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All Journal Reaktor Jurnal Teknik ITS IPTEK Journal of Proceedings Series The Journal of Pure and Applied Chemistry Research Indonesian Journal of Chemistry Walisongo Journal of Chemistry REACTOR : Journal of Research On Chemistry And Engineering Sewagati Bulletin of Chemical Reaction Engineering & Catalysis
Danawati Hari Prajitno
Departemen Teknik Kimia Industri Institut Teknologi Sepuluh Nopember Surabaya
Agriculture, Biological Sciences & Forestry Arts Humanities Chemical Engineering, Chemistry & Bioengineering Chemistry Computer Science & IT Control & Systems Engineering Education Energy Engineering Languange, Linguistic, Communication & Media Materials Science & Nanotechnology Medicine & Pharmacology Public Health Social Sciences Other

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Journal : bulletin of chemical reaction engineering

 1 
Hydrocracking of Non-edible Vegetable Oils with Co-Ni/HZSM-5 Catalyst to Gasoil Containing Aromatics Danawati Hari Prajitno; Achmad Roesyadi; Muhammad Al-Muttaqii; Lenny Marlinda
Bulletin of Chemical Reaction Engineering & Catalysis 2017: BCREC Volume 12 Issue 3 Year 2017 (December 2017)
Publisher : Masyarakat Katalis Indonesia - Indonesian Catalyst Society (MKICS)

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.9767/bcrec.12.3.799.318-328

Abstract

Biofuel has been considered as one of the environmentally friendly energy sources to substitute fossil fuel derived from non-edible vegetable oil. This research aims to investigate the effect of the non-edible vegetable oil composition on a specific hydrocarbons distribution contained in biofuel and the aromatics formation through hydrocracking reaction with the Co-Ni/HZSM-5 catalyst. The formation of aromatics from non-edible vegetable oils, such as: Cerbera manghas, rubber seed, and sunan candlenut oils, containing saturated, mono- and polyunsaturated fatty acids is presented. The hydrocracking reaction was carried out in a pressure batch reactor, a reaction temperature of 350 oC for 2 h, reactor pressure of 15 bar after flowing H2 for 1 hour, and a catalyst/oil ratio of 1 g/200 mL. Liquid hydrocarbon product was analyzed by gas chromatography-mass spectrometry. Based on the GC-MS analysis, hydrocracking on three different oils indicated that polyunsaturated fatty acids were required to produce relatively high aromatics content. The sunan candlenut oil can be converted to gasoil range hydrocarbons containing a small amount of aromatic through hydrocracking reaction. Meanwhile, the aromatics in liquid product from hydrocracking of Cerbera manghas and rubber seed oils were not found. 
Zn-Mo/HZSM-5 Catalyst for Gasoil Range Hydrocarbon Production by Catalytic Hydrocracking of Ceiba pentandra oil Yustia Wulandari Mirzayanti; Firman Kurniawansyah; Danawati Hari Prayitno; Achmad Roesyadi
Bulletin of Chemical Reaction Engineering & Catalysis 2018: BCREC Volume 13 Issue 1 Year 2018 (April 2018)
Publisher : Masyarakat Katalis Indonesia - Indonesian Catalyst Society (MKICS)

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.9767/bcrec.13.1.1508.136-143

Abstract

Biofuel from vegetable oil becomes one of the most suitable and logical alternatives to replace fossil fuel. The research focused on various metal ratio Zinc/Molybdenum/HZSM-5 (Zn-Mo/HZSM-5) catalyst to produce liquid hydrocarbon via catalytic hydrocracking of Ceiba penandra oil. The catalytic hydrocracking process has been applied in this study to crack Ceiba pentandra oil into a gasoil range hydrocarbon using Zn-Mo/HZSM-5 as a catalyst. The effect of various reaction temperature on the catalytic hydrocracking of Ceiba pentandra oil were studied. The Zn-Mo/HZSM-5 catalyst with metal ratio was prepared by incipient wetness impregnation method. This process used slurry pressure batch reactor with a mechanical stirrer. A series of experiments were carried out in the temperature range from 300-400 oC for 2 h at pressure between 10-15 bar. The conversion and selectivity were estimated. The liquid hydrocarbon product were identified to gasoline, kerosene, and gas oil. The results show that the use of Zn-Mo/HZSM-5 can produce gas oil as the most component in the product. Overall, the highest conversion and selectivity of gas oil range hydrocarbon was obtained when the ZnMo/HZSM-5 metal ratio was Zn(2.86 wt.%)-Mo(5.32 wt.%)/HZSM-5 and the name is Zn-Mo/HZSM-5_102. The highest conversion was obtained at 63.31 % and n-paraffin (gas oil range) selectivity was obtained at 90.75 % at a temperature of 400 oC. Ceiba pentandra oil can be recommended as the source of inedible vegetable oil to produce gasoil as an environmentally friendly transportation fuel. 
Bio-kerosene and Bio-gasoil from Coconut Oils via Hydrocracking Process over Ni-Fe/HZSM-5 Catalyst Muhammad Al-Muttaqii; Firman Kurniawansyah; Danawati Hari Prajitno; Achmad Roesyadi
Bulletin of Chemical Reaction Engineering & Catalysis 2019: BCREC Volume 14 Issue 2 Year 2019 (August 2019)
Publisher : Masyarakat Katalis Indonesia - Indonesian Catalyst Society (MKICS)

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.9767/bcrec.14.2.2669.309-319

Abstract

In this study, hydrocracking of coconut oil over Ni-Fe/HZSM-5 catalyst was carried out in a batch reactor under different reaction temperature. Coconut oil is proposed as one of the potential feedstock for biofuel production. The Ni-Fe/HZSM-5 catalyst was prepared by incipient wetness impregnation method. The characterization of Ni-Fe/HZSM-5 catalyst by X-Ray Diffraction (XRD), Scanning Electron Microscopy-Energy Dispersive X-ray (SEM-EDAX), and Brunauer-Emmett-Teller (BET). The chemical composition of biofuel was analyzed by Gas-Chromatography-Mass Spectrometry (GC-MS). The results from the GC-MS analysis showed that the hydrocracking reaction over 10 % (Ni-Fe)/HZSM-5 catalyst at temperature of 375 oC obtained the highest hydrocarbon content (contained 49.4% n-paraffin, 26.93 % isoparaffin, 3.58 % olefin) and the highest yield of bio-gasoil 38.6 % in the biofuel liquid hydrocarbon. Pentadecane (n-C15) and heptadecane (n-C17) were the most abundant hydrocarbon compounds in biofuel liquid hydrocarbon. Decarboxylation and/or decarbonylation was the dominant reaction pathways in this process. Based on the result, the reaction temperature had a significant effect on the distribution of biofuel composition and yield of biofuel from coconut oil.
Co-Authors Achmad Roesyadi Adi Soeprijanto Agus Budianto Agus Surono Agustiani, Elly Ahmad Nezard Dhiaulhaq Altway, Saidah Eko Supriadi Firman Kurniawansyah Hafshah Hafshah Hafshah Hafshah Ignatius Gunardi Irfan Ramadhitya Karenina Anisya Pratiwi Karenina Anisya Pratiwi Kusno Budhikarjono Lailatul Qomariyah Lenny Marlinda Lily Pudjiastuti, Lily Mahfud Mahfud Mahfud Mahfud Mochammad Zayyan Difa Fadhillah Mochammad Zayyan Difa Fadhillah Muhammad Al Muttaqii Muhammad Al Muttaqii Muhammad Al-Muttaqii Muhammad Al-Muttaqii Muhammad Al-Muttaqii Muhammad Al-Muttaqii Muhammad Iqbal N Nurjannah, N Nurjannah Ngatijo Ngatijo Nurjannah Nurjannah Nurjannah Nurjannah Rachmaniah, Orchidea Rahmat Basuki Ratna Ediati Santi Dyah Savitri Tillotama Anindita Sari Victor Purnomo Yustia Wulandari Mirzayanti Zuchrillah, Daril Ridho