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All Journal Journal of Technomaterial Physics Jurnal Hibrul Ulama
Rahmayanti, Rika
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Religion Astronomy Civil Engineering, Building, Construction & Architecture Control & Systems Engineering Earth & Planetary Sciences Electrical & Electronics Engineering Energy Materials Science & Nanotechnology Physics

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Journal : Journal of Technomaterial Physics

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Synthesis of MnFe2O4 Nanoparticles as a Basic Material for Microwave Absorber Rahmayanti, Rika; Sudiati, Sudiati
Journal of Technomaterial Physics Vol. 4 No. 2 (2022): Journal of Technomaterial Physics
Publisher : Talenta Publisher

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.32734/jotp.v4i2.7870

Abstract

This work aimed to synthesize MnFe2O4 nanoparticles using the coprecipitation method. Manganese chloride dihydrate (MnCl2.4H2O) and iron sand from South Cianjur, Indonesia, were used as a precursor for MnFe2O4 nanoparticle synthesis. The iron sand elements and compounds were tested using X-Ray Fluorescence (XRF). MnFe2O4 nanoparticle was characterized using X-Ray Diffraction (XRD), Scanning Electron Microscope-Energy Dispersive X-Ray (SEM-EDX), and Vector Network Analyzer (VNA). The X-Ray Fluorescence test result showed that 70.54% of South Cianjur contained iron sand. The SEM test result showed that the nanoparticles have an average size of  73.75 nm with a round shape, which was attributed to the agglomeration process. The EDX test result showed that the synthesized nanoparticle contained only Mn, Fe, and O elements without contaminants. The XRD test result showed that the crystal phase of MnFe2O4 was formed with a crystal size of less than 27 nm. The largest reflection losses in the 11.5 - 12.5 GHz range were found in MnFe2O4 with 1:2 variation, i.e., 35.08 dB. This study found that adding iron sand increases MnFe2O4 microwave absorption.
Co-Authors armanila, Armanila Lubis, M. Syukri Azwar Sudiati Sudiati