Dian Noviyanti Agus Imam
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The Effect of Addition of Nano hydroxyapatite Powder of Anadara granosa Shells on Surface Roughness of Heat-cured Acrylic Resin Aris Aji Kurniawan; Dian Noviyanti Agus Imam; Helmi Hirawan
Denta Journal Kedokteran Gigi Vol 14 No 2 (2020): Agustus
Publisher : Fakultas Kedokteran Gigi Universitas Hang Tuah

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.30649/denta.v14i2.5

Abstract

Background: Heat-cured acrylic resin is one of the most widely used denture base materials. However, the residual monomer can reduce its mechanical properties, which affect physical properties such as surface roughness, resulting in high porosity—the results in the growth of fungal colonies. One way to improve these properties is to add a reinforcement material such as nano-hydroxyapatite (HAp) from the Anadara granosa shell. Nano-hydroxyapatite has a large surface area to act as a filler because of its strong bonding capacity and a smoother surface, and a higher density to improve mechanical properties. Purpose: This study aims to determine HAp powder's effect from the Anadara granosa shells on the surface roughness of heat-cured acrylic resin. Methods: This type of research used an experimental laboratory, research design posttest-only control group design. Twenty-four samples were used and divided into three groups: the acrylic resin group with 1%, 3% blood cockles shell HAp, and acrylic resin without HAp with simple random sampling. Results: The results showed that the lowest mean value of surface roughness was in a group with the addition of 3% HAp, at 1.696 ± 0.25058 µm. One-Way ANOVA test on roughness showed a significant difference between groups with p = 0.000 (p <0.05). Conclusion: This study concludes that there is an effect of HAp on the roughness of heat-cured acrylic resin.
Effect of Durian Rind Nanocellulose Addition on the Vickers Hardness of Self-Cure Acrylic Resin Fabricated By Spray-on Method Dian Noviyanti Agus Imam; Ryana Budi Purnama; Rinawati Satrio; Mutia Rochmawati
Medical and Health Journal Vol 5 No 2 (2026): February
Publisher : Fakultas Kedokteran Universitas Jenderal Soedirman

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.20884/1.mhj.2026.5.2.16998

Abstract

Self-cure acrylic resin is commonly used to fabricate orthodontic baseplates in removable appliances. However, it exhibits relatively low hardness, making it susceptible to wear and deformation under masticatory forces. The addition of reinforcing materials can enhance mechanical properties such as hardness. Nanocellulose derived from durian (Durio zibethinus Murr.) rind, an agricultural waste product, is a promising bio-based reinforcing material. This study aimed to determine the effect of durian rind nanocellulose addition on the Vickers hardness of self-cure acrylic resin fabricated using the spray-on method.This laboratory experimental study employed a posttest-only control group design. Durian rind nanocellulose was synthesized via acid hydrolysis and characterized using Transmission Electron Microscopy (TEM) and Fourier Transform Infrared Spectroscopy (FTIR) to confirm morphology and functional groups before incorporation into the acrylic resin. The nanocellulose was dispersed in monomer using ultrasonic homogenization for 5 minutes to ensure uniform distribution, then applied to polymer powder using the spray-on method. Twenty-four samples were divided into three groups (n=8): 2% nanocellulose, 3% nanocellulose, and control (0% nanocellulose). The highest mean hardness value was found in the 2% nanocellulose group (30.77 ± 1.03 VHN), while the lowest was in the control group (26.90 ± 0.79 VHN). Data were normally distributed and homogeneous (Shapiro-Wilk and Levene tests). One-way ANOVA revealed significant differences among groups (p<0.05), with post hoc LSD tests confirming significant pairwise differences. This study concludes that durian rind nanocellulose addition significantly increases the Vickers hardness of self-cure acrylic resin fabricated by the spray-on method compared to the control group