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All Journal Jurnal Neutrino : jurnal fisika dan aplikasinya Alchemy : Journal of Chemistry SAINSTIS Bulletin of Chemical Reaction Engineering & Catalysis The Journal of Pure and Applied Chemistry Research JC-T (Journal Cis-Trans): Jurnal Kimia dan Terapannya Science and Technology Indonesia ALCHEMY Jurnal Penelitian Kimia JKPK (Jurnal Kimia dan Pendidikan Kimia) Bulletin of Chemical Reaction Engineering & Catalysis al Kimiya : Jurnal Ilmu Kimia dan Terapan JURNAL REKAYASA KIMIA & LINGKUNGAN
Anton Prasetyo
Program Studi Kimia, Fakultas Sains Dan Teknologi, UIN Maulana Malik Ibrahim Malang
Biochemistry, Genetics & Molecular Biology Chemical Engineering, Chemistry & Bioengineering Chemistry Education Energy Engineering Environmental Science Materials Science & Nanotechnology Medicine & Pharmacology Physics

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Journal : The Journal of Pure and Applied Chemistry Research

 1 
The Effect of Temperature Synthesis on the Plate-Like Particle of Bi4Ti3O12 Obtained by Single Molten NaCl Salt Sheley Marela; Nur Aini; Arie Hardian; Veinardi Suendo; Anton Prasetyo
The Journal of Pure and Applied Chemistry Research Vol 10, No 1 (2021): Edition January-April 2021
Publisher : Chemistry Department, The University of Brawijaya

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.21776/ub.jpacr.2021.010.01.570

Abstract

Three-layer Aurivillius compound bismuth titanate (Bi4Ti3O12) is well known for having interesting properties such as ferroelectric and photocatalyst. Many researchers reported that the unique plate-like shaped particle affecting ferroelectric and photocatalyst properties. The molten salt synthesis is the common simple method to obtain that unique morphology. In this research, Bi4Ti3O12 was synthesized using single molten salt NaCl at various temperatures, which is 800, 850, 900, and 950 oC. X-Ray Diffraction data showed that all obtained Bi4Ti3O12 have a B2cb space group with no impurities detected. The Raman spectra shows the characteristic vibration modes of Bi4Ti3O12 at 62, 117, 228, 269, 332, 364, 536, 851 cm-1. The plate-like shaped particle was confirmed by SEM analysis. Based on SEM images, the size of the particle increased along with the synthesis temperature, which is due to the thermal effect on grain growth.
Synthesis of Microsheets Bi4Ti3O12 and Bi4Ti2.95V0.05O12 via Molten NaCl-KCl Salt Method Anton Prasetyo; Andy Nur Muhammad Guntur; Suci Noerfaiqotul Himmah; Nur Aini; Usman Ali Rouf; Abdul Aziz
The Journal of Pure and Applied Chemistry Research Vol 11, No 3 (2022): Edition September-December 2022
Publisher : Chemistry Department, The University of Brawijaya

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.21776/ub.jpacr.2022.011.03.703

Abstract

Bi4Ti3O12 is a tri-layer Aurivillius member compound that was reported to have good photocatalytic properties. Metal element doping and morphological particle tuning are strategies to increase photocatalyst activity. In this research, the compound micro sheets Bi4Ti3O12 and Bi4Ti2.95V0.05O12 were synthesized using molten NaCl/KCl salt. The diffractogram shows that the Bi4Ti3O12 sample was successfully synthesized, however, there are still found impurities at the Bi4Ti2.95V0.05O12 sample. Micrographs showed that the morphology particle samples is. The results of UV-Vis DRS spectra calculation show that both samples have a band gap energy of ~2.97 eV.
Co-Authors Abdul Aziz Abi Dwi Hastono Agie Botianovi Aldi Dwi Prasetiyo Aminatus Arifah Andy Nur Muhammad Guntur Arie Hardian Dwi Rahayu Novianti Erna Hastuti Fahmi Eksa Sagita Fikri Haikal Fikri Haikal Fikri Haikal Hadi Nur Hasal Maulidianingtiyas Himmatul Barroroh Indra Nur Cahyo Khoridatud Diyanah Maksum Maksum Mohamad Thoif Muhammad Lathif al-Abror Mukhamad Nurhadi, Mukhamad Nabila Nur Agusti Nur Aini Nur Aini Nur Robi'ah Adawiyah Mahmud Puspa Sari Ratna Kusumawardani, Ratna Rini Nafsiati Saiyidatul Umah Sheley Marela Sin Yuan Lai Siti Nur Chasanah Suci Noerfaiqotul Himmah Suci Noerfaiqotul Himmah Susi Nurul Khalifah Susi Nurul Kholifah Teguh Wirawan Usman Ali Rouf Usman Ali Rouf Veinardi Suendo Vina Nurul Istighfarini