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All Journal JURNAL KIMIA SAINS DAN APLIKASI Bulletin of Chemical Reaction Engineering & Catalysis Jurnal Riset Kimia Science and Technology Indonesia Molekul: Jurnal Ilmiah Kimia Sains dan Matematika Darma Sabha Cendekia Molekul: Jurnal Ilmiah Kimia Bulletin of Chemical Reaction Engineering & Catalysis
Anung Riapanitra
Department Of Chemistry, Faculty Of Mathematics And Natural Sciences, Jenderal Soedirman University, Purwokerto|Jenderal Soedirman University|Indonesia
Astronomy Biochemistry, Genetics & Molecular Biology Chemical Engineering, Chemistry & Bioengineering Chemistry Economics, Econometrics & Finance Engineering Environmental Science Materials Science & Nanotechnology Mathematics Physics

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Pelatihan Uji Formalin Menggunakan Smartphone dan Scanner untuk Siswa SMA Amin Fatoni; Mekar Dwi Anggraeni; Anung Riapanitra; Zusfahair Zusfahair
Darma Sabha Cendekia Vol 3 No 3 (2021): Darma Sabha Cendekia - November 2021
Publisher : Pasca Sarjana | Universitas Jenderal Soedirman

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (438.058 KB) | DOI: 10.20884/1.dsc.2021.3.3.5000

Abstract

Sekolah Menengah Atas (SMA) sudah mengajarkan pembelajaran kimia, namun demikian, belum semua melaksanakan praktikum untuk lebih memahami ilmu kimia, karena keterbatasan saran terutama alat dan petunjuk praktikumnya. Keterbatasan instrumentasi yang mahal memicu para peneliti untuk memanfaatkan alat-alat sederhana disekitar kita seperti kamera smartphone, kamera poket, kamera DSLR dan alat pemindai dokumen (scanner) sebagai alternatif instrumentasi kimia. Kegiatan Pengabdian masyarakat ini dikenalkan teori untuk meningkatkan pengetahuan siswa dan praktik untuk meningkatkan keterampilan siswa tentang penggunaan kamera smartphone dan scanner sebagai alat analisis kadar formalin. Hasil kegiatan pengabdian kepada masyarakat menunjukkan pemberian materi menunjukkan peningkatan pengetahuan dari skor rata-rata 68 menjadi 80, sedangkan praktikum dikelas memberikan peningkatan pengetahuan alat, bahan dan prosedur analisis kimia menggunakan smartphonedan scanner dari skor rata-rata 54,7 menjadi 86
Ointment Formulation of Arumanis Mango (Mangifera indica L.) Leaf Extract with Chitosan Tripoliphosphate Matrix as Antibacterial Dian Riana Ningsih; Anung Riapanitra; Zusfahair Zusfahair; Uyi Sulaeman; Istinganatun Khoeriyah
Molekul Vol 18 No 1 (2023)
Publisher : Universitas Jenderal Soedirman

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.20884/1.jm.2023.18.1.5725

Abstract

This report presented the synthesis of Arumanis mango (Mangifera indica L.) leaf extract with chitosan tripolyphosphate matrix and its antibacterial activity. This research aimed to obtain an ointment formulation from mango leaf extract with chitosan tripolyphosphate matrix, to figure out the characteristics, including the particle morphology, and to determine the optimum formulation and the characterization of the antibacterial ointment. The research showed that extract morphology with chitosan tripolyphosphate was uneven-edge aggregates. Antibacterial tests were conducted on P. acnes and E. coli bacteria. The formula giving the greatest antibacterial activity was further utilized for the ointment preparations and then was characterized for 16 days. Formula C (chitosan and NaTPP 1: 0.0992(%)) gave the most excellent inhibition zone for P. acnes and E. Coli bacteria, at 7.94 mm and 10.02 mm, respectively. The obtained ointment preparation was white color homogeneous semi-solid with protective properties. The spreading power of the ointment was 5.25 – 6.25 cm, with the adhesive power of 1 – 5 seconds and pH of 6.0 – 6.4. The ointment's antibacterial activity was tested against P. acnes and E. coli bacteria using the formation of inhibition zone method. The activity of ointment prepared on day one against P. acnes and E. coli was at 14.03 mm and 14.24 mm, respectively, while the activity on day 16 against P. acnes and E. coli was at 9.33 mm and 9.98 mm, respectively.
Facile Synthesis of Ag3PO4 Photocatalyst with Varied Ammonia Concentration and Its Photocatalytic Activities For Dye Removal Febiyanto Febiyanto; Agus Soleh; Muhammad Sofi Khoerul Amal; Mohammad Afif; Sukma Sewiji; Anung Riapanitra; Uyi Sulaeman
Bulletin of Chemical Reaction Engineering & Catalysis 2019: BCREC Volume 14 Issue 1 Year 2019 (April 2019)
Publisher : Masyarakat Katalis Indonesia - Indonesian Catalyst Society (MKICS)

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.9767/bcrec.14.1.2549.42-50

Abstract

The highly active photocatalyst of Ag3PO4 could be synthesized under ammonia solution using the facile co-precipitation method with the starting material of AgNO3 and Na2HPO4.12H2O.  The variation of ammonia concentration was designed at 0.00, 0.05, 0.15, and 0.30 M. The products were characterized using X-ray diffraction, UV-diffuse reflectance spectroscopy, and scanning electron microscopy. The photocatalytic activities were evaluated using the Rhodamine B degradation under blue light irradiation.  The effect of calcination, pH condition, and visible light source irradiation was carried out in the experiment. The highest photocatalytic activity was found in the sample prepared using the addition of ammonia solution at the concentration of 0.05 M. This photocatalytic activity was 4.13 times higher compared to the Ag3PO4 prepared without the ammonia. The effective condition of photocatalytic activity was achieved at the sample prepared without calcination, degradation at pH of 7 and under blue light irradiation. 
The Surface Modification of Ag3PO4 using Tetrachloroaurate(III) and Metallic Au for Enhanced Photocatalytic Activity Uyi Sulaeman; Richo Dwi Permadi; Alfa Marcorius; Hartiwi Diastuti; Anung Riapanitra; Shu Yin
Bulletin of Chemical Reaction Engineering & Catalysis 2021: BCREC Volume 16 Issue 4 Year 2021 (December 2021)
Publisher : Masyarakat Katalis Indonesia - Indonesian Catalyst Society (MKICS)

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.9767/bcrec.16.4.10863.707-715

Abstract

The improvement of Ag3PO4 photocatalytic activity was successful by incorporating tetrachloroaurate(III) (AuCl4−)  and metallic Au on the surface of Ag3PO4. The photocatalysts were synthesized using the coprecipitation and chemisorption method. Coprecipitation of Ag3PO4 was carried out under ethanol-water solution using the starting material of AgNO3 and Na2HPO4.12H2O. AuCl4− ion and metallic Au were incorporated on the surface of Ag3PO4 using a chemisorption method under auric acid solution. The photocatalysts were characterized using XRD, DRS, SEM, and XPS. The AuCl4− ion and metallic Au were simultaneously incorporated on the Ag3PO4 surface. The high photocatalytic activity might be caused by increasing the separation of hole and electron due to capturing photogenerated electrons by metallic Au and Au(III) as electron acceptors. Copyright © 2021 by Authors, Published by BCREC Group. This is an open access article under the CC BY-SA License (https://creativecommons.org/licenses/by-sa/4.0). 
Photodegradation of Methylene Blue Dye Using BiVO₄/g-C₃N₄ Composites under Visible Light Irradiation Anung Riapanitra; Tien Setyaningtyas; Ghinatanitha Haqqu Haryadinaru
Jurnal Kimia Sains dan Aplikasi Vol 27, No 8 (2024): Volume 27 Issue 8 Year 2024
Publisher : Chemistry Department, Faculty of Sciences and Mathematics, Diponegoro University

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.14710/jksa.27.8.363-370

Abstract

This study evaluates the degradation of methylene blue through photocatalysis using BiVO4/g-C3N4 material with the help of visible light. Material characterization was conducted using X-ray diffraction, scanning electron microscopy, and UV-Vis diffuse reflectance spectroscopy data. The characterization results show that the crystal structure of BiVO4/g-C3N4 is a heterojunction between monoclinic BiVO4 and hexagonal g-C3N4, with a crystal size of about 10.16 nm and a band gap energy value of about 2.16 eV. The morphology formed is a combination of sheet and rod-like. This study optimized the photocatalytic activity of the composite by analyzing the variation of g-C3N4 concentration, degradation time, and methylene blue pH. The results show that the BiVO4/g-C3N4 sample has optimal photocatalytic and adsorption properties in sample B (1:3) with pH 7 and a degradation time of 150 minutes. Under these conditions, the BiVO4/g-C3N4 composite successfully degraded methylene blue by 94.14%. The rate kinetics of the photocatalytic reaction followed first order, with *OH species playing the most role in the degradation mechanism. These findings highlight the potential of BiVO4/g-C3N4 as an effective photocatalyst material for organic pollutant degradation applications, offering a sustainable solution for wastewater treatment.
Nigella Sativa-mediated Synthesis of BiVO4/g-C3N4 Composites for the Removal of Methylene Blue Dye Haryadinaru, Ghinatanitha Haqqu; Setyaningtyas, Tien; Riapanitra, Anung
Bulletin of Chemical Reaction Engineering & Catalysis 2025: BCREC Volume 20 Issue 2 Year 2025 (August 2025)
Publisher : Masyarakat Katalis Indonesia - Indonesian Catalyst Society (MKICS)

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.9767/bcrec.20354

Abstract

This study investigates the synthesis and photocatalytic performance of BiVO4-Nigella Sativa/g-C3N4 composites for the degradation of methylene blue dye. The composites were synthesized using a coprecipitation method and characterized through various techniques, including X-ray diffraction (XRD), Fourier-transform infrared spectroscopy (FTIR), UV-Vis diffuse reflectance spectroscopy (DRS), Brunauer-Emmett-Teller (BET) surface area analysis, and scanning electron microscopy (SEM) to determine their crystal structure, chemical composition, morphology, adsorption and photocatalytic abilities. A variation of mass ratios of BiVO4 to g-C3N4 of 1:2, 1:3, and 1:4 was used in this investigation. The photocatalytic test results indicated that the composite with a mass ratio of 1:2 achieved the highest methylene blue degradation, reaching 91.73%, which was primarily attributed to an adsorption activity of 81.12% and a photocatalytic degradation of 10.60%. The photocatalytic activity was significantly enhanced under alkaline conditions, particularly at pH levels between 9 and 10, which facilitated the formation of reactive oxygen species (ROS). The study highlights the synergistic effects of the BiVO4 and g-C3N4 combination, which promotes efficient charge transfer, reduces electron-hole recombination, and expands light absorption due to a decrease in the effective bandgap energy. Overall, the findings indicate that BiVO4-Nigella Sativa/g-C3N4 composites have considerable potential for application in wastewater treatment, particularly for the remediation of organic dye pollutants. Copyright © 2025 by Authors, Published by BCREC Publishing Group. This is an open access article under the CC BY-SA License (https://creativecommons.org/licenses/by-sa/4.0).
Construction of Ternary Heterojunction g-C3N4 /BiVO4 /GQDs Nanocomposite and Its Methylene Blue Photodegradation Performance Arieveali, Heroldinho; Setyaningtyas, Tien; Riyani, Kapti; Riapanitra, Anung
Science and Technology Indonesia Vol. 10 No. 3 (2025): July
Publisher : Research Center of Inorganic Materials and Coordination Complexes, FMIPA Universitas Sriwijaya

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.26554/sti.2025.10.3.777-788

Abstract

Ternary heterojunction g-C3N4/BiVO4/GQDs (CBG) composite photocatalysts were successfully made by high-temperature solidstate method. The prepared CBG photocatalyst was used to degrade the methylene blue (MB) solution under the simulation of visible light irradiation. The analysis of photocatalytic activity was carried out in the parameters of mass variation of composite components, pH of MB solution, and kinetic rate measurement. The results showed that the adsorption-photocatalysis synergy effect occurred at its best in CBG-20 samples with pH 9 in MB solution with a degradation kinetic rate following the pseudo-first order within 150 min of removal time as the optimum condition that could degrade MB by 94.81%. The result showed that the photocatalytic activity of theternary composite was higher than that of pristine g-C3N4, BiVO4, or the binary composite of g-C3N4/BiVO4. Trapping experiments results support the direct dual Z-scheme which shows that ·O2- is the most significant radical for the photocatalytic degradation of MB. The prepared ternary composites show outstanding application prospects in wastewater treatment.
Physicochemical Characteristics of PVDF/ZSM-5 Composite Membrane for Potential Applications in Vanadium Redox Battery Alifia, Zaskia; Haryanto, Michael Julian; Fitriyani, Devi Ayu; Riapanitra, Anung
Jurnal Kimia Sains dan Aplikasi Vol 28, No 6 (2025): Volume 28 Issue 6 Year 2025
Publisher : Chemistry Department, Faculty of Sciences and Mathematics, Diponegoro University

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.14710/jksa.28.6.299-306

Abstract

Composite membranes were synthesized using poly-(vinylidene fluoride) (PVDF) and zeolite (ZSM-5) to improve the performance of PVDF as a battery separator. The PVDF-ZSM-5 membranes, prepared with varying concentrations of ZSM-5, underwent characterizations of X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FTIR), and scanning electron microscopy (SEM). These analyses revealed a notable increase in β-phase formation in PVDF, greater porosity, and improved surface morphology due to the incorporation of ZSM-5. Evaluations of their physicochemical properties showed that these membranes resulted in electrical conductivity up to 96.4 mS/cm, enhanced contact area, porosity reaching 78.61%, and flux value up to 5.4 ×10⁻2 L m⁻2 h⁻2. Adjustments in ZSM-5 concentrations proved instrumental in fine-tuning these performance metrics. These findings highlight the potential of PVDF-ZSM-5 membranes as a cost-effective membrane separator for redox battery systems. This research lays the groundwork for future advancements and broader commercial applications in energy storage technology.
Hydrothermal and Coprecipitation Synthesis Design of BiVO4 for Methylene Blue Degradation Riapanitra, Anung; Setyaningtyas, Tien; Haryanto, Michael Julian; Haryadinaru, Ghinatanitha Haqqu
Jurnal Riset Kimia Vol. 16 No. 1 (2025): March
Publisher : Universitas Andalas

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.25077/jrk.v16i1.740

Abstract

This study investigated the characteristics and photocatalytic activity of BiVO4 photocatalyst synthesized using hydrothermal and coprecipitation methods for methylene blue (MB) degradation under visible light. The variation of synthesis parameters, including pH, calcination temperature, and pH of MB solution, affects the crystal structure, morphology, and photocatalytic efficiency of the material. XRD characterization results show that the hydrothermal method produces BiVO4 with pure scheelite(m-s) monoclinic phase and high crystallinity, while the coprecipitation method produces a combination of scheelite(m-s) monoclinic and orthorhombic Bi4V2O11 phases, which contributes to enhanced photocatalytic activity through better charge separation. The average crystal size of the hydrothermal method is 17.85 nm, larger than that of coprecipitation (11.41-14.71 nm), which gives the coprecipitated material a surface area advantage. SEM analysis showed rod-like morphology in hydrothermal, while coprecipitation produced sphere-grape-like particles. UV-Vis DRS results show that hydrothermal synthesized BiVO4 has a band gap energy of 2.28 eV, smaller than BiV(4)(400) (2.46 eV) and higher than BiV(4)(550) (2.07 eV) synthesized using coprecipitation method. This smaller band gap energy indicates that the interaction of Bi³⁺ and VO₄³- ions in the hydrothermal material is better, thus favoring visible light absorption. The highest photocatalytic activity was obtained from the coprecipitated material with a degradation efficiency of 89.32% at pH 11 within 150 min, higher than the hydrothermal material which reached 76.06% under similar conditions. This photocatalytic activity was dominated by OH* and O2-* radicals, which play a role in MB degradation. This study shows that designing synthesis pH parameters (4-7), calcination temperature (400), and coprecipitation method produced a material with optimum photocatalytic performance, making BiVO4 a superior candidate for colored wastewater treatment applications.
Co-Authors Agus Soleh Alfa Marcorius Alifia, Zaskia AMIN FATONI Anas Rohadi Anas Rohadi Arieveali, Heroldinho Dian Riana Ningsih Dyah Indriastuti Febiyanto Febiyanto Fitriyani, Devi Ayu Ghinatanitha Haqqu Haryadinaru Hartiwi Diastuti Haryadinaru, Ghinatanitha Haqqu Haryanto, Michael Julian Istinganatun Khoeriyah Kapti Riyani Kapti Riyani Kapti Riyani Mardiyah Kurniasih Mardiyah Kurniasih Mekar Dwi Anggraeni Mohammad Afif Muhamad Wisnu Nugroho Muhammad Sofi Khoerul Amal Ponco Iswanto Richo Dwi Permadi Roy Andreas Shu Yin Sukma Sewiji Tien Setyaningtyas Tien Setyaningtyas Tien Setyaningtyas Uyi Sulaeman Uyi Sulaeman Uyi Sulaeman Uyi Sulaeman Uyi Sulaeman Zusfahair Zusfahair