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All Journal IJFAC (Indonesian Journal of Fundamental and Applied Chemistry) JURNAL REKAYASA KIMIA & LINGKUNGAN
Lelifajri Lelifajri
Jurusan Kimia, Fakultas Matematika dan Ilmu Pengetahuan Alam, Universitas Syiah Kuala
Biochemistry, Genetics & Molecular Biology Chemical Engineering, Chemistry & Bioengineering Chemistry Energy Engineering Environmental Science

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Distribution pattern of Pb and Zn contamination in rivers near industrial zone in Aceh, Indonesia, revealed by principal component analysis (PCA) Lelifajri, Lelifajri; Rahmadi, Rahmadi; Idroes, Rinaldi; Supriatno, Supriatno; Safitri, Eka; Nazaruddin, Nazaruddin; Maulana, Ilham; Suhud, Khairi
Jurnal Rekayasa Kimia & Lingkungan Vol 17, No 1 (2022): Jurnal Rekayasa Kimia & Lingkungan (June, 2022)
Publisher : Chemical Engineering Department, Syiah Kuala University, Banda Aceh, Indonesia

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.23955/rkl.v17i1.22672

Abstract

The research aims to evaluate the pollution of Pb and Zn in water, sediment, and Faunus ater samples collected from Krueng Balee (KB) and Kreung Reuleung (KR) Rivers, Aceh, Indonesia. The samples were collected at the upstream, midstream, and downstream of each river and analyzed using Atomic Absorption Spectrophotometry (AAS). The distribution of Pb and Zn pollution was analyzed using Principal Component Analysis (PCA). Our investigation revealed that the presence of Pb and Zn is still safe for water and sediment samples. Nevertheless, Pb and Zn contamination found in F. ater samples had exceeded the national safety limit for food. PCA analysis revealed correlations between samples suggesting the roles of physical and chemical properties of the river in the pollutant retainment. The analysis also indicated the possible antagonism between Pb and Zn accumulation in F. ater which has never been reported previously. We suggest routine monitoring of Pb and Zn concentrations. The role of the surrounding industry in the Pb and Zn pollution should be further studied.
Adsorpsi Ion Logam Cu(II) Menggunakan Lignin dari Limbah Serbuk Kayu Gergaji Lelifajri, Lelifajri
Jurnal Rekayasa Kimia & Lingkungan Vol 7, No 3 (2010): Jurnal Rekayasa Kimia & Lingkungan
Publisher : Chemical Engineering Department, Syiah Kuala University, Banda Aceh, Indonesia

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Abstract

Adsorption of heavy metal ion Cu(II) onto modified lignin from sawdust waste have been presented. The ability of lignin from sawdust waste to adsorb the copper ion has been evaluated by varying adsorption time, pH of solution, and adsorption capacity. The concentration of copper ion was measured by atomic adsorption spectrometer. The result showed that the optimum condition of ion Cu(II) by lignin were achieved at adsorption time of 15 minutes, pH of solution of 6, and copper concentration of 20 mg/L with adsorption efficiency of 99,3 %. In this study, the maximum capacity of 15,43 mg/g and equilibrium constant of 754,96 were achieved.Keywords: adsorpsi, ion tembaga, lignin, limbah serbuk kayu gergaji
Analisis Logam Berat Pb dan Cd dalam Sampel Ikan dan Kerang secara Spektrofotometri Serapan Atom Supriatno, Supriatno; Lelifajri, Lelifajri
Jurnal Rekayasa Kimia & Lingkungan Vol 7, No 1 (2009): Jurnal Rekayasa Kimia & Lingkungan
Publisher : Chemical Engineering Department, Syiah Kuala University, Banda Aceh, Indonesia

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Abstract

The analysis of heavy metals Pb and Cd concentrations in fish and oyster have been carried out by atomic absorption spectrophotometer (AAS) method. The wet digestion method was used for preparation sample prior to AAS detection. Sample was collected from three different location rivers at Lamnyong, Pantee Pirak and Lumbago. The result showed that the Pb and Cd concentration in fish and oyster at difference location were obtained not difference significantly. Pb and Cd contents in fish and oyster were found below lethal concentration. The AAS instrument was still valid to use as the instrument which is obtained of accuration of 0.65% and precise of 0,019 ppm still lower than threshold value of 1% and 0.04 ppm.Keywords: atomic absorbance spektrophootometry, fish, kerang, heavy metal
Analysis of Lead (Pb) and Cadmium (Cd) in Oyster Crassostrea gigas and Saccostrea cucullata using Atomic Absorption and Ultraviolet-Visible Spectrophotometer Methods Lelifajri, Lelifajri; Salsabila, Salsabila; Suhud, Khairi
IJFAC (Indonesian Journal of Fundamental and Applied Chemistry) Vol 8, No 2 (2023): June 2023
Publisher : IJFAC (Indonesian Journal of Fundamental and Applied Chemistry)

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.24845/ijfac.v8.i2.55

Abstract

Lead (Pb) and Cadmium (Cd) metals are highly toxic when accumulated in the body and cause serious diseases and even death. This study aimed to determine the metal content of Pb and Cd in the oyster species Crassostrea gigas and Saccostrea cucullate in the Lampulo and Krueng Cut areas at three different places. Analysis of the metals was carried out using AAS and UV-Visible spectrophotometers. Samples were prepared using concentrated HNO3 wet destruction and the addition of dithizone. The results showed Pb measured by AAS in Saccostrea cucullata 2.33-8.00 ppb, and by UV-Vis 2.77-8.66 ppb. Pb within Crassostrea gigas by AAS method 1.77-10.30 ppb, and by UV-Vis method 2.11-10.66 ppb. The Cd metal measured by AAS in Saccostrea cucullate is 3.80-10.50 ppb, and by UV-Vis method is 4.29-10.77 ppb, whereas Cd in Crassostrea gigas measured by AAS is 12.11-13.22 ppb and by UV-Vis method is 12.77-13.66 ppb. Linearity of Pb measurements with AAS and UV-Vis was obtained R2 =0.9979 and R2 =0.9938 and for Cd were R2 =0.9986 and R2 =0.9810. Accuracy (%recorvery) of Pb measurements by AAS and UV-Vis are 80-110% and 98-113% whereas Cd showed 100-106% and 91-107% respectively. The relative value of the standard deviation (%RSD ± SD) is 0.001 indicating excellent measurement results. Based on t-test calculations, measurements of Pb and Cd levels showed no difference between the AAS method and the UV-Vis method
Co-Authors Eka Safitri Ilham Maulana N. Nazaruddin Rahmadi Rahmadi Rinaldi Idroes Salsabila, Salsabila Suhud, Khairi Supriatno