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Journal : Journal of Mechanical Engineering Science and Technology

Characterization of Hydroxyapatite Derived from Scallop Shell Waste Synthesized by Sonochemical Method with Different Temperature Calcination Pramono, Diki Dwi; Puspitasari, Poppy; Aminnudin, Aminnudin; Razak, Jeefferie Abd
Journal of Mechanical Engineering Science and Technology (JMEST) Vol 8, No 2 (2024)
Publisher : Universitas Negeri Malang

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.17977/um016v8i22024p400

Abstract

One common bio-ceramic material used in the biomedical industry is hydroxyapatite. Because of its crystallographic and molecular resemblance to the hard tissues of the human body, hydroxyapatite is thought to form. Scallop shells are one natural source of hydroxyapatite, which is high in calcium. This study examines how the calcination temperature affects the characteristics of hydroxyapatite made from leftover scallop shell. Hydroxyapatite was synthesized via the sonochemical method, with calcination conducted at temperatures of 900°C, 1000°C, and 1100°C. The hydroxyapatite that was prepared was assessed using X-ray diffraction (XRD) to determine the phase and crystallite size, Scanning Electron Microscopy (SEM) to conduct a morphological investigation, and Fourier Transform Infrared (FTIR) spectroscopy to conduct a functional group analysis. Phases resulting from varying calcination temperatures include hydroxyapatite and β-tricalcium phosphate. The crystallite size of hydroxyapatite enhanced with rising temperature. The morphology of hydroxyapatite exhibited agglomeration in all samples, with grain size escalating alongside the increase in calcination temperature. The functional groups generated under the three temperature fluctuations include O-H, P-O, PO43-, and O–P–O groups. The calcination temperature significantly influences the characteristics of produced hydroxyapatite and impacts its biocompatibility as a bone implant material.
Influence of Different Nanoparticles on Thermophysical Properties and Wear Resistance of Corn Oil-Based Cutting Fluid in MQL-CNC Milling Machining Habiby, M. Nuril Anwar; Puspitasari, Poppy; Aminnudin, Aminnudin; Pramono, Diki Dwi; Fikri, Ahmad Atif; Ghazali, Mariyam Jameelah
Journal of Mechanical Engineering Science and Technology (JMEST) Vol 9, No 1 (2025)
Publisher : Universitas Negeri Malang

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.17977/um016v9i12025p075

Abstract

Vegetable oil-based cutting fluids have emerged as a promising innovation in machining operations, supporting the advancement of sustainable and eco-friendly manufacturing practices. This study delves into the development of a biolubricant derived from corn oil, enriched with 0.15% mass fractions of various nanoparticles, including calcium carbonate (CaCO3), copper oxide (CuO), and multi-walled carbon nanotubes (MWCNT). These nano-cutting fluids were applied through the Minimum Quantity Lubrication (MQL) method during CNC milling of AISI 1045 steel. The investigation focused on evaluating thermophysical properties, including density, thermal conductivity, and dynamic viscosity, as well as tool wear performance. The results demonstrated that CuO nanoparticles yielded the highest density, while MWCNT exhibited superior thermal conductivity and viscosity. Among all samples, the fluid with MWCNT showed the most effective performance in minimizing tool wear. This study highlights the potential of nanoparticle-enriched vegetable-based cutting fluids as high-performance, environmentally responsible alternatives to conventional mineral oil-based lubricants, promoting greener machining in the manufacturing industry.