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All Journal JURNAL KIMIA SAINS DAN APLIKASI Jurnal Teknosains
Susanto Susanto
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Pencucian material magnetik pasir besi lansilowo menggunakan larutan asam klorida Ricka Prasdiantika; Susanto Susanto
Jurnal Teknosains Vol 10, No 1 (2020): December
Publisher : Universitas Gadjah Mada

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.22146/teknosains.43985

Abstract

Iron sand was widely used in various fields such as in the manufacturing of magnets, cement, and steel. Iron sand has the main composition of iron oxide and several impurities of oxides. To remove these impurities, iron sand needs to be washed with acidic solution such as HCl solution. This study aims to minimize impurities in the magnetic material of Lansilowo iron sand. Iron sand was prepared using an external magnet to obtain magnetic material. The magnetic material was washed using distilled water and 0.5 M HCl solution. The drying process was carried out at 80oC for 24 hours. Magnetic material was crushed, weighed, and characterized. Material characterization was carried out using X-Ray Fluorescence (XRF), Fourier Transform Infrared (FT-IR) Spectrophotometer, and X-Ray Diffractometer (XRD). The Characterization results showed that washing of magnetic material using H2O-HCl 0.5 M was able to increase the percentage of Fe element composition in Lansilowo iron sand. The iron oxide contained in Lansilowo Iron Sand remains magnetite. The washing the iron sand magnetic material using 0.5 M HCl solution succeeded in removing impurities such as Mg, Pr, K, Cl, P, S, Co, Ce, and Sn as well as reducing the percentage of the Si and Al elements.The washing magnetic material using 0.5 M H2O-HCl produced higher XRD intensities than those washed with H2O. The washing magnetic material with 0.5 M H2O-HCl was result particle size of 37,70 ± 4,62 nm and crystallinity of 53.12%.
Synthesis and Characterization of Triamine modified coated Iron Sand Hybrid Nanomaterials originating from Kendal Coast Ricka Prasdiantika; Susanto Susanto; Yustika Kusumawardani
Jurnal Kimia Sains dan Aplikasi Vol 23, No 3 (2020): Volume 23 Issue 3 Year 2020
Publisher : Chemistry Department, Faculty of Sciences and Mathematics, Diponegoro University

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (3731.456 KB) | DOI: 10.14710/jksa.23.3.68-74

Abstract

Nanomaterials have broad and unique applications in various fields. In this research, synthesis of Iron Sand Magnetic Hybrid nanomaterials coated with propyldiethylenetriammine modified silica (PB@SiO2@TA) originating from the coast of Muara Kencan, Kendal Regency. This study began with iron sand preparation, continued with activation, dispersing iron sand, then coating iron sand with propyldiethylenetriammine modified silica. The resulting product was characterized by X-Ray Fluorescence (XRF), Fourier Transform Infrared (FT-IR) Spectrophotometer, X-Ray Diffractometer (XRD), and Transmission Electron Microscope (TEM). The characterization results show that the iron sand of the coast of Muara Kencan Beach has a high iron oxide content (81.66%) with minerals in the form of magnetite. The characterization results also showed that the nanomaterial hybrid iron sand coated with propyldiethylenetriammine modified silica (PB@SiO2@TA) was successfully synthesized with a crystal size of 36.21 nm, with better particle dispersion than the prepared iron sand.
Co-Authors Ricka Prasdiantika Yustika Kusumawardani