Natural zeolite from Manikin (ZAM), Kupang Regency, has been successfully characterized by XRF, FTIR-ATR, powder-XRD and SEM. XRF results show that the three most abudant elements in ZAM are Si (68.1%); Fe (11.9%) and K (9.76%). Meanwhile, there is absorption at wave number 100.45 cm-1 which indicates the presence of asymmetric O-Si-O and O-Al-O. Based on the XRD diffraction pattern of the powder analyzed by the rietvield method, it shows that ZAM consists of SiO2 and mordenite-type zeolite minerals complexed with Na and Ca metals. As for morphology of ZAM, it consists of various shapes and one of them is sharp like a needle.
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