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All Journal JURNAL KIMIA SAINS DAN APLIKASI e-Journal Pustaka Kesehatan Jurnal Pengembangan Pendidikan STOMATOGNATIC- Jurnal Kedokteran Gigi Jurnal Kimia Terapan Indonesia Eksakta : Berkala Ilmiah Bidang MIPA Jurnal Ilmiah Farmasi Farmasyifa Jurnal Ilmiah Ibnu Sina (JIIS): Ilmu Farmasi dan Kesehatan Al-Khidmah Jurnal Pengabdian Masyarakat Journal of Pharmacy Science and Technology Borneo Journal of Pharmacy
Ayik Rosita Puspaningtyas1
Faculty Of Pharmacy, University Of Jember, Jember, East Java|University Of Jember|Indonesia
Religion Agriculture, Biological Sciences & Forestry Humanities Astronomy Biochemistry, Genetics & Molecular Biology Chemical Engineering, Chemistry & Bioengineering Chemistry Civil Engineering, Building, Construction & Architecture Computer Science & IT Decision Sciences, Operations Research & Management Education Energy Engineering Environmental Science Health Professions Immunology & microbiology Languange, Linguistic, Communication & Media Library & Information Science Materials Science & Nanotechnology Mathematics Mechanical Engineering Medicine & Pharmacology Social Sciences

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Journal : Journal of Pharmacy Science and Technology

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PENGEMBANGAN VALIDASI METODE DAN PENETAPAN KADAR AKRILAMIDA PADA UBI JALAR GORENG SECARA KROMATOGRAFI LAPIS TIPIS-DENSITOMETRI Ayik Rosita P
JOURNAL OF PHARMACY SCIENCE AND TECHNOLOGY Volume 2 No. 2: Desember 2021
Publisher : Prodi Farmasi Fakultas Kedokteran Universitas Hang Tuah

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.30649/pst.v3i1.107

Abstract

A thin-layer chromatography (TLC) Densitometric method for analyzing acrylamide in fried sweet potatoes is not reported before. The research aims to determine the development of acrylamide validation and acrylamide concentration in fried sweet potatoes. The retardation factor for evaluating acrylamide uses silica gel column 254 with range 0.4-0.5 and eluate by methanol: benzene (2:1) was analyzed in a maximum wavelength of 200 nm. Linear response of acrylamide standard was tested within a 120-300 ppm concentration range, and the correlation coefficient (r) more remarkable than 0,99, detection limit 17.45 ppm and quantitative limit 52.36 ppm. Sample preparation was performed by ethanol 70%. The precision resulted from 2,67%, and this result was less than 16% (literature). Percentage of recoveries 98,18 %, and in the literature, 98%-102%. The TLC densitometric method is selective, precise, and accurate. Finally, the research showed that fried sweet potatoes contain acrylamide less than 230,32 ng samples, so the selection is very safe to consume.
Co-Authors . Ifada Ari Satia Nugraha Bambang Kuswandi Brahmansyah Diar Rosiarto Carolin Enjelin Rumaikewi Dian Agung Pangaribowo Dian Agung Pangaribowo Diana Holidah Dyah Purwaningtyas Dyan Wigati Eka Mustika Wati Estu Wilujeng Fathunnisa Fathunnisa Fifteen Aprila Fifteen Aprila Fajrin Hadiyatun Nuroniyah Hasana, Ani Riani Ika Oktavianawati Ika Oktavianawati Indah Purnama Sari Indah Purnama Sary Indah Purnama Sary Indah Purnama Sary, Indah Purnama Lindawati Setyaningrum Maasyitoh Sari Latifah Mohammad Rofik Usman Nia Kristiningrum Puspita Arum Wijayanti Tasya Salsabila Multazam Triodora Hutahuruk Wahyu Novandari Herdiyanti Yuni Retnaningtyas