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Jurnal Sains Materi Indonesia
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Jurnal Sains Materi Indonesia (Indonesian Journal of Materials Science), diterbitkan oleh Pusat Teknologi Bahan Industri Nuklir - BATAN. Terbit pertama kali: Oktober 1999, frekuensi terbit: empat bulanan.
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Articles 10 Documents
Search results for , issue "Vol 21, No 4: JULY 2020" : 10 Documents clear
SYNTHESIS AND CHARACTERIZATION OF HPMC/HAp/Fe3O4 COMPOSITE FOR HYPERTHERMIA APPLICATION Muflikhah Muflikhah; Wildan Zakiah Lubis; Irma Septi Ardiani; Khoirotun Nadiyyah; Sulistioso Giat Sukaryo
Jurnal Sains Materi Indonesia Vol 21, No 4: JULY 2020
Publisher : Center for Science & Technology of Advanced Materials - National Nuclear Energy Agency

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.17146/jsmi.2020.21.4.6023

Abstract

SYNTHESIS AND CHARACTERIZATION OF HPMC/HAp/Fe3O4 COMPOSITE FOR HYPERTHERMIA APPLICATION. Magnetic material become subject of intense research for hyperthermia application, and injectable magnetic hyperthermia for bone cancer is one of this research interest. In this study, composite of hydroxyapatite (HAp) and Fe3O4 in Hydroxypropyl-methyl cellulose (HPMC) matrix (HPMC/HAp/Fe3O4) has been synthesized in gel form that are expected can be applied for injectable bone substitute (IBS) in hyperthermia therapy. Composites were made using conventional methods by mixing HAp powder with ferrofluid Fe3O4 in HPMC solution. The composition of the composites were varied with the mass comparison of HPMC: HAp: Fe3O4 was 1: 0: 0; 1: 3: 0; 1: 2: 0.5; 1: 1: 0.25; and 1: 0: 3. The physical, chemical, and magnetic properties of the composites were characterized using X-Ray Diffractometer (XRD), Fourier Transform Infrared Spectrometry (FT-IR), Particle Size Analyzer (PSA), and Vibrating Sample Magnetometer (VSM). The XRD characterization results of the HPMC/HAp/Fe3O4 composite showed the crystalline phase of the constituent components. Saturation magnetization of the HPMC/HAp/Fe3O4 composite was 2.72 emu/g and 1.79 emu/g for the composition of 1: 2: 0.5 and 1:1:0.25 respectively. HPMC/HAp/Fe3O4 composite has superparamagnetic and biocompatible properties, so that can be applied as IBS in hyperthermia therapy for bone cancer.
THE EFFECT OF MILLING TIME AND PERCENTAGE OF DISPERSING AGENT ON THE CHARACTERISTIC OF SOLVENT-BASED BLACK PAINT FROM CARBON BLACK PIGMENT Ratnawati Ratnawati; Joko Noveriarto; Aniek S Handayani; Is S Purwaningsih; Iyus Hendrawan
Jurnal Sains Materi Indonesia Vol 21, No 4: JULY 2020
Publisher : Center for Science & Technology of Advanced Materials - National Nuclear Energy Agency

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.17146/jsmi.2020.21.4.5984

Abstract

THE EFFECT OF MILLING TIME AND PERCENTAGE OF DISPERSING AGENT ON THE CHARACTERISTIC OF SOLVENT-BASED BLACK PAINT FROM CARBON BLACK PIGMEN. The need for black paint made from carbon black pigment increasing year by year especially in the automotive world. The production of black paint is performed by milling the resin, pigment, additive/dispersing agent, and solvent. In the manufacturing process, it takes a relatively long time with precise dispersing agent composition toward pigment to get the product with blackness/solid black according to the expected quality. This work aims to study the role of the milling time of carbon black fw 200 beads on a 3 liter ball mill and the percentage of dispersing agents on paint color quality, especially blackness. The variations in milling time were 36, 48, and 60 hours and the weight percentage of dispersing agent toward pigment were 80%, 100%, and 120%. The optimum results obtained are at the milling time of 48 hours and on the percentage of dispersing agent of 120% with the product characteristics fulfills the requirement namely: 10 μm of particle fineness, 111.5 krebs unit of viscosity, 36.97% of solid content, 0.9839 gr/cc of specific gravity with desirable solid black color.
COVER JUSAMI VOL.21, NO.4, JULY 2020 JUSAMI JUSAMI
Jurnal Sains Materi Indonesia Vol 21, No 4: JULY 2020
Publisher : Center for Science & Technology of Advanced Materials - National Nuclear Energy Agency

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.17146/jsmi.2020.21.4.6159

Abstract

PROPERTIES OF EDIBLE FILM FROM MODIFIED SAGO STARCH PRECIPITATED BY BUTANOL Riska Surya Ningrum; Dewi Sondari; Putri Amanda; Bernadeta Ayu Widyaningrum; Dian Burhani; Fazhar Akbar; Yulianti Sampora
Jurnal Sains Materi Indonesia Vol 21, No 4: JULY 2020
Publisher : Center for Science & Technology of Advanced Materials - National Nuclear Energy Agency

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.17146/jsmi.2020.21.4.6022

Abstract

ROPERTIES OF EDIBLE FILM FROM MODIFIED SAGO STARCH PRECIPITATED BY BUTANOL. The edible film is a thin layer that can be used as food packaging and safe for consumption. Starch is a material that can be used as an edible film because it is biodegradable, non-toxic, able to form a strong and transparent film. In this research, sago starch has been precipitated using butanol for 1, 2, 3, 4, and 5 hours. Precipitated sago is reacted with 3% glycerol and then formed into a film by printing it on a petri dish. Characterizations of edible films are FTIR, contact angle, water solubility, swelling power, WVTR, and mechanical properties (thickness, tensile strength, and elongation). Edible film (B2) has the best mechanical properties, that is high hydrophobicity (contact angle is 60,351 degree), tensile strength (6,8843 N/mm2), and elongation (49,5081 %), also low water solubility (0,3352 %), moisture content (18,6005 %), and WVTR (0,02986 g s-1 m-2).
CHARACTERIZATION OF COMPOSITE CONTAINING LDPE (LOW DENSITY POLY ETHYLENE) AND MODIFIED PINEAPPLE LEAF FIBER Lestari Wardani; Noerati Noerati; Doni Sugiyana
Jurnal Sains Materi Indonesia Vol 21, No 4: JULY 2020
Publisher : Center for Science & Technology of Advanced Materials - National Nuclear Energy Agency

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.17146/jsmi.2020.21.4.6036

Abstract

CHARACTERIZATION OF COMPOSITE CONTAINING LDPE ( LOW DENSITY POLY ETHYLENE) AND MODIFIED PINEAPPLE LEAF FIBER. Pineapple leaf fiber could be used as a reinforcing material in natural fiber composites production with a synthetic polymer matrix. The typical problem in this process was the weak bond between the fiber component and the matrix. This study aimed to improve the bonds strength between pineapple leaf fibers and the polymer matrix of LDPE (Low Density Poly Ethylene) by modifying pineapple leaf fibers. The modification of pineapple leaf fibers was carried out through an enzymatic process using the xylanase enzyme. A modified fiber was then used as a fiber component in the composite using a commercial LDPE plastic matrix. Composites were made by the sandwich method using a hotpress machine at a temperature of 130 °C for 10 minutes. The evaluation of the composites were carried out by testing the tensile strength properties using the Tensolab tool and thermal properties using the TGA (Thermal Gravimetry Analysis) instrument. The results of the mechanical properties test of the composite showed the modified pineapple leaf fiber-based composite had a better tensile strength (34.3 MPa) than the untreated pineapple leaf fiber-based composite (30.2 MPa). The results of the thermal properties test showed the decreasing of the mass occurred at temperature of 300-350 °C due to degradation of the fiber,and it completely degraded at temperature of 450 °C.
PREFACE JUSAMI VOL.21, NO.4, JULY 2020 JUSAMI JUSAMI
Jurnal Sains Materi Indonesia Vol 21, No 4: JULY 2020
Publisher : Center for Science & Technology of Advanced Materials - National Nuclear Energy Agency

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.17146/jsmi.2020.21.4.6160

Abstract

EFFECT OF ULTRASONIC TREATMENT ON THE CONSOLIDATION OF ODS STEEL FeCrY2O3 PROCESSING WITH CAPSULATED SINTERING PROCESS. Marzuki Silalahi; Bernardus Bandriyana; Harum Andriadi Bayu; Bambang Sugeng; Rohmad Salam
Jurnal Sains Materi Indonesia Vol 21, No 4: JULY 2020
Publisher : Center for Science & Technology of Advanced Materials - National Nuclear Energy Agency

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.17146/jsmi.2020.21.4.5969

Abstract

EFFECT OF ULTRASONIC TREATMENT ON THE CONSOLIDATION OF ODS STEEL FeCrY2O3 PROCESSING WITH CAPSULATED SINTERING PROCESS. A new method on the synthesis of ODS (Oxide Dispersion Strengthened) steel for advanced nuclear material was performed by ultrasonic treatment to improve the consolidation process. The raw material of Fe, Cr and Y2O3powder with the composition of Fe-15 wt% Cr, 0.5 wt% and Ytria (Y2O3)  as disperzoid were  processed by the powder metallurgy method with the main process of pre-alloying, iso-compaction and sintering process. The pre-alloying process was carried out by mixing the alloying elements using ultrasonically treatment at frquency of 20 kHz with variation of  40, 50 and 60 % amplitude. Iso-compaction process was done using the load of  800 psi to obtain a pellet-shaped sample, then continued by the sintering process for consolidation. The sintering process was done in two stages, 1-step sintering and 2-steps sintering, using the heating furnace by putting the sample in a quartz capsule to prevent oxidation attack. Scanning Electron Microscopy-Energy Dispersive X-ray Spectroscopy (SEM-EDS), X-ray Diffraction (XRD), and Micro-hardness tests were carried out to analyze the microstructure and phase formation in relation to the consolidation process. The highest hardness occurred in the addition of treatment with an amplitude of 60% which produces a micro structure with the most fine grain. For 1-step sintering process, the highest hardness of 134.51 VHN obtained at 40 % amplitude. The hardness of the alloy depends on the size of the grain boundary associated with the difficulty of the dislocation movement.
BIOREDUCTION AND CHARACTERIZATION OF SILVER NANOPARTICLES FROM OIL PALM EMPTY FRUIT BUNCH Siti Suhartati; Iwan Syahjoko Saputra; Dwinna Rahmi; Yoki Yulizar; Sudirman Sudirman
Jurnal Sains Materi Indonesia Vol 21, No 4: JULY 2020
Publisher : Center for Science & Technology of Advanced Materials - National Nuclear Energy Agency

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.17146/jsmi.2020.21.4.6032

Abstract

BIOREDUCTION AND CHARACTERIZATION OF SILVER NANOPARTICLES FROM OIL PALM EMPTY FRUIT BUNCH (OPEFB). The synthesis of silver nanoparticles was successfully carried out by extracting oil palm empty fruit bunch. The precursor used was silver nitrate (AgNO3) with a concentration of 9x10-4 M and 5 wt% of the oil palm empty fruit bunch extract. OPEFB acted as a capping agent in the synthesis of silver nanoparticles. The bioreduction method Ag+ to Ag0 produced a silver nanoparticle colloid in brown color. The results of the UV-Vis spectrophotometer showed the silver nanoparticles colloids spectrum at a wavelength of 420 nm with an absorbance value of 0.5. FTIR shows the reduction and shift of absorption peak in the hydroxyl functional group (-OH) at wavenumbers of 3323 cm-1 and the presence of absorption peaks at 560 cm-1. While, XRD pattern showed the specific crystallinity peaks of silver nanoparticles at 2θ: 33.24°; 39.98°; 61.23°; dan 79.13° respectively with the face-centered cubic crystal structure (FCC) and crystallite size of 15 nm. PSA analysis showed two specific peaks with an average size distribution silver nanoparticles of 43.5 nm and a PDI value of 0.4. Analysis of TEM shows the average particle size of 20 nm with a spherical particle shape.
RADIATION SYNTHESIS OF POLY(VINYL ALCOHOL) PVA–(POLYVINYL PYRROLIDONE) PVP FOR IMMOBILIZATION OF CAPTOPRIL Hariyanti Hariyanti; Erizal Erizal; M Yasin Yunus; Indah Lestari; Ditri Risska Rahmadhani
Jurnal Sains Materi Indonesia Vol 21, No 4: JULY 2020
Publisher : Center for Science & Technology of Advanced Materials - National Nuclear Energy Agency

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.17146/jsmi.2020.21.4.5943

Abstract

RADIATION SYNTHESIS OF PVA POLY(VINYL ALCOHOL)–PVP (POLYVINYLPYRROLIDONE) for IMMOBILIZATION OF CAPTOPRIL. The aim of this work is to prepare Polyvinyl alcohol (PVA)- Polyvinylpyrrolidone (PVP) hydrogel with varying irradiation doses and drug dose to be used as a matrix for immobilization and control drug release of captopril. Immobilization and release of captopril in PVA-PVP hydrogel copolymer have been carried out. A mixture of PVA-PVP (6:4 w/w) solution containing captopril (10-20 mg), freeze-thawing, irradiated using gamma rays at various irradiation doses (0-20 kGy). The gel fraction and water absorption were determined gravimetrically. The pores structure of hydrogels were observed using SEM (Scanning Electron Microscope). The captopril released from hydrogel in NaCl 0.9% solution was measured using a UV-Vis spectrophotometer. After evaluated, it was found that with increasing dose up to 20 kGy, the gel fraction increases, and water absorption decreases, and the cumulative drug released decreases. SEM measurement showed that hydrogel had heterogeneous pores. PVA-PVP hydrogel prepared using gamma rays can be considered as a matrix for drug release.
KEYWORD INDEX Jusami Jusami
Jurnal Sains Materi Indonesia Vol 21, No 4: JULY 2020
Publisher : Center for Science & Technology of Advanced Materials - National Nuclear Energy Agency

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.17146/jsmi.2020.21.4.6468

Abstract

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