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All Journal Communications in Science and Technology Chemistry Indonesian Journal of Chemical Research Indonesian Journal of Chemical Analysis (IJCA)
Ozi Adi Saputra, Ozi Adi
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Biochemistry, Genetics & Molecular Biology Chemical Engineering, Chemistry & Bioengineering Chemistry Engineering Environmental Science

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Silylated-montmorillonite as co-adsorbent of chitosan composites for methylene blue dye removal in aqueous solution Saputra, Ozi Adi; Kurnia; Pujiasih, Septi; Rizki, Vanani Nur; Nurhayati, Betty; Pramono, Edi; Purnawan, Candra
Communications in Science and Technology Vol 5 No 1 (2020)
Publisher : Komunitas Ilmuwan dan Profesional Muslim Indonesia

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (1045.12 KB) | DOI: 10.21924/cst.5.1.2020.182

Abstract

Industrialization plays important role in the economy of developing countries, including increasing community welfare. However, the presence of poorly industries waste disposal system has negative impact to the environment. Therefore, it is necessary to overcome this problem with low-cost technology, called adsorption. In this research, silylated-montmorillonite (sMMt) has been successfully prepared as supporting material for adsorption of methylene blue by chitosan. The sMMt was characterized by FTIR, XRD, and elemental mapping techniques. The chitosan/sMMt composites were prepared through dissolution-precipitation method and produced rod-like morphology as observed by SEM. The adsorption process was carried out in a batch method by studying the pH and the adsorption contact time. The adsorption kinetic mechanism of the chitosan/sMMt nanocomposite followed pseudo-second order rather than Lagergren model indicating chemisorption predominant. The addition of silylated-montmorillonite into chitosan enhanced the methylene blue dye removal performance, which evidenced by improving Qe values by 10% compared to chitosan.
Advances in Mesoporous Silica Nanoparticles: Synthesis, Characterization, and Biomedical Uses Saputra, Ozi Adi; Safitriono, Wahyu Nur; Istiqomah, Annisa; Kumalasari, Meiyanti Ratna; Irmawan, Muhammad; Wibowo, Fajar Rakhman
Indonesian Journal of Chemical Analysis (IJCA) Vol. 7 No. 2 (2024): Indonesian Journal of Chemical Analysis
Publisher : Universitas Islam Indonesia

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.20885/ijca.vol7.iss2.art9

Abstract

Mesoporous silica nanoparticles (MSNs) have drawn significant attention due to their exceptional properties and diverse range of applications, particularly in nanomedicine. The distinctive properties of MSNs, such as their high surface area, tunable pore size, and versatile surface chemistry, make them ideal candidates for various biomedical applications. This review aims to present a detailed understanding of MSNs, from synthesis and characterization to their versatile applications in biomedicine, highlighting their significant potential in advancing healthcare technologies. The synthesis methods for MSNs were comprehensively discussed, emphasizing the influence of parameters like solvent, base, alkoxysilane concentrations, and template surfactants on the size and shape of the nanostructures. Different types of MSNs, including MCM-41, SBA-15, KIT-6, and hollow MSNs, are discussed, along with their synthesis protocols and unique characteristics. The review also covers various spectroscopic techniques, such as XRD, XPS, FTIR, NMR, and fluorescence spectroscopy, which are crucial for characterizing MSNs. Furthermore, the biomedical applications of MSNs are highlighted, demonstrating their potential in drug delivery systems, imaging, and diagnostics. The review concludes with a discussion of the future perspectives and challenges in the field, providing insights into potential developments and the prospects for clinical translation.
Utilization of Lignin from Oil Palm Empty Fruit Bunches (OPEFB) for the Fabrication of Eco-Friendly Superhydrophobic Sponges Kumalasari, Meiyanti Ratna; Nainggolan, Yuni Damayanti; Nababan, Jesika; Isaura, Anastasya; Simbolon, Wenika; Togatorop, Hana Esrani; Saputra, Rizki Rachmad; Beladona, Siti Unvaresi Misonia; Saputra, Ozi Adi
Indonesian Journal of Chemical Research Vol 13 No 3 (2026): Edition for January 2026
Publisher : Jurusan Kimia, Fakultas Sains dan Teknologi, Universitas Pattimura

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.30598/ijcr.2026.13-mei

Abstract

The escalation of crude oil exploitation poses significant risks of leakage and oil spills in the oceans. Therefore, this research aims to synthesize superhydrophobic sponges utilizing lignin derived from Oil Palm Empty Fruit Bunch (OPEFB) waste. Lignin was isolated from OPEFB with the addition of 15% NaOH, followed by neutralization and purification using H₂SO₄, which yielded a recovery of 30.3%. Subsequently, melamine sponges were modified via a facile dip-coating technique using a mixture of lignin, Polydimethylsiloxane (PDMS), and (3-aminopropyl)triethoxysilane (APTES). The physicochemical properties and material performance were characterized using 1H-NMR, FTIR, and Water Contact Angle (WCA) measurements. 1H-NMR analysis confirmed the successful isolation of the lignin structure, while FTIR spectra verified the effective deposition of the silane-lignin layer on the sponge skeleton. Contact angle analysis results indicated a significant surface transformation, where the sponge shifted from a superhydrophilic nature 0° to a highly superhydrophobic state (170.91°). With such performance, this material holds great potential as an effective, eco-friendly adsorbent for oil spill remediation in aquatic environments.
Co-Authors Annisa Istiqomah, Annisa Candra Purnawan Edi Pramono Fajar Rakhman Wibowo Irmawan, Muhammad Isaura, Anastasya Kurnia Nababan, Jesika Nainggolan, Yuni Damayanti Nurhayati, Betty Pujiasih, Septi Rizki Rachmad Saputra Rizki, Vanani Nur Safitriono, Wahyu Nur Sari, Meiyanti Ratna Kumala Simbolon, Wenika Siti Unvaresi Misonia Beladona Togatorop, Hana Esrani