Subaer Subaer
Jurusan Fisika FMIPA Universitas Negeri Makassar

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Journal : INDONESIAN JOURNAL OF APPLIED PHYSICS

Analisis Petrografi Fasa Molybdenum (Mo) dari Oksida Primer Fe2O3 Deposit Bontocani dengan Teknik X-Ray Mapping dan Difraksi Sinar-X Subaer S; Nurhayati N; Nurhasmi N; Nurfadillah N
INDONESIAN JOURNAL OF APPLIED PHYSICS Vol 4, No 02 (2014): October
Publisher : Department of Physics, Sebelas Maret University

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.13057/ijap.v4i02.4976

Abstract

A researh related to petrogaphy analysis of molybdenum (Mo) has been conducted. The main objective of this study is to get quantitative information about the composotion of molybdenum (Mo) as a minor phase of primer mineral Fe2O3 deposited at Bontocani, District of Bone South Sulawesi. The petrography analysis was performed on 10 samples by means of Tescan Vega3SB Scanning Electron Microscopy (SEM) coupled with Bruker X-Ray Mapping and Energy Dispersive Spectroscopy (EDS). Crystallinity level and chemical composition(phase) mineral constituent were performed by using MiniFlexII X-Ray Diifraction (XRD). The petrography analysis in the form of elemental mapping show the position of Mo along with Fe, S and other elements. The XRD analysis showed that that the Mo mineral of Bontocani deposit is found in the form of pure Mo element with a concentration of 0.2 – 8.0 wt%, compound of Fe17(Mo3)0.1 and Fe2(MoO4)3 with a concentration of 2.04 wt% and 14.0 wt%.
Sintering Temperature Effect to the Synthesis of SiC Produced from Rice Husk ash and 2B Graphite Pencils Resky Irfanita; Asnaeni Ansar; Ayu Hardianti Pratiwi; Jasruddin J; Subaer S
INDONESIAN JOURNAL OF APPLIED PHYSICS Vol 5, No 01 (2015): IJAP Volume 05 Issue 01 Year 2015
Publisher : Department of Physics, Sebelas Maret University

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.13057/ijap.v5i01.258

Abstract

The objective of this study is to investigate the effect of sintering temperature on the synthesis of SiC produced from rice husk ash (RHA) and 2B graphite pencils. The SiC was synthesized by using solid state reaction method sintered at temperatures of 750°C, 1000°C and 1200°C for 26 hours, 11.5 hours and 11.5 hours, respectively. The quantity and crystallinity level of SiC phase were measured by means of Rigaku MiniFlexII X-Ray Diffraction (XRD). The microstructure of SiC was examined by using Tescan Vega3SB Scanning Electron Microscopy (SEM). The XRD results showed that the concentration (wt%) of SiC phase increases with the increasing of sintering temperature. SEM results showed that the crystallinity level of SiC crystal is improving as the sintering temperature increases