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All Journal ALCHEMY Jurnal Penelitian Kimia Agroindustrial Technology Journal Chemistry Indonesian Journal of Chemical Research Jurnal Sylva Lestari
Manggar Arum Aristri
Department Of Forest Management, Faculty Of Agriculture, Universitas Sebelas Maret
Agriculture, Biological Sciences & Forestry Biochemistry, Genetics & Molecular Biology Chemical Engineering, Chemistry & Bioengineering Chemistry Earth & Planetary Sciences Energy Engineering Environmental Science Industrial & Manufacturing Engineering Materials Science & Nanotechnology

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Kolagen dari Limbah Tulang Ayam (Gallus gallus domesticus) terhadap Aktivitas Anti Aging secara In Vitro Eka Budiarti; Perlambang Budiarti; Manggar Arum Aristri; Irmanida Batubara
ALCHEMY Jurnal Penelitian Kimia Vol 15, No 1 (2019): March
Publisher : UNIVERSITAS SEBELAS MARET (UNS)

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.20961/alchemy.15.1.23046.44-56

Abstract

Limbah tulang ayam meningkat seiring dengan peningkatan konsumsi ayam. Namun, belum banyak penelitian yang memanfaatkan limbah tulang sebagai sumber kolagen. Penelitian ini bertujuan mengetahui pengaruh ukuran kolagen terhadap aktivitas anti aging berupa aktivitas antioksidan, antiglikasi, dan inhibitor tirosinase  secara in vitro dan mendapatkan teknik isolasi kolagen anti aging optimum dari tulang ayam. Isolasi kolagen dilakukan dengan variasi  konsentrasi NaOH, yaitu 0,05 M; 0,10 M; dan 0,20 M, dilanjutkan dengan perendaman menggunakan asam asetat 1 M. Kolagen yang diisolasi dengan NaOH 0,10 M merupakan kolagen dengan ukuran partikel, rendemen, dan antiglikasi terbesar (berturut-turut 2,34 µm, 12,59%, 61,06%) dan memiliki spektrum inframerah yang paling sesuai dengan kolagen standar. Kolagen ini kemudian diaduk dengan kecepatan 1000 rpm selama 6 dan 8 jam untuk pengecilan ukuran. Kolagen dengan pengadukan 6 jam mempunyai ukuran partikel lebih kecil (1,34 µm) dibandingkan dengan pengadukan 8 jam (1,80 µm). Kolagen dengan ukuran 1,34 µm menunjukkan aktivitas terbaik yaitu aktivitas antioksidan terhadap 2,2-difenil-1-pikrilhidrazil (DPPH) sebesar 24,70% dan inhibitor tirosinase sebesar 26,77%. Berdasarkan aktivitas antioksidan, antiglikasi, dan antitirosinase, kolagen dengan perendaman NaOH 0,10 M dan pengadukan selama 6 jam memiliki sifat anti aging yang paling baik.In Vitro Anti-Aging Activity of Chicken (Gallus gallus domesticus) Bone Waste Collagen. Chicken bone waste increases with increasing chicken compsumtion. However, study on utilizing chicken bone for collagen source has not been widely explored. This study aims to determine the effect of collagen size on their anti aging activity, and to obtain the optimum condition to produce the chicken (Gallus gallus domesticus) collagen in the high yield and the best activity. Collagen isolation was carried out in various NaOH concentrations of 0.05 M, 0.10 M, and 0.20 M, followed by the maceration on acetic acid 1 M. The isolation in NaOH 0.10 M produced the collagen with particle size of 2.34 µm in yield of 12.59% and anti-glycation of 61.06%. The revealed infrared spectrum of the isolated collagen is almost the same with the spectrum of the standart collagen. The collagen in 2.34 µm was further stirred at a 1000 rpm for 6 and 8 hours to reduce the size. Collagen stirred in 6 hours has a smaller particle size (1.34 µm) compared with that of stirred in 8 hours which has a particle size of 1.80 µm. The collagen with size of 1.34 µm showed the best activity, which revealed the antioxidant activity of 2,2-diphenyl-1-picrylhydrazyl (DPPH) of 24.70% and tyrosinase inhibitors of 26.77%. Based on antioxidant activity, anti-glycation, and anti-tyrosinase, the collagen which was isolated in 0.10 M NaOH and was stirred in 6 hours has the best anti-aging property.
Development of Differential Pulse Anodic Stripping Voltammetry Technique for Cadmium(II) Detection and Its Application in Water Spinach Putra, Budi Riza; Aristri, Manggar Arum; Rohaeti, Eti; Wahyuni, Wulan Tri
Indonesian Journal of Chemical Research Vol 9 No 2 (2021): Edition for September 2021
Publisher : Jurusan Kimia, Fakultas Sains dan Teknologi, Universitas Pattimura

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.30598/ijcr.2021.9-riz

Abstract

Cadmium is a toxic pollutant that is harmful to the environment and humans. The purpose of this research was to develop a method for cadmium(II) detection using differential pulse anodic stripping voltammetry (DPASV) using a glassy carbon electrode. The developed method was then applied for cadmium detection in the vegetable samples which is water spinach. The developed method was optimized in several parameters such as potential window, deposition potential, deposition time, and scan rate. The developed method for cadmium(II) detection was also investigated in its analytical performance includes linearity, precision, detection limit, and quantitation limit. The optimum conditions for cadmium(II) detection in 0.1 M KCl using DPASV technique obtained such as potential window from -1200 to -100 mV, deposition potential of -1100 mV (vs Ag/AgCl), and deposition time of 360 s. It was obtained good linearity for cadmium(II) detection using the DPASV technique with an R2 of 0.996. The precision was expressed as %SBR with 0.66%. The detection and quantitation limits for cadmium(II) detection were 0.4206 µM~0.0771 ppm and 0.5525 µM~0.1013 ppm, respectively. The developed method was then applied for cadmium(II) measurement in the water spinach sample and the obtained cadmium(II) concentration in water spinach was 0.2399 mg/Kg.
Ramie Fibers from Agroforestry System as Sustainable Materials for Functional Textiles: A Review Aristri, Manggar Arum; Hidayat, Wahyu; Iswanto, Apri Heri; Lubis, Muhammad Adly Rahandi
Jurnal Sylva Lestari Vol. 12 No. 3 (2024): September
Publisher : Department of Forestry, Faculty of Agriculture, University of Lampung

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.23960/jsl.v12i3.986

Abstract

Agroforestry system is a form of integrated land use involving forestry and agriculture, which is expected to help overcome the problems of increasing demand for agricultural land, decreasing environmental quality and poverty rates, and resulting in increasingly complex global issues. This system includes a combination of forestry crops with agricultural crops or other plants that can grow together on the same land. The application of agroforestry can improve agricultural welfare, overcome the environmental crisis and poverty, and maintain the sustainability of natural resource conservation. Ramie (Boehmeria nivea) fiber is an interesting plant to cultivate using an agroforestry system. It is easy to cultivate, positively impacts the environment, and has many application benefits because it is known as a strong and long-lasting fiber. On the other hand, the textile industry in Indonesia still predominantly uses cotton fiber which has low productivity, so the value of cotton imports increases yearly. Given the increasing demand for environmentally friendly and sustainable textiles, researchers and industry stakeholders are looking for other materials that provide functionality and environmental advantages. Ramie fiber is a type of natural fiber with advantages compared to other natural fibers, such as tensile strength, mechanics, and cellulose content, which has similar characteristics to cotton so that ramie can be applied as a functional textile material to replace cotton. This review paper aims to provide an in-depth overview of all ramie fiber properties, methods, and applications for functional textiles. This article highlights the environmental benefits of ramie fiber and its potential to encourage a more sustainable textile industry, citing various sources. Keywords: agroforestry, forestry crops, functional textile, ramie fiber, ramie’s properties
Isolation and Characterization of Cellulose from Biomass: A Methodological Review: Isolation and Characterization of Cellulose from Biomass: A Methodological Review Hanifah, Aisyah; Sumirat, Riska; Soerya, Sarah Fitri; Aristri, Manggar Arum
Agroindustrial Technology Journal Vol. 9 No. 1 (2025): Agroindustrial Technology Journal [ATJ]
Publisher : Universitas Darussalam Gontor

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.21111/atj.v9i1.14568

Abstract

The isolation and characterization of cellulose from biomass have garnered increasing research interest due to cellulose’s pivotal role in supporting sustainable material innovations across various industries. This study presents a comprehensive review of recent advancements in cellulose isolation methods, including chemical, mechanical, and enzymatic techniques, emphasizing their efficiencies in yield and purity. A bibliometric analysis using VOSviewer was also conducted to map research trends, identify leading authors and institutions, and visualize keyword co-occurrence networks from publications between 2015 and early 2025. The bibliometric results revealed three major thematic clusters in cellulose research: extraction and pretreatment technologies, material characterization techniques, and structural property analysis. Publication trends indicated dynamic research developments, particularly a surge in interest following advances in green extraction technologies. Overall, this review highlights the shift towards sustainable cellulose isolation strategies, evaluating the advantages and disadvantages of various methodologies. It provides insights into the strengths and limitations of current techniques, while also outlining potential future directions for research and industrial applications. Keywords: Biomass, Bibliometric Analysis, Cellulose, Characterization, Isolation.
Effectiveness of Different Extraction Techniques on the Yield and Antityrosinase Activity of Merbau (Intsia bijuga (Colebr.) Kuntze) Wood Extract Sari, Ratih Afrida Lismana; Sari, Rita Kartika; Safitri, Utami Dyah; Aristri, Manggar Arum; Wahyuningrum, Maeda; Lubis, Muhammad Adly Rahandi
Jurnal Sylva Lestari Vol. 13 No. 3 (2025): September
Publisher : Department of Forestry, Faculty of Agriculture, University of Lampung

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.23960/jsl.v13i3.1140

Abstract

This study employed various extraction techniques to determine the yield, phytochemical profile, and antityrosinase activity of merbau wood (Intsia bijuga (Colebr.) Kuntze) extracts. The extraction techniques consisted of two factors: the type of extraction methods (conventional maceration – CM, ultrasound-assisted extraction – UAE, and magnetic stirrer – MS) and the number of extraction repetitions (first repetition – F1, second repetition – F2, and third repetition – F3). The interaction of the extraction methods and the number of extractions affects the extraction yield, antityrosinase activity, and its phytochemical profile. Merbau wood extracted using the UAE-F1 extraction method resulted in the highest yield (13.38%). In contrast, the UAE-F3 extract showed the strongest antityrosinase activity (IC50 value of 1.548 ppm) and the highest total phenol content (692.86 mg/g AGE). Fourier transform infrared analysis of the F1 extract showed that all samples contained the same functional groups, namely C=C (1600–1475 cm-1) and O-H (3800–3000 cm-1), indicating structural similarity among the extracts. Merbau wood extraction using the UAE method, both in the first, second, and third extractions, produced the highest yield, antityrosinase activity, and total phenol content of the extract compared to the CM and MS extraction methods. Keywords: antityrosinase activity, Intsia bijuga, maceration, total phenolic content, ultrasound-assisted extraction
Bio-Polyurethane Resins Derived from Liquid Fractions of Lignin for the Modification of Ramie Fibers Aristri, Manggar Arum; Lubis, Muhammad Adly Rahandi; Laksana, Raden Permana Budi; Falah, Faizatul; Fatriasari, Widya; Ismayati, Maya; Wulandari, Asri Peni; Nurindah
Jurnal Sylva Lestari Vol. 9 No. 2 (2021): May
Publisher : Department of Forestry, Faculty of Agriculture, University of Lampung

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.23960/jsl29223-238

Abstract

Lignin is a biopolymer from agro-forestry biomass which provides greater prospects for higher added value applications in renewable and sustainable products. In this study, technical lignin from black liquor was used as a pre-polymer for the preparation of bio-polyurethane (Bio-PU) resins. Briefly, the isolated lignin was fractionated using ethyl acetate (EtAc) and methanol (MeOH). The liquid fractions of lignin, such as lignin-EtAc (L-EtAc) and lignin-methanol (L-MeOH), were mixed with 10% of polymeric isocyanate (based on the weigth of liquid fractions) to obtain Bio-PU resins. The isolated lignin, fractionated lignin, and lignin-derived Bio-PU resins were characterized using several techniques. The obtained Bio-PU resins then were used to modify ramie fibers using vacuum impregnation method. Fourier Transform Infrared (FTIR) spectroscopy, Differential Scanning Calorimetry (DSC), and Thermogravimetric Analysis (TGA) revealed that the isolated lignin had quite similar characteristics to lignin standar. Fractionation of lignin with EtAc and MeOH altered its characteristics. FTIR, DSC, and TGA showed that solid fractions of lignin had similar characteristics to lignin standard and isolated lignin, while the liquid fractions had characteristics from lignin and the solvents. The absorption band of isocyanate (-N=C=O) groups was shifted to 2285 cm-1 from 2240 cm-1 owing to the reaction with the -OH groups in lignin, forming urethane (R-NH-C=O-R) groups at 1605 cm-1 in Bio-PU resins. Thermal properties of Bio-PU resins derived from L-EtAc exhibited greater endothermic reaction compared to Bio-PU-L-MeOH. As a result, the free -N=C=O groups in Bio-PU resins have reacted with -OH groups on the surface of ramie fibers and improved its thermal properties. Modification of ramie fibers with Bio-PU resins improved the fibers' thermal stability by 15% using Bio-PU-LEtAc for 60 min of impregnation. Keywords: bio-polyurethane resins, impregnation, lignin fractions, ramie fibers, thermal stability
Co-Authors Apri Heri Iswanto Asri Peni Wulandari Asri Peni Wulandari, Asri Peni Budi Riza Putra Dyah Safitri Eka Budiarti Eti Rohaeti Faizatul FALAH Faizatul Falah Hanifah, Aisyah Irmanida Batubara Ismayati, Maya Laksana, Raden Permana Budi Lubis, Muhammad Adly Rahandi Maya Ismayati Muhammad Adly Rahandi Lubis Muhammad Rasyidur Ridho Nurindah Nurindah Nurindah Perlambang Budiarti Raden Permana Budi Laksana Rita Kartika Sari Sarah Fitri Soerya Sari, Ratih Afrida Lismana Sumirat, Riska Wahyu Hidayat Wahyuningrum, Maeda Widya FATRIASARI Widya Fatriasari Wulan Tri Wahyuni