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Zainab Ramli
Ibnu Sina Institute for Fundamental Science Studies, Universiti Teknologi Malaysia
Astronomy Chemistry Earth & Planetary Sciences Mathematics Physics

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Influence of TiO2/TS-1 Calcination on Hydroxylation of Phenol Ratna Ediati; Maria Ulfa; Hamzah Fansuri; Zainab Ramli; Hadi Nur; Didik Prasetyoko
Journal of Mathematical and Fundamental Sciences Vol. 46 No. 1 (2014)
Publisher : Institute for Research and Community Services (LPPM) ITB

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.5614/j.math.fund.sci.2014.46.1.7

Abstract

Titanium oxide (TiO2) was impregnated on the surface of titanosilicate-1 (TiO2/TS-1) and used as catalyst for hydroxylation of phenol with hydrogen peroxide. Calcination was conducted at various temperatures (400, 500, 600 and 700°C)in order to observe the effect on the structure and physicochemical properties towards catalytic activity for producing hydroquinone. The structure and physicochemical properties of the TiO2/TS-1 catalyst were characterized by several techniques, such as X-ray diffraction (XRD), infrared spectroscopy, nitrogen adsorption, pyridine adsorption and hydrophilic measurement. The results show that by increasing the calcination temperature,the surface acidity of the catalyst was also increased.TheTiO2/TS-1 catalyst calcined at 500°Cproved to be optimal for hydroquinone production, in which the anatase-rutile phase may be present dispersed on the MFI framework.
Co-Authors Didik Prasetyoko Hadi Nur Hamzah Fansuri Maria Ulfa Ratna Ediati