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All Journal Jurnal Teknologi Perikanan dan Kelautan Hemera Zoa Jurnal Online Mahasiswa (JOM) Bidang Ilmu Sosial dan Ilmu Politik Science and Technology Indonesia JURNAL TEKNIK El-Faqih : Jurnal Pemikiran dan Hukum Islam Jurnal Teknik Elektro JAMER Jurnal Media Akademik (JMA) Jurnal Pengabdian Masyarakat Indonesia (JPMI)
Muhammad Imron
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Journal : Science and Technology Indonesia

 1 
Pillarization of double layer hydroxides using H3[-PW12O40]nH2O: effect of pillarization time Muhammad Imron; Muhammad Said
Science and Technology Indonesia Vol. 2 No. 2 (2017): April
Publisher : Research Center of Inorganic Materials and Coordination Complexes, FMIPA Universitas Sriwijaya

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (603.57 KB) | DOI: 10.26554/sti.2017.2.2.45-49

Abstract

The pillarization of Mg/Al double layer hydroxides using polyoxometalate H3[α-PW12O40]·nH2O by comparing the pillarization time i.e. 3 hours, 6 hours, 9 hours, 12 hours, 24 hours, 36 hours and 48 hours has been done. The product of a pillarization was characterized using an FT-IR spectrophotometer and XRD analysis. The result characterization of FT-IR spectrophotometer does not show the optimum of pillarization each time condition. Characterization using XRD shows the optimum pillarization process at 36 hours by showing the existence of double layer hydroxides material at diffraction angle 11.69o deg, 18.30o deg and 34.71o deg. Diffraction in the 60o-63o deg indicates the existence of a pillarization double layer hydroxides. Keywords: Layered double hydroxides, pillarization, polyoxometalate H3[α-PW12O40]·nH2O.
Adsorption of procion red using layer double hydroxide Mg/Al Muhammad Imron; Muhammad Said; Aldes Lesbani
Science and Technology Indonesia Vol. 2 No. 3 (2017): July
Publisher : Research Center of Inorganic Materials and Coordination Complexes, FMIPA Universitas Sriwijaya

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (398.765 KB) | DOI: 10.26554/sti.2017.2.3.64-67

Abstract

Layer double hydroxide Mg/Al was synthesized by inorganic synthetic method. Material was characterized using FTIR and XRD analyses and used as adsorbent of procion red dye in aqueous medium. Factors that affect the adsorption process are adsorption time as the kinetic parameter; and the temperature and concentration of procion red as the thermodynamic parameter. FTIR spectra of layer double hydroxides showed unique vibration at wavenumber 1300 cm-1 and 1600 cm-1. Characterization using XRD shows diffraction angles at 29o, 27o, and 28o, which are typical of Mg/Al double layer hydroxides. Adsorption of procion red using layer double hydroxide Mg/Al resulted adsorption rate 7.1 minutes-1, maximum adsorption capacity 111.1 mg/g at 60 oC with increasing energy by increasing adsorption temperature. Keywords: Layered double hydroxides, adsorption, procion red.
Co-Authors Aldes Lesbani Andi Setiawan Andri Sulistyani Atin Supriatin Babun Suharto Bambang Purwantara Daniel Rezki Elva Ramadianti Elva Ramadiyanti Emarotus Sholeha Evi Dwi Mualifah Farihin Hery Widijanto Moch. Chotib Muhammad Said Mulyono S. Baskoro novy rachma herawati Oloan Parlindungan Ronny I. Wahju Tri Wahyu Hidayat Widyu Nazzillah Khoirun Nisa Yanyan Setiawan Yulia Amelia