More than half a percent of fifth-grade students of SD Muhammadiyah 1 Palopo lack mastery of mufradāt, so that it affects the quality of language skills to be achieved. Therefore, the researcher tries to overcome this problem by applying the Tamyiz method which aims to (1) observe and report on the implementation of the Tamyiz method, (2) describe students' mastery of mufradāt, and ( 3) determine the effect of applying the Tamyiz method on the mastery of mufradāt of fifth-grade students of SD Muhammadiyah 1 Palopo. This type of research is experimental research designed using one group pre-test post-test. The data needed for this study were collected through participant observation, tests, closed questionnaires, structured interviews, and documentation collected from Arabic teachers and fifth-grade students of SD Muhammadiyah 1 Palopo, totaling 25 students. The result showed that the value of sig. (2 tailed) from the pre-test and post-test data is <0.05, which is 0.000. That is, the hypothesis is accepted. In other words, there is a significant difference between the pre-test and post-test mean score. Thus, the mastery of students' mufradāt has increased after the implementation of the Tamyiz method.
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