah 4 hari. Penentuan kondisi sensor optimal terjadi pada waktu 30 detik dengan batas pencucian 120 detik. Validasi metode sensor menghasilkan linearitas pada rentang konsentrasi 100 – 1000 ppm dengan nilai R 2 sebesar 0,9984. LoD dan LoQ masing-masing sebesar 65,45 ppm dan 218,16 ppm. Karakterisasi sensor menggunakan spektrofotometer FTIR dari bilangan gelombang 4000 sampai 400 cm-1. Spektrum IR yang dihasilkan menunjukkan keberhasilan dalam sintesis sol-gel, karena pada penelitian ini SiO2 muncul pada bilangan gelombang sekitar 433 cm-1. Setelah tahap sensor dengan merendam sensor pada analisa CN - 0,01 M dan CN - 0,1 M tidak ada tanda-tanda munculnya gugus Fe-S pada bilangan gelombang 4000-400 cm-1, karena daerah serapannya berada pada 380- 311 cm -1.
Synthesis of Colorimetric Sensor for Cyanide Detection with Iron(III) Chloride reagent Using Sol Gel Method with Smarthphone Combination Rohsaita, Amalia; Thohir, Muhammad Bakhru; Surya Efendi, Meilisa Rusdiana; Kusumaning Tiyas, Windi Pangesti; Nursaida, Marta Citra
Hydrogen: Jurnal Kependidikan Kimia Vol. 12 No. 3 (2024): June-July 2024
Publisher : Universitas Pendidikan Mandalika

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.33394/hjkk.v12i3.11887

Abstract

Sensor untuk mendeteksi ion sianida (CN - ) telah berhasil dilakukan dengan metode sol-gel menggunakan prekursor tetraetil ortosilikat dan pereaksi FeCl3. Penelitian ini bertujuan untuk mengetahui kondisi optimal sintesis, kondisi optimal sensor, menentukan LoD dan LoQ. Sintesis dilakukan dengan mencampurkan prekursor dengan pelarut etanol. Selanjutnya ditambahkan H2O, Triton X-100, reagen dan katalis ke dalam campuran. Variasi yang dilakukan adalah konsentrasi reagen dan waktu penuaan terbaik. Hasil sensor dinyatakan dalam nilai Euclidean Distance (ED) titik Merah-Hijau-Biru (RGB) yang diperoleh. Kondisi optimal untuk penyensoran dilakukan dengan memvariasikan waktu kontak. Pada sintesis sol gel konsentrasi reagen terbaik diperoleh pada konsentrasi 0,1 M dan waktu penuaan terbaik adalah 4 hari. Penentuan kondisi sensor optimal terjadi pada waktu 30 detik dengan batas pencucian 120 detik. Validasi metode sensor menghasilkan linearitas pada rentang konsentrasi 100 – 1000 ppm dengan nilai R 2 sebesar 0,9984. LoD dan LoQ masing-masing sebesar 65,45 ppm dan 218,16 ppm. Karakterisasi sensor menggunakan spektrofotometer FTIR dari bilangan gelombang 4000 sampai 400 cm-1. Spektrum IR yang dihasilkan menunjukkan keberhasilan dalam sintesis sol-gel, karena pada penelitian ini SiO2 muncul pada bilangan gelombang sekitar 433 cm-1. Setelah tahap sensor dengan merendam sensor pada analisa CN - 0,01 M dan CN - 0,1 M tidak ada tanda-tanda munculnya gugus Fe-S pada bilangan gelombang 4000-400 cm-1, karena daerah serapannya berada pada 380- 311 cm -1.
Synthesis AuNPs Using Moringa oleifera Extract and Potential Study as Colorimetric Microplastic Detection Thohir, Muhammad Bakhru; Setyaningrum, Dyah; Efendi, Meilisa Rusdiana Surya; Saputra, Arya Ananda; Nursaida, Marta Citra
Hydrogen: Jurnal Kependidikan Kimia Vol. 13 No. 3 (2025): June 2025
Publisher : Universitas Pendidikan Mandalika

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.33394/hjkk.v13i3.16603

Abstract

Nanoparticles are multipurpose materials that have been utilized in the medical, energy, and environmental monitoring fields. The advantage of nanoparticles is that they have unique physicochemical properties such as surface area, optical activity, and surface modifiability. One of the important uses of nanoparticles is for environmental monitoring. This is because the surface of nanoparticles can be modified, and with their small size, they can reach analytes in difficult matrices. However, conventional synthesis methods of nanoparticles have been unsustainable. Therefore, the synthesis of AuNPs using bioreductors was considered urgent. The aim of this research was to determine the optimum conditions for the synthesis of AuNPs with Moringa oleifera (MO) as a bioreductor to obtain AuNPs-MO, to characterize the synthesized AuNPs-MO, and to study the application of AuNPs-MO for monitoring microplastic pollutants. This research was conducted through the stages of extraction, determination of optimum conditions, characterization, and literature study of the potential of AuNPs-MO as a detector. Determination of optimum conditions was carried out by applying variations in pH and precursor-reducing agent ratio. The optimal pH was found to be 6, and the optimal volume ratio was 15:5 (mL). Characterization of AuNPs-MO was conducted using FTIR and PSA. The FTIR spectra showed identical absorption patterns for AuNPs synthesized with bioreductants, and the particle size was found to be 61.15 nm. In addition, microplastics were detected using AuNPs both directly, through surface modification with proteins, and indirectly, with the assistance of acetone. From this series of experiments, satisfactory results were obtained.
New Synthesis Method of AuNPs Using Moringa oleifera Extract as Bioreductor and Potential Study as Colorimetric Microplastic Detection Thohir, Muhammad Bakhru; Setyaningrum, Dyah; Saputra, Arya Ananda; Nursaida, Marta Citra
Jurnal Akta Kimia Indonesia (Indonesia Chimica Acta) Volume 18, No 2: December 2025
Publisher : Hasanuddin University

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.70561/ica.v18i2.44733

Abstract

Nanoparticles are multipurpose materials that have been utilized in the medical, energy, and environmental monitoring fields. The advantage of nanoparticles is that they have unique physicochemical properties such as surface area, optical activity, and surface modifiability. One of the important uses of nanoparticles is for environmental monitoring. This is because the surface of nanoparticles could be modified, and with their small size, they could reach analytes in difficult matrices. However, the synthesis of nanoparticles has been an unsustainable process. Therefore, the synthesis of AuNPs using bioreductors finds its urgency. The aim of this research is to determine the optimum conditions for the synthesis of AuNPs-MO, the character of the synthesized AuNPs-MO, and to study the application of AuNPs-MO for monitoring microplastic pollutants. This research was conducted through the stages of extraction, determination of optimum conditions, characterization, and literature study of the potential of AuNPs-MO as a detector. Determination of optimum conditions was carried out by applying variations in pH and precursor-reducing agent ratio. Characterization of AuNPs-MO was done with FTIR and PSA. In addition, microplastic detection models with AuNPs-MO have been obtained directly and indirectly. From this series of experiments, satisfactory results have been obtained.
Co-Authors Dyah Setyaningrum, Dyah Effendi, Meilisa Rusdiana Surya Kusumaning Tiyas, Windi Pangesti Mochammad Imron Awalludin Rohsaita, Amalia Saputra, Arya Ananda Thohir, Muhammad Bakhru