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Optimization of Rice Bran Oil Bleaching via Carotenoid Adsorption onto Activated Carbon using Response Surface Methodology (RSM) Damayanti, Astrilia -; Harianingsih, Harianingsih; Bahlawan, zuhriyan Ash Shiddieqy; Dillah, Shohib Qomad; Dewi, Yasinda Verrel Dinara Shinka; Kristi, Silvia Yolanda; Prasetyo, Ridwan Anung
Reaktor Volume 23 No.2 August 2023
Publisher : Department of Chemical Engineering, Faculty of Engineering, Universitas Diponegoro

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.14710/reaktor.23.2.53-61

Abstract

Rice bran oil (RBO) is a by-product of rice processing with a good fatty acid profile and high oxidative stability. This study aims to optimize the bleaching stage of the rice bran oil refining process to determine the minimum levels of carotenoids in RBO by using the Response Surface Methodology (RSM). This research used the Central Composite Design (CCD) experimental design with three variables: bleaching temperature (50, 80, 1100C), bleaching time (20, 40, 60 minutes), and activated carbon concentration (0.4, 0.8, 1.2%). As a result, the model was enhanced to explain the correlation of each variable and the different data variations. This study employed the Derringer method to determine the most optimal variable variation that produces the lowest carotene levels. This study found that the optimal carotene level was 4.87 mg/kg with an activated carbon concentration of 1.18%, temperature of 500C, and time of 53.155 minutes.
Optimization of Acid Degumming of Crude Rice Bran Oil (CRBO) on Phospholipid Removal Using Response Surface Methodology (RSM) Damayanti, Astrilia; megawati, megawati; Winaningsih, Ima; Wicakso, Doni Rahmat; Nuryoto, Nuryoto; Rumbino, Yusuf; Prasetyo, Ridwan Anung; Rizki, Muhammad Prabu
Jurnal Rekayasa Kimia & Lingkungan Vol 20, No 1 (2025): Jurnal Rekayasa Kimia & Lingkungan (June, 2025)
Publisher : Chemical Engineering Department, Syiah Kuala University, Banda Aceh, Indonesia

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.23955/rkl.v20i1.43691

Abstract

Rice bran, a byproduct of milling rice, has 60% nutritional content and potential for processing into higher-selling goods like rice bran oil (RBO). Degumming is the first stage of refining crude oil. This research aims to remove phospholipids in crude rice bran oil (CRBO) by optimizing acid degumming. Three variables were optimized in this study using Design Expert v13's response surface methodology (RSM) employing central composite design (CCD) experimental design: the amount of phosphoric acid (0.1, 0.15, and 0.2 %w/w), the degumming temperature (50, 70, and 90 C), and the degumming time (20, 30, 40 minutes). The experimental values and predicted results did not correlate well with percentages (%) of error, with more than 50% occurring in 4 of 19 runs. The model's p-value of 0.4939 ( 0.05) is non-significant, with the coefficient determination, R2 being 0.5026. Optimization with desirability value ( 0.5) results showed a phospholipid removal response of 40.479% under conditions of adding 0.1%w/w phosphoric acid, temperature of 83.21 C, and degumming time of 40 minutes, which were determined by Derringers methodology..