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All Journal Science and Technology Indonesia Jurnal Penelitian Sains INDONESIAN JOURNAL OF APPLIED PHYSICS
Alfikro, Ihsan
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Astronomy Biochemistry, Genetics & Molecular Biology Chemical Engineering, Chemistry & Bioengineering Chemistry Energy Environmental Science Materials Science & Nanotechnology Mathematics Physics

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Synthesis of Ion Imprinted Polymers (IIPs) Adsorbent Materials Using Fe(III) Leaching Process with Variation of Hydrochloric Acid Solvent Concentration and Heat Treatment Royani, Idha; Maimunah; Edianta, Jaya; Alfikro, Ihsan; Fiber Monado; Jorena; Satya, Octavianus Cakra; Virgo, Frinsyah
Science and Technology Indonesia Vol. 9 No. 2 (2024): April
Publisher : Research Center of Inorganic Materials and Coordination Complexes, FMIPA Universitas Sriwijaya

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.26554/sti.2024.9.2.336-344

Abstract

Fe(III)-IIPs material was prepared using a cooling-heating method with different leaching variations. The synthesis process used several chemical components, including EGDMA, MAA, and BPO as the crosslinker, functional monomer, and initiator. This study focused on the template formation process of IIPs with leaching variations, using parameters such as molarity concentration, solution mixture, and temperature to influence the amount of template formed in the polymer body. The spectra of XRD showed a widening value of FWHM as higher molarity was applied during the leaching process, with the widest one at 0.163 rad for IIPs 3 M. Fe(III) peak is located at 680-610 cm−1 or 1386-1350 cm−1 within the unleached sample, according to FTIR spectra. It also can be traced at minimum intensity in leached samples. SEM data processing showed that higher concentrations were essential in releasing Fe(III) ions from the polymer body. Meanwhile, heat treatment did not strongly impact the template formation sites of IIPs. Synthesized Fe(III)-IIPs materials had adsorption capacity, optimum time, and efficiency of 9.35 mg.g−1, 40 minutes, and 93.48%, respectively. Based on the results, Fe(III)-IIPs materials had great potential as adsorbents for removing metal pollutants from water.
Synthesis and Characterization of Polyvinyl Alcohol (PVA) Nanofiber Membranes with Annonamuricata and Terminalia catappa Leaf Extract Fitria, Silfiyana; Almafie, Muhammad Rama; Alfikro, Ihsan; Monado, Fiber; Sriyanti, Ida; Royani, Idha
Science and Technology Indonesia Vol. 10 No. 3 (2025): July
Publisher : Research Center of Inorganic Materials and Coordination Complexes, FMIPA Universitas Sriwijaya

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.26554/sti.2025.10.3.837-846

Abstract

Polyvinyl alcohol (PVA) is hydrophilic, flexible, elastic, and environmentally friendly, leading to the wide use as a binder in nanofiber matrices. The nanofibers of PVA are frequently combined with extract possessing antibacterial properties for characterization. Therefore, this study aimed to produce PVA nanofibers incorporating soursop leaf extract (ALE) and catappa leaf extract (CLE) using electrospinning for the investigation of the physicochemical, mechanical, and antibacterial properties. Electron microscopy showed that the electrospun nanofibers had a yellowish-brown surface with diameters ranging from 962 nm to 1323 nm. Fourier Transform Infrared (FTIR) analysis revealed the presence of functional groups interacting through hydrogen bonding, leading to a shift in wavenumbers. The tensile strength of PAC-1, PAC-2, and PAC-3 nanofibers decreased from 8.46 MPa to 4.27 MPa, followed by a reduction in Young’s modulus from 20.2 MPa to 0.89 MPa. The effect of extract concentration on the reduction in tensile strength and Young’s modulus was related to aggregation in certain areas of the nanofibers and weakened intermolecular polymer interactions. Pure extract had strong antibacterial activity and nanofiber membranes had moderate activity with inhibition zones ranging from 12.3 to 16.8 mm and 8.0 to 14.4 mm, respectively. The results showed that the produced fibers could be used in the biomedical field for wound dressings and filtration, as well as in textiles.
Simple Linear Regression Analysis of Temperature Trends using R Language: Case Study of Palembang City 1991-2020 Alfikro, Ihsan; Harisdianto, Harisdianto; Adnan, Assaidah; Affandi, Azhar Kholiq; Setiabudidaya, Dedi
Jurnal Penelitian Sains Vol 26, No 2 (2024)
Publisher : Faculty of Mathtmatics and Natural Sciences

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.56064/jps.v26i2.984

Abstract

Global warming is the most world priority of environment issues, which is indicate continously increment of  global mean temperature of Earth. Various research shown detrimental impact of Earth environment, due to increment of Earth temperature. Our study provide temperature trend of small scope observation unit, the urban area of Palembang City at latitude 2,9° and longtitude 104,7° for 30 years, from 1991-2020. Linear regression analysis shown the temperature increase on skin temperature (TS) and temperature at 2 meter range (T2M) are 0,4°C and 0,46°C, respectively. These variable can become indicator of global warming occurance on small scope of observation unit.Keywords: Global warming, Temperature trend, Linear regression
Evaluation of Ferric Ion Adsorption On The Surface Imprinting Adsorbent Alfikro, Ihsan; Jorena, Jorena; Koriyanti, Erry; Satya, Octavianus Cakra; Monado, Fiber; Royani, Idha
INDONESIAN JOURNAL OF APPLIED PHYSICS Vol 14, No 2 (2024): October
Publisher : Department of Physics, Sebelas Maret University

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.13057/ijap.v14i2.89893

Abstract

Rapidity in technological aspects encourages industrial sector to utilize and apply the latest technology to accelerate and optimize production in its field. Thus, waste from industry polluting various aspects of environment, such as water, gives rise to environmental impacts. Heavy metals, including iron, are one of the most common and dangerous pollutants often found in water environments. Therefore, consideration of methods for heavy metal separation from water becomes important. The adsorption method has been used for separating heavy metals because of its simplicity, thus effectively cuts energy consumption and costs in process. However, heavy metal characteristics in water can vary depending on the element. Consequently, understanding the heavy metal characteristics in water is important, hence capable of formulate appropriate and effective adsorption systems. This study, Fe(III)-IIPs was applied to adsorb and separate iron from water through repeated adsorption with parameter improvements. The pH parameter plays an important role, with ion competition happens at pH <2 and the formation of iron hydroxide species at pH >4.5, which results in adsorption inhibition. The modeling of adsorption kinetic equation was found that the adsorption system carries chemisorption characteristics, with adsorption capacity of 11.15 mg/g and reaction rate constant of 19 min-1.
Co-Authors Affandi, Azhar Kholiq Almafie, Muhammad Rama Assaidah, Assaidah Dedi Setiabudidaya Edianta, Jaya Erry Koriyanti Fiber Monado Fitria, Silfiyana Frinsyah Virgo Harisdianto, Harisdianto Ida Sriyanti Idha Royani Jorena Jorena Jorena, Jorena Maimunah Octavianus Cakra Satya