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Journal : Jurnal IPTEK

Pemurnian Ethanol Secara Destilasi Dengan Penambahan Garam KCl Sato, Abas; Rahardianto, Adi; Santoso, Andy Bagoes
Jurnal IPTEK Vol 19, No 2 (2015): December
Publisher : LPPM Institut Teknologi Adhi Tama Surabaya (ITATS)

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.31284/j.iptek.2015.v19i2.3

Abstract

One of the methods of ethanol mixture separation is distilation with addition of potassium chloride salt as entrainer. The aim of this research is to determine the effect of salt additiont and the reflux ratio, to ethanol product concentration, and also determine the best operating condition of the highest ethanol concentration in the distillation product.  The material used in the research are ethanol, potassium chloride and water. Equipment used is a series of sieve tray type distillation tower in diameter of 2.5 inch. Variable used in this research are: potassium chloride salt addition (0; 5; 10) grams/liter of alcohol solution, the concentration of ethanol feed (10; 50; 90) weight percent and  reflux ratio (0,5; 1; 1.5 ), the fixed variable are  ethanol feed in 4th tray, the flow rate (1250 ml/min), destillation time (120 minutes), and the number of sieve tray (11 trays). The research were carried out by introducing ethanol in specific concentration into the feed storage and reboiler and also potassium chloride into the salt storage. The reboiler is heated until evaporation of ethanol occur and distillation were carried out. Ethanol as product of distillation are measured its volume and concentration. The result is that the highest ethanol concentration is 98% by concentration of  feed  (50-90)%, addition of potassium chloride salt of 10 g rams/ liter, and  reflux ratio of 1.5.
The Effectiveness of Alum Made of Uncoated Aluminium Foil Waste in Improving the Quality of Liquid Waste of the Tofu Industry Nyoman Sri Widari; Agung Rasmito; Abas Sato
Jurnal IPTEK Vol 25, No 2 (2021)
Publisher : LPPM Institut Teknologi Adhi Tama Surabaya (ITATS)

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.31284/j.iptek.2021.v25i2.2292

Abstract

Aluminium foil waste increases every year in line with technology development, especially in the food and beverage industry. It will cause significant environmental problems because the packaging cannot be destroyed in the soil. Therefore, it is necessary to reprocess a large amount of aluminium waste into an alternative product such as alum which can be applied directly to the treatment of liquid tofu waste. In this study, uncoated aluminium foil waste was used, which was taken at random landfill sites and then washed and cut into small pieces. Dissolution of aluminium using KOH solution then the solution obtained is reacted with H2SO4 solution and the reaction is carried out at a temperature of 70oC. The experimental results got a maximum yield of 63.69% with Al2O3  content of 15.18% using 3 M KOH concentration and 5 M H2SO4 concentration. The obtained alum was then applied to the tofu industrial liquid waste. With the use of 800 ppm alum, there was a 60% decrease in the colour content of the Pt-Co unit, a 95.8% decrease in NTU and a 63.33% decrease in TDS. The quality of the liquid waste obtained met the technical requirements of raw water that can be treated by SNI 6773: 2008.
Pemurnian Ethanol Secara Destilasi Dengan Penambahan Garam KCl Abas Sato; Adi Rahardianto; Andy Bagoes Santoso
Jurnal IPTEK Vol 19, No 2 (2015)
Publisher : LPPM Institut Teknologi Adhi Tama Surabaya (ITATS)

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.31284/j.iptek.2015.v19i2.3

Abstract

One of the methods of ethanol mixture separation is distilation with addition of potassium chloride salt as entrainer. The aim of this research is to determine the effect of salt additiont and the reflux ratio, to ethanol product concentration, and also determine the best operating condition of the highest ethanol concentration in the distillation product.  The material used in the research are ethanol, potassium chloride and water. Equipment used is a series of sieve tray type distillation tower in diameter of 2.5 inch. Variable used in this research are: potassium chloride salt addition (0; 5; 10) grams/liter of alcohol solution, the concentration of ethanol feed (10; 50; 90) weight percent and  reflux ratio (0,5; 1; 1.5 ), the fixed variable are  ethanol feed in 4th tray, the flow rate (1250 ml/min), destillation time (120 minutes), and the number of sieve tray (11 trays). The research were carried out by introducing ethanol in specific concentration into the feed storage and reboiler and also potassium chloride into the salt storage. The reboiler is heated until evaporation of ethanol occur and distillation were carried out. Ethanol as product of distillation are measured its volume and concentration. The result is that the highest ethanol concentration is 98% by concentration of  feed  (50-90)%, addition of potassium chloride salt of 10 g rams/ liter, and  reflux ratio of 1.5.
The Effectiveness of Alum Made of Uncoated Aluminium Foil Waste in Improving the Quality of Liquid Waste of the Tofu Industry Widari, Nyoman Sri; Rasmito, Agung; Sato, Abas
Jurnal IPTEK Vol 25, No 2 (2021): December
Publisher : LPPM Institut Teknologi Adhi Tama Surabaya (ITATS)

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.31284/j.iptek.2021.v25i2.2292

Abstract

Aluminium foil waste increases every year in line with technology development, especially in the food and beverage industry. It will cause significant environmental problems because the packaging cannot be destroyed in the soil. Therefore, it is necessary to reprocess a large amount of aluminium waste into an alternative product such as alum which can be applied directly to the treatment of liquid tofu waste. In this study, uncoated aluminium foil waste was used, which was taken at random landfill sites and then washed and cut into small pieces. Dissolution of aluminium using KOH solution then the solution obtained is reacted with H2SO4 solution and the reaction is carried out at a temperature of 70oC. The experimental results got a maximum yield of 63.69% with Al2O3  content of 15.18% using 3 M KOH concentration and 5 M H2SO4 concentration. The obtained alum was then applied to the tofu industrial liquid waste. With the use of 800 ppm alum, there was a 60% decrease in the colour content of the Pt-Co unit, a 95.8% decrease in NTU and a 63.33% decrease in TDS. The quality of the liquid waste obtained met the technical requirements of raw water that can be treated by SNI 6773: 2008.