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All Journal JURNAL KIMIA SAINS DAN APLIKASI Jurnal Pengabdian UntukMu NegeRI JURNAL PHOTON
Prasetya
Department Of Chemistry, Faculty Of Mathematics And Natural Sciences And Health, Universitas Muhammadiyah Riau, Pekanbaru|Universitas Muhammadiyah Riau|Indonesia
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Karakterisasi Hasil Sintesis Fotokatalis TiO2 Dengan Metode Sol-Gel dan Hidrothermal Untuk Aplikasi Limbah Petroleum Manja Nanda Resa Manja; Hasmalina Nasution; Zumrotun Nasihah; Tengku Finalia; Laila Rahmadanis; Prasetya Prasetya; Rahmadini Syafri; Sri Hilma Siregar
Sistem Informasi Vol 12 No 2 (2022): Jurnal Photon
Publisher : LPPM Universitas Muhammadiyah Riau

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.37859/jp.v12i2.3473

Abstract

Petroleum waste (crude oil) has become one of the sources of pollution in the sea. The pollution caused comes from several factors, oil spills from tankers, deliberate disposal of irresponsible industries. The layer of crude oil on the surface of the air holds back gas exchange from the atmosphere and reduces the solubility of oxygen in the waters so that it interferes with the respiration and photosynthesis processes in phytoplankton which are food producers in the sea. This study aims to characterize the synthesized TiO2 photocatalyst material using two methods, namely Sol-Gel (SG) and Hydrothermal (HD) which will then be used for applications in petroleum waste. To determine effectiveness of TiO2 photocatalyst in reducing crude oil spills on the sea surface based on fatty oil parameter tests. The synthesis of TiO2 was carried out by the solgel method (SG) and the hydrothermal method (HD) at various temperatures of 300 oC, 500 oC, and 700 oC. Characterization of the material formed using the SEM-EDX instrument, showed that in general it is spherical in shape, and is composed of C, O and Ti elements. The maximum effectiveness of SG-300, SG-500, and SG-700 was able to reduce fat oil content by 57.19%, 66.14% and 41.42% while HD-300, HD-500, and HD-700 were able to reduce fatty oil content. maximum of 60.87%. , 56.41% and 45.68% in the 120 minute irradiation time. The results showed that the photodegradation process in petroleum waste treatment using TiO2 material was able to reduce the fat oil content.
Titanium Dioxide (TiO2) Modified Bentonite for Photodegradation in Methylene Blue Dye Sri Hilma Siregar; Prasetya Prasetya; Norramizawati Norramizawati; Marlian Marlian; Aulia Rizki Ramadhanti
Jurnal Kimia Sains dan Aplikasi Vol 26, No 4 (2023): Volume 26 Issue 4 Year 2023
Publisher : Chemistry Department, Faculty of Sciences and Mathematics, Diponegoro University

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.14710/jksa.26.4.143-150

Abstract

Dye is one of the waste waters, which will be a problem if the content is excessive in the water. Modifying bentonite with titanium dioxide (TiO2) as a photocatalyst for removal of dye waste. In this study, composite synthesis was carried out by mixing bentonite and TiO2 suspensions. The mass of bentonite is 20 g, and the mass variations of TiO2 are 10%, 20%, 30%, 40%, 50%, 60%, 70%, 80%, 90%, and 100%. The resulting composite was heated using a furnace at 550°C for 5 hours. Bentonite-TiO2 composites were characterized using Fourier Transform Infrared, X-Ray Diffraction, and Scanning Electron Microscope-Energy Dispersive X-Ray (SEM-EDX). Photodegradation of methylene blue dye with bentonite-TiO2 was carried out by varying the mass of bentonite-TiO2 photocatalysts (0.02, 0.04, 0.06, 0.08 g); variations in pH (1, 3, 5, 7, and 9), and variations in UV irradiation time (30, 60, 90, and 120 minutes). The results of characterization with FTIR showed the presence of Ti-O-Ti vibrations at wavenumber 1419 cm-1 and Si-O-Ti at wave numbers 780 cm-1 and 799 cm-1. Characterization of 20% bentonite-TiO2 by XRD showed rutile, anatase, and montmorillonite phases. The SEM-EDX bentonite-TiO2 characterization results produced some small particles with a layered structure with TiO2 particles clumping and still in the form of agglomerates, and the EDX results showed the chemical composition of Si and Ti. The results of photodegradation showed that the best activity for the bentonite-TiO2 composite occurred in photocatalyst BT-20% with a mass of 0.08 g, pH 1, and UV irradiation time of 120 minutes with methylene blue 99.942% degraded.
Co-Authors Akbar, Unggul Aulia Rizki Ramadhanti Aulia Rizki Ramadhanti Fitra Perdana Hasmalina Nasution Hasmalina Nst Jasril Jasril Jufrizal Syahri Laila Rahmadanis Manja Nanda Resa Manja Marlian Marlian Nasution, Annio Indah Lestari Norramizawati Norramizawati Nurlailli Nasution Olif Syahbella Rahmadini Syafri Rahmiwati Hilma Rian Putra Siti Zahidah Sri Hilma Siregar Tengku Finalia Trisiwi Kusuma Ningrum Unggul Akbar Wahyuni Puspita Sanda Wirdati Irma Yeni Yernita Yuhelson Zumrotun Nasihah