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Jurnal Kimia Terapan Indonesia

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Published by Lembaga Ilmu Pengetahuan Indonesia

ISSN : 08532788 EISSN : 25277669 DOI : -

Biochemistry, Genetics & Molecular Biology Chemical Engineering, Chemistry & Bioengineering Chemistry Materials Science & Nanotechnology

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Articles 8 Documents

Search results for , issue "Vol 15, No 2 (2013)" : 8 Documents clear

PENENTUAN KONDISI OPTIMUM FERMENTASI PADAT Trichoderma hamatum PADA MEDIA TUMBUH DEDAK PADI DALAM PRODUKSI SELULASE MENGGUNAKAN RESPONSE SURFACE METHODOLOGY Teuku Beuna Bardant; Haznan Abimanyu; Putri Lili Epriyani
Jurnal Kimia Terapan Indonesia Vol 15, No 2 (2013)
Publisher : Research Center for Chemistry - LIPI

Optimum condition for solidfermentation of Trichoderma hamatum inrice bran in order to produce cellulase hadbeen studied by using Response Surfacemethodology (RSM). Fermentationcondition variables that observed waswater to rice bran ratio, urea andinoculums additions cellulase activity inFPU/gds (gram of dry solid) became theonly dependent variable. The result ofempirical equation from this study wasproven to be valid within water to ricebran ratio 0,5 - 0,7, urea and inoculumsaddition where 2-3 % and 1-2% of ricebran weight respactively. Maximumcellulase activity that can be obtain withinthese ranges was 4.99 Â± 0.92 FPU/gds.Keywords: Cellulase, Trichodermahamatum, rice bran, solid fermentation

KARAKTERISTIK BIO-OIL HASIL PIROLISIS AMPAS TEBU Emi Erawati; Wahyudi Budi Sediawan; Panut Mulyono
Jurnal Kimia Terapan Indonesia Vol 15, No 2 (2013)
Publisher : Research Center for Chemistry - LIPI

Bagasse (Saccarum oficinarum L) is a waste of sugar mills that can be utilized for a variety of chemicals. The purposes of this study are to determine the percentage of compounds and physical properties of bio-oil, to determine the effect of variations of particle size and heating rate on the yields of bio-oil. Pyrolysis has been carried out in a reactor made of steel pipe type 5737 with dimension: diameter 7.62 em and a length of 3 7 cm.. The reactor was inserted into the furnace with a diameter of 15.24 em and a length of 40 em. One hundred and fifty grams of bagasse (Saccarum oficinarum L) has been inserted into the reactor without the presence of oxygen at atmospheric pressure. Pyrolysis has been carried out at the particle size of (-20+25) mesh, (-25+30) mesh, (-30+35) mesh, (- 35+40) mesh, and -40 mesh with electrical voltage of 100, 105, 115, and 120 volt. Produced of bio-oil has the following properties: brown color, pH of 2.96 to 3.03, viscosity of 1.3306 to 1.5101 cp, and density of 1.03 to 1.5 g/mL. The largest content of the compound is acetic acid (59, 72%). The highest yields percentage of the particle size is (40,32%) on (-20+25 mesh) with the highest yields percentage of electrical voltage is 38,82% on 105 volt.Keywords : Bagasse, acetic acid, bio-oil, pyrolysis, yields

POTENSI TEMPE PASTA STERIL IRADIASI SEBAGAI NUTRISI ENTERAL PASIEN YANG MENGGUNAKAN ALAT BANTU NASO GASTRIC TUBE (NGT) Zubaidah Irawati; R. S. Adji Koesoemowidodo; Ades Puspita; Swasono R Tamat
Jurnal Kimia Terapan Indonesia Vol 15, No 2 (2013)
Publisher : Research Center for Chemistry - LIPI

Food irradiation process has a potential topromote of a safe, adequate and nutritiousfood supply for hospital diets. It has twoapplications that can contribute to thehealth and well being of humanity, i.e. theelimination of foodborne pathogensmicroorganisms, and the preservation offoods by the destruction of pests. Effects ofionizing radiation on tempe pasta selectedas samples for patient food intake throughNaso Gastric Tube (NGT) has beenstudied. Tempe pasta was vacuum packedin a laminate pouch of po lyesteraluminumfoil- linear low densitypolyethylene and gamma irradiated atdoses of 10 kGy and 25 kGy , respectivelyunder cryogenic condition and then storedat room temperature for 6 and 12weeks. Some quality parameters wereobserved. There was no significantdifferences between un irradiated andirradiated tempe pasta on the moisturecontent, pH, protein content and viscosity.Meanwhile isojlavon genestein contentand antioxidant capacity showed anincrease by increasing irradiation dose upto 12 weeks of storage. Malonaldehydecontent in tempe pasta was accelerating byincreasing the irradiation dose andextending the storage period but Peroxidevalue was not detected in all treatedsamples. The irradiated tempe pasta atcertain degree of viscosity and particlesize could be considered as protein basefood intake for immunocompromisedpatients through Naso Gastric Tube(NGT).Keywords: Tempe pasta, food irradiation,isojlavon genestine, nutritious food,immunocompromised patients.

PENGARUH TEKANAN REAKTOR PADA PENGHIDRORENGKAHAN TAR BATUBARA Novie Ardhyarini; Daliya Indra Setiawan; Syntha Nardey
Jurnal Kimia Terapan Indonesia Vol 15, No 2 (2013)
Publisher : Research Center for Chemistry - LIPI

Coal gasificationproduce tar as aside-product. Coal tar is a complexmixture, and consists of various functionalgroups mainly polyaromatic compounds.Due to its chemical composition, coal taris categorized as hazardous material. Thephysical and chemical properties of coaltar is similar to crude oil, but it has higherpolyaromatics and impurities. Thoseproblems are the main challenges ofprocessing coal tar into fuel. Therefore, anupgrading process is required This paperdiscussed upgrading coal tar into fuel byhydrocracking in an autoclave reactorusing catalyst of nickel-molybdenum withalumina-silica support. Effect of reactorpressure was observed Hydrocrackingproduct at 450Â°C and 120bar showed thebest result where the HIC molar ratioincreased 26% and the specijic gravitydecreased 19%. The impurities of sulphurand nitrogen decreased 88,5% and 72%respectively. Hydrocracking productwasdistilled using a simulated distillation bygas chromatography. Based on simulateddistillation analysis, the product could befractionated into 2,2%vol of light end,33.8%vol of naphtha, and 48%vol ofmiddle distillate. These results showed thatcoal tar is potential to be processed intofuel. Furthermore, the utilization of coaltar can be a solution of waste treatment aswell.Keywords :Coal tar, waste, hydro cracking,autoclave reactor, fuel

PREPARASI PEREAKSI KIT IMMUNORADIOMETRlCASSAY FREE PROSTATE SPECIFIC ANTIGEN UNTUK DETEKSI KANKER PROSTAT Puji Widayati; Gina Mondrida; Sri Setiyowati; Agus Ariyanto; V. Yulianti Susilo; Wening Lestari
Jurnal Kimia Terapan Indonesia Vol 15, No 2 (2013)
Publisher : Research Center for Chemistry - LIPI

Prostate Specific Antigen (PSA) is a glycoprotein with a molecular weight of approximately 34,000 daltons serine protease secreted exclusively by prostatic epithelial cells that lining acini and prostate gland. Increased of PSA levels can be caused by prostate cancer or benign prostate enlargement (benign prostatic hyperplasia, BPH). PSA in the blood was found in the free condition (free PSA) and most of the bound protein (complexed-PSA, c-PSA). Measuring levels of PSA was found in the blood can be done by several methods such as by immunoradiometricassay (IRMA) methods or ELISA methods. IRMA method is one of immunoassay techniques using radionuclides ,/' 125 oJ I as a tracer, so the sample in small 13 quantity can be detected The purpose of this study was obtained PSA reagent kit that includes 1251labeled PSA as a tracer, PSA coated tube and PSA standard that requirements of the kit, then it can be optimized assay design, that eventually PSA reagent kit can be used for early detection of prostate cancer. It has been done labeling of Mab PSA using 125 1with reaction time was 90 seconds, amount of PSA MAb was 75 ugram and the activity of Na_ 125I was 1000 flCi. Preaparation of PSA coated tube using 0.05 M Na2C03 solution, at pH: 9.6 with volume was 250 ml., standard PSA with 0.025 Mphosphate buffer at pH 7.4 containing 5% BSA and 0.1% NaN3, and resulting at 1,25% and 14,12% respectively of NSB and BIT that requirement of the kit.Keywords: Prostate cancer, PSA, IRMA,NSB, Maximum Binding

HIDROLISIS LIGNOSELULOSA PELEPAH DAN TANDAN KOSONG KELAPA SAWIT DENGAN KATALIS ZIRKONIA TERSULFATASI Anis Kristiani; Kiky Corneliasari Sembiring; Haznan Abimanyu; Fauzan Aulia
Jurnal Kimia Terapan Indonesia Vol 15, No 2 (2013)
Publisher : Research Center for Chemistry - LIPI

Lignocellulosic biomass which are frond and empty fruit bunches (EFB) is second generation raw material for ethanol production. Lignocellulose usage is expected to create a green process. Utilization of lignocellulose materials into ethanol involved four main processes, i.e pretreatment, hydrolysis/sacharification, fermentation, distillation and dehydration ethanol that was product. This research aims to optimize hydrolysis process of EFB and frond by using sulfated zirconia catalyst characterized its physical and chemical properties as a solid acid catalyst. Catalytic hydrolysis process conducted at 160 DCfor 3 hours gave the highest TRS (Total Reducing Sugar) which is 17,51 % for EFB while for frondfor 2 hours which is 19,23 % .Keyword: Hydrolysis, solid acid catalyst, lignocellulose, frond, EFB, sulfated zirconia

SINTESIS XANTON DARI ASAM 2-PHENOXYBENZOIC ACID SEBAGAI BAHAN DASAR OBAT MALARIA BARU Amanatie Amanatie; Jumina Jumina; Mustofa Mustofa; M. Hanafi
Jurnal Kimia Terapan Indonesia Vol 15, No 2 (2013)
Publisher : Research Center for Chemistry - LIPI

Synthesis of xanthone was conducted from the raw material of 2-phenoxybenzoic acid through acid-catalyzed-cyclization. The product was characterized using UV- Vis, 1 13 d FT-IR, H-NMR, C-NMR, an LC-MS Cyclization of 2-phenoxybenzoic acid using sulfuric acid catalyt gave xanthone in 86.11 % yield. These compounds as the basis of new malaria drugs.Keywords 2-phenoxybenzoic acid, Synthesis, Xanthone, Characterized.

SINTESIS DAN KARAKTERISASI SELULOSA BAKTERI-SITRATKITOSAN SEBAGAI PEMBALUT LUKA ANTIMIKROBA Farah Nurlidar; Lely Hardiningsih; Darmawan Darwis
Jurnal Kimia Terapan Indonesia Vol 15, No 2 (2013)
Publisher : Research Center for Chemistry - LIPI

Bacterial cellulose, produced by Acetobacter xylinum, is an interesting material for using as a wound dressing since it provides moist environment to a wound resulting in a better wound healing. However, bacterial cellulose (BC) itself has no antibacterial activity to prevent wound infection. To achieve antibacterial activity, chitosan were impregnated into bacterial cellulose by cross linking reaction using citric acid as cross linker. The thickness, water and saline absorption capacity, water vapour transmission rate (WVTR), mechanical properties and antibacterial activity of composite were investigated. The result show an important increase in absorption capacity when BC was treated with citric acid and chitosan and the maximum value was reached at 21.5 gig in DM water and 8.2 gig in salinesolution}. The WVTR analysis of all the test membranes was found to be less than WVTR value of control without sample. The result also showed that bacterial cellulose-citrate-chitosan (BC-AST) exhibited antibacterial activity against E. coli, S. typhi, P. aeruginosa and S. aureusKeywords: Antibacterial, bacterial cellulose, citric acid, chitosan, wounddressing.

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