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Sunarto Sunarto
FMIPA UNY
Decision Sciences, Operations Research & Management

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EFFECT OF MORDAN SYNTHESIS OF CANNED WASTE TO POWER IKAT DAN LAJU REMOVED METHYL VIOLET COLOR DYES BY FABRIC FIBER EFFECT OF MORDAN SYNTHESIS OF CANNED WASTE TO POWER Jaslin Ikhsan; Endang Widjayanti LFX; Sunarto Sunarto
Jurnal Penelitian Saintek Vol 19, No 1: April 2014
Publisher : Institute of Research and Community Services, Universitas Negeri Yogyakarta

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (1379.186 KB) | DOI: 10.21831/jps.v19i1.2330

Abstract

This study aims to determine: the binding capacity of cloth toward methylene violet (MV) dye, the rate of releaseof methyl violet from cloth due to washing, and the effect of the addition of the mordant to the binding capacity and the rate of release. pH, temperature, and equilibrium time were always maintained in all experiments. Data of binding capacity were collected by isothem experiments and performed by measuring the concentration of methyl violet bound by cloth at various added-concentrations of methylene violet. Collected  data were analyzed with a Langmuir and Freundlich isotherm equations. Data of release rate were collected by mesuring the concentration of free methylene violet dye in solution due to washing as a function of time. The release data were analyzed using the Lagergren rate equation. The analysis showed that bonding between methylene violet and cloth occurs with releasing protons and via hydrogen bonds. Binding capacity was represented by the Freundlich isotherm equation on which the capacity was decreased by the addition of mordant, with represented bythe constants of k 1 , 2.45 x 10 -8  and 1.75 x 10-8  M MV per gram of cloth, respectively. The addition of mordant also deceleratedoubly the releaseof MV from cloth due to washing whose constants k - 2 were 2103.039 and 1013.958 mmol g-1 min-1, respectively.   
LANTANUM COMPLEXASI STUDY WITH MAKROSIKLIS COMPOUND AND CHARACTERIZATION AS SELECTIVE ELECTRONIC ION LANTANUM Suyanta Suyanta; Sunarto Sunarto; Lis Permana Sari
Jurnal Penelitian Saintek Vol 16, No 2: Oktober 2011
Publisher : Institute of Research and Community Services, Universitas Negeri Yogyakarta

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (525.497 KB) | DOI: 10.21831/jps.v16i2.3389

Abstract

The aim of this research are (1) to study the complexation constant of La(III) ion by N,N’-dikarboksimetildiaza-18-crown-6 ligant with difference concentration of KNO3, and (2) to study the lanthanum (III) ion selective electrode (La-ISE) potential response which follows the Nernst equation. The characters of the electrode studied are: response time, life time, detection limit, dynamic range and selectivity. The complexation constant of La(III) ion by N,N’- dikarboksimetildiaza-18-crown-6 ligant are finded by potentiometry titration with 0.0005 M, 0.001 M, dan 0.005 M KNO3 supported electrolite. The titration are doing by 0.00794 M KOH until pH 7. The result of constant complexation (Kf) La(III) ion with N,N’-dikarboksimetildiaza-18-crown-6 difference KNO3 0.005 M, 0.001 M, dan 0.005 M simultaniuesly are 101,02 , 101,12, dan 101,32. The electrode had a response time of 27.14 ± 4.79 seconds and could be used for 50 days. The linear range was between 10-5 M to 10-1 M and the detection limit is 3.92x10-6 M.
TRANSISI FASA TITATNIUM OKSIDA MELALUI KONDENSASI EX-SITU HIDROGEN TITANAT TIPE STRUKTUR LEPIDOKSROSIT Hari Sutrisno; Sunarto Sunarto
Jurnal Penelitian Saintek Vol 15, No 1: April 2010
Publisher : Institute of Research and Community Services, Universitas Negeri Yogyakarta

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (3666.901 KB) | DOI: 10.21831/jps.v15i1.1732

Abstract

The objectives of the research are to study of the structure type of titanium dioxide (TiO2) obtained form the ex-situ condensation of hydrated hydrogen titanates with the structure type of lepidocrocite. Hydrated hydrogen titanates were obtained by ion exchabge of H+ for Cs+ in cesium titanates by 1 M HCl solution by Chimie Douce method. The results show that TiO2 (B), anatase, and anatase-rutile mixture were obtained heat treatment of hydrated hydrogen titanate at 100, 200, 300, 500, and 600oc respectively. The powders were characterized by X-rays diffractometer (XRD), High Resolution Scanning Electron Microscopy (HRSEM) and High Resolution Transmission Electron Microscopy (HRTEM). The research indicated that the protonic titanate, H0.54 Ti1.865 0.135O4 0.5H2O ( =vacancy), lost the interlayer water by being heated up to 200oC to produce a dehydrated phase, H0.54 Ti1.865 0.135O4. Above 300oC, the dehydrated phase completely transformed to TiO2(B) and anatase was obtained as pure phase at 600oC. The phase transformed as the following process: H0.54Ti1.865 0.135O4 0.5H2O à H0.54Ti1.865 0.135O4 0.25H2Oà H0.54Ti1.865 0.135O4 à TiO2(B) à TiO2-anatase.
Co-Authors Endang Widjayanti LFX Hari Sutrisno Jaslin Ikhsan Rr. Lis Permana Sari Suyanta Suyanta