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All Journal Bulletin of Chemical Reaction Engineering & Catalysis Jurnal Zarah Orbital: Jurnal Pendidikan Kimia JKPK (Jurnal Kimia dan Pendidikan Kimia) SAP (Susunan Artikel Pendidikan) Bivalen: Chemical Studies Journal UNESA Journal of Chemical Education Prosiding Seminar Nasional PPG Universitas Mulawarman Bulletin of Chemical Reaction Engineering & Catalysis

Mukhamad Nurhadi, Mukhamad

Program Magister Pendidikan Kimia, Fakultas Keguruan Dan Ilmu Pendidikan, Universitas Mulawarman

Author-ID : 3273174

Religion Humanities Chemical Engineering, Chemistry & Bioengineering Chemistry Computer Science & IT Education Other

Published : 43 Documents Claim Missing Document

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PENERAPAN MODEL PEMBELAJARAN BERBASIS MASALAH UNTUK MENURUNKAN MISKONSEPSI SISWA TENTANG KONSEP REAKSI REDOKS rizki, Maulidina; Nurhadi, Mukhamad; Widiyowati, Iis Intan
Jurnal Zarah Vol 8 No 1 (2020): Jurnal Zarah
Publisher : Fakultas Keguruan dan Ilmu Pendidikan, Universitas Maritim Raja Ali Haji

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.31629/zarah.v8i1.1974

Penelitian ini bertujuan untuk mengetahui penerapan model Pembelajaran Berbasis Masalah (PBM) untuk mengurangi miskonsepsi tentang pokok bahasan reaksi redoks. Sampel pada penelitian ini adalah siswa kelas X MIPA 1 SMAN 8 Samarinda yang berjumlah 35 siswa. Teknik pengambilan sampel yang dilakukan yaitu purposive sampling. Pengumpulan data menggunakan teknik tes berupa soal ulangan harian yang dilengkapi pendeteksi miskonsepsi tipe Three Tier Diagnostic Test dan teknik non tes sebagai data penunjang penelitian. Hasil penelitian menunjukkan miskonsepsi rata-rata siswa pada pembelajaran langsung adalah 50,71% dan setelah diterapkan pembelajaran ulang menggunakan model PBM rata-rata miskonsepsi siswa turun menjadi 12,14%. Berdasarkan hasil analisis data miskonsepsi tersebut diperoleh kesimpulan bahwa penerapan model pembelajaran PBM dapat mengurangi miskonsepsi siswa tentang konsep reaksi redoks sebesar 76,05%.

EFEKTIVITAS PENGGUNAAN MODEL PEMBELAJARAN POGIL UNTUK MENURUNKAN MISKONSEPSI SISWA KELAS XI MIPA 5 DI SMA NEGERI 4 SAMARINDA PADA POKOK BAHASAN HIDROLISIS GARAM Arpiana, Devi; Nurhadi, Mukhamad
Jurnal Zarah Vol 8 No 1 (2020): Jurnal Zarah
Publisher : Fakultas Keguruan dan Ilmu Pendidikan, Universitas Maritim Raja Ali Haji

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.31629/zarah.v8i1.2055

Penelitian ini bertujuan untuk mengetahui efektivitas penggunaan model pembelajaran POGIL untuk menurunkan miskonsepsi siswa kelas XI MIPA 5 di SMA Negeri 4 Samarinda pada pokok bahasan hidrolisis garam. Subjek dalam penelitian ini adalah siswa kelas XI MIPA 5 yang berjumlah 36 siswa. Penggunaan model pembelajaran langsung menjadi kegiatan belajar pertama untuk mengetahui miskonsepsi awal yang terjadi pada siswa. Selanjutnya dilakukan dengan pengulangan kegiatan belajar dengan menggunakan model pembelajaran POGIL. Instrumen yang digunakan untuk mengukur miskonsepsi yang terjadi pada siswa adalah Three Tier Diagnostic Test. Hasil penelitian menunjukkan bahwa miskonsepsi yang terjadi pada pembelajaran langsung sebesar 63,89% dan menurun sebesar 26,94% pada pembelajaran POGIL. Sehingga dapat disimpulkan bahwa penggunaan model pembelajaran POGIL berhasil dan efektif digunakan dalam pengurangan miskonsepsi siswa sebesar 57,83%.

PENGARUH PENGGUNAAN MEDIA ROLLING BALL DALAM MODEL PEMBELAJARAN PREDICT, OBSERVE, EXPLAIN (POE) TERHADAP HASIL BELAJAR KIMIA PADA MATERI LAJU REAKSI Abdurrahim; Nurhadi, Mukhamad; Hartati, Yuli
Jurnal Zarah Vol 8 No 1 (2020): Jurnal Zarah
Publisher : Fakultas Keguruan dan Ilmu Pendidikan, Universitas Maritim Raja Ali Haji

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.31629/zarah.v8i1.2130

Penelitian ini bertujuan untuk mengetahui pengaruh penggunaan media Rolling Ball dalam model pembelajaran Predict, Observe, Explain (POE) terhadap hasil belajar kimia kelas XI IPA pada materi laju reaksi di SMA Negeri 4 Samarinda tahun ajaran 2019/2020. Penggunaan media Rolling Ball dapat meningkatkan kreatifitas dan keaktifan siswa melalui model pembelajaran POEdalam 3 tahapan utama, yaitu memprediksi apa yang terjadi (predict), melakukan pengamatan dan diskusi untuk membuktikan prediksi (observe), dan menjelaskan hasil pengamatan dan diskusi (explain). Jenis penelitian yang digunakan adalah Static Group Comparison dengan metode pre-experimental. Sampel dalam penelitian ini adalah siswa kelas XI MIPA 1 (eksperimen) dan kelas XI MIPA 2 (kontrol), dengan jumlah siswa masing-masing sebanyak 36 siswa. Hasil penelitian menunjukkan nilai rata-rata kelas eksperimen adalah 89,11 dan kelas kontrol adalah 86,11. Data kemudian dianalisis dengan menggunakan uji t, dan didapatkan thitung > ttabel yaitu sebesar 3,89 > 1,67, sehingga dapat disimpulkan terdapat pengaruh penggunaan media Rolling Ball dalammodel pembelajaran POE terhadap hasil belajar siswa kelas XI IPA pada materi laju reaksi di SMA Negeri 4 Samarinda tahun ajaran 2019/2020 pada taraf signifikan 5%.

PENGEMBANGAN MODUL KIMIA BERBASIS MULTIPEL REPRESENTASI BERBANTUAN POWERPOINT PADA MATERI LARUTAN ELEKTROLIT DAN NON ELEKTROLIT Herman, Heri; Nurhadi, Mukhamad; Gunawan, Rahmat
Jurnal Zarah Vol 9 No 1 (2021): Jurnal Zarah
Publisher : Fakultas Keguruan dan Ilmu Pendidikan, Universitas Maritim Raja Ali Haji

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.31629/zarah.v9i1.2323

Penelitian ini bertujuan untuk mengembangkan modul pembelajaran kimia berbasis multipel representasi berbantuan powerpoint pada pokok bahasan larutan elektrolit dan non elektrolit yang valid, efektif, dan praktis. Metode penelitian yang digunakan adalah metode research and development (R&D) dengan mengadaptasi model pengembangan ADDIE yang dikembangkan oleh Robert Maribe Branch yang terdiri atas analysis, design, development, implementation, evaluation. Sampel penelitian ini adalah 30 siswa kelas X IPA SMAN 12 Samarinda. Teknik pengumpulan data yang digunakan adalah angket dan tes dengan instrumen penelitian berupa lembar validasi, soal pretest dan posttest, dan angket respon siswa. Hasil analisis menunjukkan bahwa modul dan animasi sangat valid dengan nilai validasi dari ahli materi sebesar 94,60%, ahli media sebesar 90,91%, dan ahli IT sebesar 86,84%. Kepraktisan berdasarkan hasil analisis angket respon siswa sebesar 88,01% dengan kriteria sangat praktis. Keefektifan berdasarkan hasil analisis pretest dan posttest siswa dengan nilai N-gain sebesar 0,78 dengan kriteria sangat efektif. Dengan demikian, modul dan powerpoint pembelajaran yang dikembangkan layak digunakan sebagai sumber belajar siswa kelas X IPA dan guru mata pelajaran kimia.

Effective TiO2-Sulfonated Carbon-derived from Eichhornia crassipes in The Removal of Methylene Blue and Congo Red Dyes from Aqueous Solution Iis Intan Widiyowati; Mukhamad Nurhadi; Muhammad Hatami; Lai Sin Yuan
Bulletin of Chemical Reaction Engineering & Catalysis 2020: BCREC Volume 15 Issue 2 Year 2020 (August 2020)
Publisher : Department of Chemical Engineering - Diponegoro University

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.9767/bcrec.15.2.6997.476-489

The study of TiO2-sulfonated carbon-derived from Eichhornia crassipes (TiO2/SCEC), as an effective adsorbent to remove Methylene blue (MB) and Congo red (CR) dyes from aqueous solution, has been conducted. The preparation steps of TiO2/SCEC adsorbent involved the carbonisation of E. crassipes powder at 600 °C for 1 h, followed by sulfonation of carbon for 3 h and impregnation through titanium(IV) isopropoxide (500 µmol). The physical properties of the adsorbents were characterized by using X-ray fluorescence (XRF), Fourier transform infrared, X-ray diffraction (XRD), Scanning electron microscopy with Energy dispersive X-ray (SEM-EDX), Thermogravimetric analysis (TGA) and nitrogen adsorption-desorption studies. The dye removal study using TiO2/SCEC adsorbent was carried out by varying of contact time, adsorbent dosage, initial dye concentration, pH, particles size of adsorbent and temperature. The kinetics models were determined by the effects of contact time and the thermodynamic parameters (ΔH, ΔS, and ΔG), which were calculated by the effects of temperature. The results showed that the maximum dye removal capacity of TiO2/SCEC were 18.8 mg.g-1 for MB and 36.5 mg.g-1 for CR. The removal of MB and CR dyes using TiO2/SCEC adsorbent performed a pseudo-second order kinetic models with spontaneity. Copyright © 2020 by Authors, Published by BCREC Group. This is an open access article under the CC BY-SA License (https://creativecommons.org/licenses/by-sa/4.0).

Kinetic Study of Styrene Oxidation over Titania Catalyst Supported on Sulfonated Fish Bone-derived Carbon Ratna Kusumawardani; Mukhamad Nurhadi; Teguh Wirawan; Anton Prasetyo; Nabila Nur Agusti; Sin Yuan Lai; Hadi Nur
Bulletin of Chemical Reaction Engineering & Catalysis 2022: BCREC Volume 17 Issue 1 Year 2022 (March 2022)
Publisher : Department of Chemical Engineering - Diponegoro University

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.9767/bcrec.17.1.13133.194-204

The kinetic evaluation of titania supported sulfonated fish bone-derived carbon (TiO2/SFBC) as a catalyst in styrene oxidation by aqueous hydrogen peroxide was carried out. The catalysts were prepared by carbonation of fishbone powder at varying temperatures 500, 600 and 700 °C, respectively for 2 h, followed by sulfonation with sulfuric acid (1M) for 24 h and impregnated by varied titania concentration 500, 1000 and 1500 µmol. The physical properties of catalysts were characterized using Fourier transform infrared (FTIR) spectroscopy, X-ray diffraction (XRD), Scanning Electron Microscope-Energy Dispersive X-Ray (SEM-EDX) and the nitrogen adsorption-desorption analysis. The catalytic activity result showed that TiO2/SFBC can be used as a potential catalyst in styrene oxidation. Worth noting that the sulfonation process has not only transformed the TiO2/FBC particulates (without sulfonation) to cuboid-shaped TiO2/SFBC (with sulfonation) but also contributed to the high selectivity of benzaldehyde. On the other hand, carbonization at different temperatures has an indistinct effect on catalytic performance due to their similar surface areas. The styrene conversion rate responded positively with the increasing amount of titania in the functionalized composites. The styrene oxidation by aqueous H2O2 unraveled the first-order reaction with the activation energy of ⁓63.5 kJ. Copyright © 2022 by Authors, Published by BCREC Group. This is an open access article under the CC BY-SA License (https://creativecommons.org/licenses/by-sa/4.0).

Carbon-containing Hydroxyapatite Obtained from Fish Bone as Low-cost Mesoporous Material for Methylene Blue Adsorption Mukhamad Nurhadi; Ratna Kusumawardani; Wirhanuddin Wirhanuddin; Rahmat Gunawan; Hadi Nur
Bulletin of Chemical Reaction Engineering & Catalysis 2019: BCREC Volume 14 Issue 3 Year 2019 (December 2019)
Publisher : Department of Chemical Engineering - Diponegoro University

The carbon-containing hydroxyapatite has been synthesized using the fish bone obtained from East Kalimantan, Indonesia. The synthesis was conducted at varying calcination temperature (300-700 °C) and duration time (1-5 h). The carbon-containing hydroxyapatite were characterized by using Nitrogen adsorption-desorption, Fourier transform infrared spectroscopy, X-ray diffraction (XRD), Scanning electron microscopy (SEM), and Thermogravimetric analysis (TGA) and Differential thermal analysis (DTA). The carbon-containing hydroxyapatite nanoparticles consisted of the mesoporous structure with a specific surface area of 159 m2.g-1 and pore size of 44 Å. The carbon-containing hydroxyapatite nanoparticles were utilized as the adsorbent for the removal of methylene blue by varying the contact time, initial dye concentration, pH, adsorbent dosage and temperature. The maximum amount of adsorption capacity was 56.49 mg.g-1. The adsorption was well fitted with the Langmuir adsorption model (R2 ~ 0.998) and the pseudo-second-order model. This indicated that the dye molecules were adsorbed on the surface-active site of carbon-containing hydroxyapatite via chemical binding, forming an adsorbate monolayer. Hence, the adsorption capability corresponds to the physical properties such as the surface area and pore volume of hydroxyapatite because the larger surface area consists of higher binding sites for the adsorption. Thermodynamic parameters, including the Gibbs free energy (ΔG), enthalpy (ΔH), and entropy (ΔS), indicated that the adsorption of methylene blue onto the carbon-containing hydroxyapatite nanoparticles was spontaneous. Thus, carbon-containing hydroxyapatite nanoparticles can be applied as a low-cost adsorbent for the treatment of industrial effluents that are contaminated with the methylene blue.

Kinetic of Adsorption Process of Sulfonated Carbon-derived from Eichhornia crassipes in the Adsorption of Methylene Blue Dye from Aqueous Solution Mukhamad Nurhadi; Iis Intan Widiyowati; Wirhanuddin Wirhanuddin; Sheela Chandren
Bulletin of Chemical Reaction Engineering & Catalysis 2019: BCREC Volume 14 Issue 1 Year 2019 (April 2019)
Publisher : Department of Chemical Engineering - Diponegoro University

The evaluation of kinetic adsorption process of sulfonated carbon-derived from Eichhornia crassipes in the adsorption of methylene blue dye from aqueous solution has been carried out. The sulfonated carbon-derived from E. crassipes (EGS-600) was prepared by carbonation of E. crassipes powder at 600 °C for 1 h, followed by sulfonation with concentrated sulfuric acid for 3 h. The physical properties of the adsorbents were characterized by using Fourier transform infrared spectroscopy, X-ray diffraction (XRD), scanning electron microscopy (SEM), and nitrogen adsorption-desorption studies. Adsorption study using methylene blue dye was carried out by varying the contact time and initial dye concentration for investigated kinetics adsorption models. The effect of varying temperature was used to determine the thermodynamic parameter value of ΔG, ΔH, and ΔS. The results showed that the equilibrium adsorption capacity was 98% when EGS-600 is used as an adsorbent. The methylene blue dye adsorption onto adsorbent takes place spontaneity and follows a pseudo-second-order adsorption kinetic model.

Catalytic Performance of TiO2–Carbon Mesoporous-Derived from Fish Bones in Styrene Oxidation with Aqueous Hydrogen Peroxide as an Oxidant Mukhamad Nurhadi; Ratna Kusumawardani; Teguh Wirawan; Sumari Sumari; Sin Yuan Lai; Hadi Nur
Bulletin of Chemical Reaction Engineering & Catalysis 2021: BCREC Volume 16 Issue 1 Year 2021 (March 2021)
Publisher : Department of Chemical Engineering - Diponegoro University

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.9767/bcrec.16.1.9729.88-96

The catalytic performance of titania-supported carbon mesoporous-derived from fish bones (TiO2/CFB) has been investigated in styrene oxidation with aqueous H2O2. The preparation steps of (TiO2/CFB) catalyst involved the carbonization of fish bones powder at 500 °C for 2 h. followed by impregnation of titania using titanium(IV) isopropoxide (500 µmol) precursor, and calcined at 350 °C for 3 h. The physical properties of the adsorbents were characterized using Fourier transform infrared, X-ray diffraction (XRD), Scanning electron microscopy with energy dispersive X-ray (SEM-EDX), and nitrogen adsorption-desorption studies. The catalytic test was carried out using styrene oxidation with H2O2 as an oxidant at room temperature for 24 h. Its catalytic activity was compared with Fe2O3/CFB, CuO/CFB, TiO2, and CFB catalysts. It is demonstrated that the catalytic activity of TiO2/CFB catalyst has the highest compared to Fe2O3/CFB, CuO/CFB, TiO2, and CFB catalysts in the oxidation of styrene with styrene conversion ~23% and benzaldehyde selectivity ~90%. Kinetics of TiO2/CFB catalyzed oxidation of styrene has been investigated and mechanism for oxidation of styrene has been proposed. Copyright © 2021 by Authors, Published by BCREC Group. This is an open access article under the CC BY-SA License (https://creativecommons.org/licenses/by-sa/4.0).

Modification of Coal Char-loaded TiO2 by Sulfonation and Alkylsilylation to Enhance Catalytic Activity in Styrene Oxidation with Hydrogen Peroxide as Oxidant Mukhamad Nurhadi
Bulletin of Chemical Reaction Engineering & Catalysis 2017: BCREC Volume 12 Issue 1 Year 2017 (April 2017)
Publisher : Department of Chemical Engineering - Diponegoro University

The modified coal char from low-rank coal by sulfonation, titanium impregnation and followed by alkyl silylation possesses high catalytic activity in styrene oxidation. The surface of coal char was undergone several steps as such: modification using concentrated sulfuric acid in the sulfonation process, impregnation of 500 mmol titanium(IV) isopropoxide and followed by alkyl silylation of n-octadecyltriclorosilane (OTS). The catalysts were characterized by X-ray diffraction (XRD), IR spectroscopy, nitrogen adsorption, and hydrophobicity. The catalytic activity of the catalysts has been examined in the liquid phase styrene oxidation by using aqueous hydrogen peroxide as oxidant. The catalytic study showed the alkyl silylation could enhance the catalytic activity of Ti-SO3H/CC-600(2.0). High catalytic activity and reusability of the o-Ti-SO3H/CC-600(2.0) were related to the modification of local environment of titanium active sites and the enhancement the hydrophobicity of catalyst particle by alkyl silylation.

Co-Authors Abdul Majid Abdul Majid Alsultan, Abdulkareem Ghassan Anjelica Octavia Arung Anton Prasetyo Arpiana, Devi A’an Suri Purwandari Cheng Loong Ngan Darna Yunita Degirmenci, Volkan Eko Saputro Fahria Aryani Farah Erika Fathur Insani Ridho Goh, Chien Yong Guo, Yubei Hadi Nur Hadi Nur Hadi Nur Hadi Nur Hadi Nur Hadi Nur Hadi Nur Hadi Nur Hadi Nur Haiyan Li Hartati, Yuli Herman, Heri Iis Intan Widiyowati Jefi Jefi Kelvert Kong Lai Sin Yuan Lai, Sin Yuan Lau, Alysa Lik Quan Lau Maasje C. Watulingas Mahashanon Arumugam Maria Ulfah Maulidina Rizki Medita Hermawanti Muhammad Hatami Munik Endang Rizkiana Mursyidah Mursyidah Nabila Nur Agusti Nazarudin Nazihah, Diyani Septihadi Nezalsa Fortuna Nova Sukmawati Muskita Nur Anisa, Nela Octavia A., Anjelica Pintaka Kusumaningtyas Pristiningtyas Ambarwati Rahmadani, Agung Rahmat Gunawan RAHMAT GUNAWAN Ratna Kusuma Wardani Ratna Kusumawardani, Ratna Retno Pujisupiati Rezky Oktafiani Rinda Angghita Putri Rizky Handayani Robbiatul Adawiyah Rony, Zahara Tussoleha Sekar Sulistyaningwarni Sheela Chandren Sheela Chandren Siew Fan Wong Sin Yuan Lai Sin Yuan Lai Sin Yuan Lai Sin Yuan Lai Sin Yuan Lai Sin Yuan Lai Sin Yuan Lai Sin Yuan Lai Siti Mutmainah Siti Rahma Soerja Koesnarpadi Sri Lestari Suciyanti Jufri Sulastria Marsuki Sumari Sumari Syaiful Bahri Teguh Wirawan Teguh Wirawan, Teguh Usman Sain Watulingas, Maasje C. Wirhanuddin Wirhanuddin Wirhanuddin, Wirhanuddin Yun Hin, Taufiq-Yap Yuniar Ponco Prananto Yuniati Mangesa Zhiying Zhu Zhiying Zhu

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