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Ekstraksi Minyak Atsiri pada Daun Jeruk Manis (Citrus Aurantium) dengan Menggunakan Metode Microwave Hydrodistilation (MHD) Putri Agustin, Mawardhi Nabilla; Andreyan Poerwo Negoro; Ditta Kharisma Yolanda Putri; Meta Fitri Rizkiana; Istiqomah Rahmawati
Journal of Biobased Chemicals Vol. 3 No. 2 (2023): Journal of Biobased Chemicals
Publisher : Program Studi Teknik Kimia Universitas Jember

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.19184/jobc.v3i2.435

Abstract

This study aims to utilize sweet lime leaves which are only waste that has no value, where sweet lime leaves are one of the ingredients that contain essential oils. Apart from the skin, it turns out that this sweet lime leaf can also be extracted using the Microwave Hydrodistillation (MHD) method. This study uses three variables namely; the F/S ratio used was 0.375 g/mL; 0.5g/mL; 0.65 g/mL, power 150 watts, 300 watts, and 450 watts, and time 30, 60, and 90 minutes. The extraction method is carried out using fresh ingredients with a solvent volume of 200 ml. The test carried out is the GC-MS test. The results of the test method and the purpose of this study were to determine the limonene content in the extraction of sweet lime leaves using the MHD method with variations in ratio, power, and time. The optimum yield of essential oils is at a power of 300 W, 90 minutes, and a ratio of 0.625 with a yield of 0.373%. The biggest components produced in the MHD method of extracting citrus leaves were Germacrene D 29.51%, Alpha-Copaene 18.47%, CIS-CAROPHYLNE 15.42%, 9-Eicosene (E) 8.58% and Limonene 5.51%.
Extraction of Turmeric Leaves (Curcuma longa L.) as a Natural Preservative for Tuna Fish Using Ultrasound-Assisted Extraction (UAE) Method Salma, Isni Salma Salsabillah; Rossi Agnessi Pebriana; Bekti Palupi; Ditta Kharisma Yolanda Putri; Istiqomah Rahmawati
Journal of Biobased Chemicals Vol. 4 No. 1 (2024): Journal of Biobased Chemicals
Publisher : Program Studi Teknik Kimia Universitas Jember

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.19184/jobc.v4i1.822

Abstract

Turmeric leaves (Curcuma longa L.) contain phytochemical compounds that can be utilized as natural food preservatives or bioformalin due to its antibacterial properties. The extraction method used in this study is Ultrasound-Assisted Extraction (UAE), with the aim to determine the effect of variable sample-solvent ratio, time, and particle size on total flavonoid, tannin, and alkaloid compounds, as well as to determine the optimal shelf life of fresh tuna. This study used sample-solvent ratio variables of 1:10, 1:15, and 1:20; time variables of 10, 20, and 30 minutes; and particle size variables of 60, 80, and 100 mesh. The highest total flavonoid compound was obtained in the variable sample-solvent ratio of 1:20, particle size of 100 mesh, and time of 20 minutes at 98,076 mg/L. The highest total tannin compound was obtained in the variable sample-solvent ratio of 1:15, particle size of 60 mesh, and time of 10 minutes at 41,697 mg/L. The highest total alkaloid compound was obtained in the variable sample-solvent ratio of 1:10, particle size of 100 mesh, and time of 20 minutes at 10,092 mg/L. The optimum curing time for tuna is 36 hours at room temperature with variable sample-solvent ratio, time, and particle size of 1:20 g/mL, 20 minutes, and 100 mesh with 20% concentration. The running has the highest flavonoid compounds, so it can be concluded that flavonoid compounds have a major effect on the preservation process of tuna.
EKSTRAKSI PROTEIN DARI SPIRULINA SP DALAM PELARUT ETANOL TERBANTUKAN GELOMBANG ULTRASONIK Boy Arief Fachri; Bekti Palupi; Istiqomah Rahmawati; Meta Fitri Rizkiana; Helda Wika Amini
Jurnal Penelitian Sains dan Teknologi Indonesia Vol 1 No 1 (2022): Jurnal Hasil Penelitian UNIVERSITAS JEMBER
Publisher : Lembaga Penelitian dan Pengabdian Kepada Masyarakat (LP2M) Universitas Jember

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.19184/jpsti.v1i1.90

Abstract

Protein merupakan komponen nutrisi yang dibutuhkan oleh manusia untuk kesehatan tubuh. Salah satu sumber protein yang melimpah di Indonesia adalah alga Spirulina Sp. Ekstraksi protein alga, sulit dilakukan. Hal ini dikarenakan, protein tersimpan dalam sel-sel alga yang memiliki dinding yang sangat keras. Metode konvensional yang selama ini dilakukan membutuhkan waktu yang sangat lama, dan energi yang besar. Untuk mengatasi hal itu, sebuah metode alternatif yang diajukan dalam penelitian ini, adalah metode ekstraksi ultrasonik. Tujuan penelitian ini adalah untuk menentukan kondisi optimum ekstraksi protein dari Spirulina Sp dan mengetahui pengaruh parameter ekstraksi terhadap yield. Sprirulina Sp yang tekah dikeringkan dan dihaluskan diumpankan ke dalam ekstraktor yang berisi etanol. Gelombang ultrasonic, kemudian dialirkan ke dalam ekstraktor melalui probe. Setelah, eaktu ekstraksi tercapai, ekstrak dan residu dipisahkan dengan cara sentrifugasi dengan kecepatan 10000 rpm pada suhu kamar. Selanjutnya, yield protein ekstrak dihitung dengan analisa Lowry-Bradford. Pengaruh parameter proses seperti rasio bahan baku-pelarut (0:1-0.5) g/mL, ukuran partikel bahan baku (600-800) mesh dan waktu ekstraksi 15-45 menit) terhadap yield akan diamati dalam penelitian ini. Berdasarkan hasil penelitian, dapat disimpulkan bahwa yield tertinggi sebesar 80,87 % diperoleh pada kondisi rasio bahan baku-pelarut 0.2 g/mL, ukuran partikel bahan baku 700 mesh dan waktu ekstraksi 30 menit. Sementara itu, ukuran partikel merupakan parameter yang paling signifikan.
Application of Appropriate Technology Purification Oil Based on Cocoa Bark (Theobroma cacao L.) As Bio-Adsorbent for Purification of Used Cooking Oil in Kedaton Plantation, Panti Village Hakiki, Rizki Maulana; Tiana Febrianti Eka Prasetyani; Rossi Agnessi Pebriana; Amelia Permata Ayunda; Syeikh Maulana Bima Suci; Amellyah Isna Ainaiyah; Mutiara Rengganis Nurul Putri Azhari; Isni Salma Salsabillah; Sekar Jasmin Azzahra; Nico Dimas Saputro; Istiqomah Rahmawati
Jurnal Inovasi Sains dan Teknologi untuk Masyarakat Vol. 2 No. 2 (2024): November
Publisher : Faculty of Mathematics and Natural Sciences, University of Jember. Jl. Kalimantan No.37, Krajan Timur, Jemberlor, Kec. Sumbersari, Jember Regency, East Java 68121

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.19184/instem.v2i2.1158

Abstract

Using cooking oil repeatedly will have an impact on health. Cooking oil repeatedly changes color to a darker color, produces an unpleasant odor, and has high levels of fatty acids. Cooking oil experiences changes due to the chemical properties of cooking oil, such as a reaction where the color changes to brown when cooking oil is used at high temperatures by reacting with air. Therefore, it is necessary to purify used cooking oil to be used as a material that is more beneficial to society. The utilization of cocoa shell waste into carbon that has been processed is used for the adsorption process of purification of used cooking oil. The process of purifying used cooking oil begins with making activated charcoal, chemical activation of activated charcoal with hydrochloric acid (HCl), assembling appropriate technology for oil purification, adsorption process of used cooking oil which goes through several stages of purification, namely zeolite stone, cotton, cocoa charcoal, cotton and filter cloth. , and the process of using purified used cooking oil into aromatherapy candles. The materials used in making candles are paraffin and used cooking oil in a 1:1 ratio. Candles are packaged attractively to provide consumers and add selling value. This activity attracted the enthusiasm of the community to utilize used cooking oil into aroma therapy candles. In addition, the Panti Village Tourism Awareness Group is interested in utilizing used cooking oil to make souvenir aroma therapy candles at Panti village tourist attractions.It is hoped that using used cooking oil that has been purified into aromatherapy candles will become a source of income for the people of Kedaton Plantation, reducing waste disposal so that the environment will be better protected.
Evaluasi Efektivitas Kolom Biofilter dengan Media Campuran untuk Pengolahan Limbah Cair Tahu Eka, Silvia Devi Eka Putri; Mutiara Dewi Rukmana; Istiqomah Rahmawati; Tazkia Maulida Putri; Zahwa Annaya
Journal of Biobased Chemicals Vol. 5 No. 1 (2025): Journal of Biobased Chemicals
Publisher : Program Studi Teknik Kimia Universitas Jember

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.19184/jobc.v5i1.5595

Abstract

Indonesia's increasing number of tofu industries has led to a rise in waste volume from this sector, requiring exceptional management. Tofu wastewater, a byproduct of tofu production that is no longer utilized, contains a high concentration of organic matter and can adversely affect water supplies if discharged untreated. This study aims to investigate an efficient filtration technique using filtration media for processing tofu wastewater. The biofilter column used in this study was made from a Le Minerale gallon and comprised layers of zeolite, bio balls, bearings, and activated charcoal to filter and purify the water from organic substances. The results showed that while filtration effectively reduced Total Dissolved Solids (TDS) from 995 ppm to 129 ppm after the fourth filtration, it was ineffective in neutralizing the pH of the tofu wastewater, which remained at pH 4 before and after filtration. This indicates that the wastewater remains acidic and cannot be directly discharged into the environment. Additionally, conductivity and salt levels increased after multiple filtrations, possibly due to ion release from the filter materials or saturation effects. This study reveals that the column configuration and filtration materials used were ineffective in removing acidic components from tofu wastewater. Therefore, design adjustments and filtration media selection are needed to achieve better results in treating tofu wastewater.