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Ekstraksi limonit dengan metode dua tahap reduksi selektif dan magnetic separation dengan variasi waktu tahan dan suhu rendah Budiyanto, Eko; Yuono, Lukito Dwi; Bahfie, Fathan; Sulistiyo, Danang
TURBO [Tulisan Riset Berbasis Online] Vol 10, No 1 (2021): Jurnal TURBO Juni 2021
Publisher : Universitas Muhammadiyah Metro

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.24127/trb.v10i1.1586

Abstract

The use of limonite and saprolite nickel ore with low Ni content as raw material for the manufacture of FeNi metal with a content of> 5% Ni has not been widely used. This is because to process limonite and saprolite ore into high levels of FeNi concentrate, it requires greater energy. The purpose of this study was to see the beneficiation process of low grade laterite nickel ore (limonite type, with 1-2% Ni content) at low temperature and holding time with graphite reducing agents and adding additives to iron nickel concentrate and nickel iron concentrates with nickel content above 5%. The method used in this research is to provide services with temperature variations of 250°C, 300°C, and 350°C with a holding time of 60 minutes and 90 minutes in the heat process stage 1 and continued in the heat process stage 2, namely at a temperature of 1150°C with a holding time of 60 minutes. The concentrates and tailings resulted from magnetic separation were then subjected to XRF testing and optical microscopy. With the erasing process and the holding time, the nickel content was quite high, namely 5-6%. With this, it can be neglected that the beneficiation process with this method is very effective and optimal. The levels of Fe in the concentrate obtained from several tests have increased and decreased with the addition of temperature and holding time.
DAMPAK PENINGKATAN PANAS DAN JENIS REDUKTAN TERHADAP SAPROLIT: STUDI PENDAHULUAN Bahfie, Fathan; Manaf, Azwar; Astuti, Widi; Nurjaman, Fajar; Prasetyo, Erik; Susanti, Diah; Sipahutar, Wahyu Solafide
Indonesian Mining Journal Vol 27 No 1 (2024): Indonesian Mining Journal, April 2024
Publisher : Balai Besar Pengujian Mineral dan Batubara tekMIRA

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.30556/imj.Vol27.No1.2024.1533

Abstract

Indonesia significantly contributes to the global electric vehicle battery market due to its substantial medium- and low-grade nickel reserves. This study utilized saprolitic nickel ore from Halmahera, Maluku, Indonesia. However, the research on saprolite needs some improvements due to its complex mineral composition, which affected on the roasting process significantly. Therefore, a thorough understanding of the properties of laterite ores is critically important, particularly concerning laterite pre-reduction processes. The ore was finely sieved to a particle size of less than 100 mesh and then heated at temperatures of 250, 900, and 1150°C with the variation of reductant (anthracite and palm kernel charcoal). Extensive mineralogical analysis was conducted using X-ray diffraction (XRD), X-ray fluorescence (XRF), and scanning electron microscopy with energy-dispersive spectroscopy (SEM-EDS). The analysis of saprolite showed that it contains about 1.82% nickel, 30.47% iron, 10-20% magnesium, 4.86% aluminum, and 8.1% silicon by weight. Its mineral composition is mainly 53.1% goethite, 38.3% lizardite, and 8.7% quartz. The study found that goethite in saprolite was transformed into hematite around 250°C. At 900°C, the forsterite was crystallized, and at 1150°C, the ferronickel was formed. The transformation of lizardite is important as it affected on nickel diffusion within the iron matrix, which impacted on the material's properties. A thermal upgrading method with reductants like anthracite and palm kernel charcoal was used at lower temperatures to enhance the properties of saprolite. These findings provided valuable insights into saprolite's mineralogical composition and behavior, potentially offering improvements in various industrial processes and applications.
DAMPAK PENINGKATAN PANAS DAN JENIS REDUKTAN TERHADAP SAPROLIT: STUDI PENDAHULUAN Bahfie, Fathan; Manaf, Azwar; Astuti, Widi; Nurjaman, Fajar; Prasetyo, Erik; Susanti, Diah; Sipahutar, Wahyu Solafide
Indonesian Mining Journal Vol 27 No 1 (2024): Indonesian Mining Journal, April 2024
Publisher : Balai Besar Pengujian Mineral dan Batubara tekMIRA

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.30556/imj.Vol27.No1.2024.1533

Abstract

Indonesia significantly contributes to the global electric vehicle battery market due to its substantial medium- and low-grade nickel reserves. This study utilized saprolitic nickel ore from Halmahera, Maluku, Indonesia. However, the research on saprolite needs some improvements due to its complex mineral composition, which affected on the roasting process significantly. Therefore, a thorough understanding of the properties of laterite ores is critically important, particularly concerning laterite pre-reduction processes. The ore was finely sieved to a particle size of less than 100 mesh and then heated at temperatures of 250, 900, and 1150°C with the variation of reductant (anthracite and palm kernel charcoal). Extensive mineralogical analysis was conducted using X-ray diffraction (XRD), X-ray fluorescence (XRF), and scanning electron microscopy with energy-dispersive spectroscopy (SEM-EDS). The analysis of saprolite showed that it contains about 1.82% nickel, 30.47% iron, 10-20% magnesium, 4.86% aluminum, and 8.1% silicon by weight. Its mineral composition is mainly 53.1% goethite, 38.3% lizardite, and 8.7% quartz. The study found that goethite in saprolite was transformed into hematite around 250°C. At 900°C, the forsterite was crystallized, and at 1150°C, the ferronickel was formed. The transformation of lizardite is important as it affected on nickel diffusion within the iron matrix, which impacted on the material's properties. A thermal upgrading method with reductants like anthracite and palm kernel charcoal was used at lower temperatures to enhance the properties of saprolite. These findings provided valuable insights into saprolite's mineralogical composition and behavior, potentially offering improvements in various industrial processes and applications.
Studi pengaruh kadar mangan dan temperatur austenisasi terhadap struktur mikro dan sifat mekanik baja mangan Bahfie, Fathan; Aleiya, Zakhrofa; Milandia, Anistasia; Nurjaman, Fajar
Dinamika Teknik Mesin: Jurnal Keilmuan dan Terapan Teknik Mesin Vol 10, No 1 (2020): Dinamika Teknik Mesin: Jurnal Keilmuan dan Terapan Teknik Mesin
Publisher : Universitas Mataram

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (306.34 KB) | DOI: 10.29303/dtm.v10i1.317

Abstract

High manganese steel or austenitic manganese steelcommonly are used in mining industries such as thecomponent in an excavator, hammer mill, crusher, andjaw crusher plates. Those components are the alloy caststeel with containing manganese (Mn) about 11-18%.The mechanical properties of austenitic manganesesteel are depending on the amount of manganese andcarbon. The austenitic steel has three dominantproperties, i.e. high hardness; good wear resistance, andhigh impact resistance. The objectives of this researchare investigating the effect of the composition ofmanganese and the austenitization temperature on themicrostructure and mechanical properties of austeniticmanganese steel. Each variation of manganesecomposition was 5.87%. 9.42% and 15.28%. It washeated at 950, 1000 and 1050oC for 60 minutes and thenquenched with water. The result showed that the highesthardness was 46 HRC where the composition ofmanganese and the austenitization temperature was5.87%. and 1050oC. The lowest hardness number was16.3 HRC where the content of manganese and thetemperature was 9.42%. and 1050oC. The results agreedwith the microstructure of the increase in carbides andthe composition of manganese increased too. For thewear resistance properties, the optimum one was 6.78 x10-6 mm3/m at the composition of manganese andtemperature of 5.87% and 1050oC.