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All Journal EKSAKTA: Journal of Sciences and Data Analysis Alchemy : Journal of Chemistry Agrovigor: Jurnal Agroekoteknologi CHEMPUBLISH JOURNAL Bubungan Tinggi: Jurnal Pengabdian Masyarakat Bima Abdi: Jurnal Pengabdian Masyarakat Journal of Agro Plantation (JAP)
Sarwendah Ratnawati Hermanto
Politeknik Negeri Ketapang
Agriculture, Biological Sciences & Forestry Chemical Engineering, Chemistry & Bioengineering Chemistry Earth & Planetary Sciences Education Energy Languange, Linguistic, Communication & Media Materials Science & Nanotechnology Social Sciences Other

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Journal : EKSAKTA: Journal of Sciences and Data Analysis

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Saccharin Extraction And Analysis Of Drug And Food Samples By Derivative Ultraviolet (UV) Spectrophotometry Sarwendah Ratnawati Hermanto; Roto Roto; Agus Kuncaka
EKSAKTA: Journal of Sciences and Data Analysis VOLUME 18, ISSUE 2, August 2018
Publisher : Fakultas Matematika dan Ilmu Pengetahuan Alam

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.20885/eksakta.vol18.iss2.art1

Abstract

Saccharin extraction and analysis of drug and food samples was investegated by spectrophotometry ultraviolet (uv) derivative method were studied. The saccharin extraction was carried out using solvent of ethanol/chloroform (2:8 v/v). The limit of detection (LOD) and limit of quantification (LOQ) of the proposed method were  0.50 ppm and 1.82 ppm for the second order and 0.47 ppm and 1.58 ppm for the fourth, while for the zero order were 2,75 ppm and 8,55 ppm. The calibration curve was linear in the concentration range from 20-100 ppm (R2= 0.996 for the second order and R2=0.997 for the fourth). The percent recovery of saccharin was in the range 95.20-104.40% for the second order and 97.20-102.40% for the fourth. The range of saccharin concentration (w/w) in drugs, candies and toothpaste for the fourth derivative were 1.39±0.02 mg/kg until 7.15±0.05 mg/kg, 0.21±0.01 mg/kg until 2.09±0.01 mg/kg, and 0.15±0.03 mg/kg until 0.63±0.04 mg/kg, respectively. 
Co-Authors Agus Kuncaka Ahmad Ravi akhdiyatul, akhdiyatul Alfath Desita Jumiar Beny Setiawan Elan Adiat Nur Endang Tri Wahyuni Eni Aprianingrum Indra Pratiwi Isna Nurhidayati Nur Aida Nurhayati Nurhayati Nurul Hidayat Aprilita Polonia, Betti Ses Eka Rosmalinda Rosmalinda Roto Roto Sawaludin Sopiana Sopiana Umroh Umroh Venti Jatsiyah