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Reaktor
Published by Universitas Diponegoro
ISSN : 08520798     EISSN : 24075973     DOI : https://doi.org/10.14710/reaktor.xx.x.xx-xx
Core Subject : Science, Engineering,
Chemical Engineering, Chemistry & Bioengineering Control & Systems Engineering Energy Materials Science & Nanotechnology
Reaktor invites contributions of original and novel fundamental research. Reaktor publishes scientific study/ research papers, industrial problem solving related to Chemical Engineering field as well as review papers. The journal presents paper dealing with the topic related to Chemical Engineering including: Transport Phenomena and Chemical Engineering Operating Unit Chemical Reaction Technique, Chemical Kinetics, and Catalysis Designing, Modeling, and Process Optimization Energy and Conversion Technology Thermodynamics Process System Engineering and products Particulate and emulsion technologies Membrane Technology Material Development Food Technology and Bioprocess Waste Treatment Technology
Arjuna Subject : Teknik (semua kategori) - Teknik (Lain-Lain)
Articles 8 Documents
 1 
Search results for , issue "Volume 16 No.1 Maret 2016" : 8 Documents clear
Studi Kinetika Hidrolisis Tandan Kosong Kelapa Sawit (TKKS) Dengan Proses Fermentasi Padat Menggunakan Jamur Aspergillus niger Fitri Nur Kayati; Siti Syamsiah; Wahyudi Budi Sediawan; Sutijan Sutijan
Reaktor Volume 16 No.1 Maret 2016
Publisher : Dept. of Chemical Engineering, Diponegoro University

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (632.293 KB) | DOI: 10.14710/reaktor.16.1.1-8

Abstract

Kinetic of hydrolysis of Oil Palm Empty Fruit Bunch (OPEFB) by Solid State Fermentation using Aspergillus niger is studied. Hydrolysis of OPEFB to simple sugars using Aspergillus niger as raw material for other products is a potential alternative of bioconversion of lignocellulose. Formulating the kinetics of hydrolysis during solid substrate cultivication is useful for effective scale up of this technology as well as for better understanding of the process. The aim of this study was to develop kinetics models to describe the solid state fermentation of OPEFB. First, OPEFB were ground and classified by size using screen, with size range of : -30+40 mesh, -40+80 mesh and -80 mesh. It turned out that the proposed based on first order reaction kinetics model can quantitatively describe the process reasionally well. Furthermore, the values of the parameters involved in the kinetics models for each size for OPEFB particle were also obtained. The smaller the particle, the larger the hydrolysis reaction rate constant would be. It means that the rate of hydrolysis increases by the reduction of the particle size. Meanwhile, the sugars consumption rate constant decreases also by the reduction of OPEFB particle size. The highest concentration of simple sugars produced in this experiment was 7,847 g/L. Kata kunci : kinetic, Aspergillus niger,solid state fermentation, OPEFB, particle sizeHidrolisis tandan kosong kelapa sawit (TKKS) menjadi gula sederhana dengan menggunakan jamur Aspergillus niger merupakan alternatif biokonversi lignoselulosa yang potensial. Tujuan penelitian ini adalah mengembangkan model kinetika untuk mendiskripsikan proses fermentasi padat dengan bahan baku TKKS. Tahap pertama, TKKS digiling dan dikelompokkan sesuai ukuran dengan menggunakan ayakan,  dengan variasi ukuran antara -30+40 mesh, -40+80 mesh dan -80 mesh. Model kinetika yang telah disusun didasarkan pada reaksi orde satu. Model tersebut dapat menggambarkan secara kuantitatif proses fermentasi tersebut. Selain itu, nilai – nilai parameter dalam kinetika reaksi untuk setiap ukuran partikel juga akan diperoleh dari model tersebut. Semakin kecil ukuran partikel, semakin besar pula konstanta kecepatan reaksi hidrolisis. Sebaliknya konstanta konsumsi gula menurun seiring dengan penurunan ukuran partikel TKKS. Konsentrasi gula sederhana tertinggi yang dihasilkan dalam penelitian ini adalah sebesar 7,847% g/L.   Kata kunci: kinetika, Aspergillus niger, fermentasi padat, TKKS, ukuran partikel  
AMOKSIMASI SIKLOHEKSANON DENGAN KATALIS MoO3/TS-1 MENGGUNAKAN HIDROGEN PEROKSIDA SEBAGAI AGEN PENGOKSIDASI Rakhmadi Harsanto; Imroatul Qoniah; Didik Prasetyoko; Ratna Ediati
Reaktor Volume 16 No.1 Maret 2016
Publisher : Dept. of Chemical Engineering, Diponegoro University

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (503.686 KB) | DOI: 10.14710/reaktor.16.1.41-48

Abstract

AMMOXIMATION OF CYCLOHEXANONE OVER Mo-IMPREGNATED TITANIUM SILICALITE USING HYDROGEN PEROXIDE AS AN OXIDANT. Ammoximation of cyclohexanone reaction using 1% MoO3/TS-1 catalyst have been made with hydrogen peroxide as an oxidant. Reaction carried out with the batch method using methanol and acetonitrile as solvent. Reaction products analyzed using gas chromatography. The 1% MoO3/TS-1 catalyst shows the highest activity than the TS-1. The increased of 1% MoO3/TS-1 catalytic activity due to hydrophilicity properties higher than TS-1. Reaction using methanol shows the highest activity compared with reactions using acetonitrile. The optimum calcination temperature for 1% MoO3/TS-1 catalyst to gives the highest activity is 400 ºC.   Keywords: ammoximation of cyclohexanone; TS-1; 1% MoO3/ TS-1 Abstrak Amoksimasi sikloheksanon menggunakan katalis 1% MoO3/TS-1 telah dilakukan dengan menggunakan hidrogen peroksida sebagai agen pengoksidasi. Reaksi dilakukan dengan metode batch menggunakan pelarut metanol dan asetonitril. Produk reaksi dianalisis dengan kromatografi gas. Katalis 1% MoO3/TS-1 menunjukkan aktivitas katalitik yang lebih tinggi daripada katalis TS-1. Peningkatan aktivitas katalitik 1% MoO3/TS-1 dikarenakan sifat hidrofilisitasnya lebih tinggi dibandingkan TS-1. Reaksi katalisis yang menggunakan pelarut metanol memberikan aktivitas katalitik lebih tinggi daripada reaksi yang menggunakan pelarut asetonitril. Suhu kalsinasi paling optimum pada katalis 1% MoO3/TS-1 untuk memberikan aktivitas katalitik tertinggi adalah 400ºC. Kata kunci: amoksimasi sikloheksanon; TS-1; 1 % MoO3/ TS-1 
Front Matter Reaktor Vol 16 No. 1 Maret 2016 Widayat, W
Reaktor Volume 16 No.1 Maret 2016
Publisher : Dept. of Chemical Engineering, Diponegoro University

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (348.851 KB) | DOI: 10.14710/reaktor.16.1.i-v

Abstract

Karakterisasi Pengemas Kertas Aktif dengan Penambahan Oleoresin dari Ampas Pengepresan Rimpang Temulawak (Curcuma xanthorrhiza Roxb) Windi Atmaka; Godras Jati Manuhara; Noreka Destiana; K Kawiji; Lia Umi Khasanah; Rohula Utami
Reaktor Volume 16 No.1 Maret 2016
Publisher : Dept. of Chemical Engineering, Diponegoro University

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (317.644 KB) | DOI: 10.14710/reaktor.16.1.32-40

Abstract

CHARACTERIZATION OF ACTIVE PAPER PACKAGING INCOORPORATED WITH OLEORESIN EXTRACTED FROMSOLID WASTE OF PRESSED Curcuma xanthorrhiza Roxb ROOT. Curcuma xanthorrhiza Roxb is the medicinal plant that is widely extracted for instant drinks by herbal industry. In producing this instant Curcuma xanthorrhiza Roxb, solid waste is also produced and then thrown away. The waste actually still contain oleoresin as an active material. In this study, active paper packaging were incorporated with oleoresin extraxted from the waste at 0, 2, 4, and 6% (w/w) level. The aims of this study was to determine the effect of oleoresin concentration on physical, chemical, and antimicrobial activity characteristics of active paper packaging. Based on this research, the incorporation of the oleoresin decreased moisture content, tensile strength, folding endurance and but increased antimicrobial activity of Aspergillus niger.   Keywords: active paper packaging; curcuma xanthorrhiza Roxb.; oleoresin; residue Abstrak Temulawak (Curcuma xanthorrhiza Roxb) adalah tanaman herbal yang lazim diolah industri herbal menjadi minuman instan. Produksi minuman instan temulawak menghasilkan limbah padat berupa ampas yang tidak dimanfaatkan dan biasanya hanya dibuang begitu saja. Padahal ampas temulawak masih mengandung oleoresin yang berperan sebagai senyawa aktif. Penelitian kertas aktif dilakukan dengan menambahkan oleoresin ampas temulawak dengan konsentrasi 0, 2, 4, dan 6% (b/b). Tujuan dari penelitian ini adalah untuk mengetahui pengaruh penambahan oleoresin ampas temulawak terhadap karakter fisikokimia, aktivitas antimikroba dan sensoris pengemas kertas aktif. Dari penelitian ini menunjukkan bahwa penambahan oleoresin ampas temulawak menurunkan kadar air, nilai ketahanan tarik, ketahanan lipat, dan karakter sensori (warna, tekstur dan overall), namun meningkatkan aktivitas antimikroba terhadap Aspergillus niger. Kata kunci: pengemas kertas aktif; temulawak; oleoresin; ampas  
Back Matter Reaktor Vol 16 No. 1 Maret 2016 Widayat, W
Reaktor Volume 16 No.1 Maret 2016
Publisher : Dept. of Chemical Engineering, Diponegoro University

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (548.125 KB) | DOI: 10.14710/reaktor.16.1.%p

Abstract

MODIFIED STARCH OF AMORPHOPHALLUSCAMPANULATUS AS A NOVEL ADSORBENT FOR WATERADSORPTION Ajeng Yulianti Dwi Lestari; Mohamad Djaeni; Ahmad M Fuadi
Reaktor Volume 16 No.1 Maret 2016
Publisher : Dept. of Chemical Engineering, Diponegoro University

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (751.28 KB) | DOI: 10.14710/reaktor.16.1.9-22

Abstract

A novel adsorbent manufactured from Amorphophallus campanulatus (Porang or Suweg or Elephant Foot Yam or Foot Yam) starch and employed to adsorb water from wet air. The experiment focused on the adding of sodium hydroxide in various concentration of sodium hydroxide (10:1, 10:2.5, 10:5 10:10, 10:20, 10:30, 10:40 mmol/mmol) and its effect to form the new adsorbents shape and chemical bonds. Experimental data were also fitted with several models of isotherm adsorption and adsorption kinetics.Analysis with FTIR and SEM showed that sampel C7 (modified starch with NaOH 40:10 mol) is the adsorbent that could adsorp more water from air and also proofed that foot yam starch can be feasible to be synthesize as an adsorbent for water adsorption.The results also showed that this novel adsorbent fitted with pseudo second order kinetic model and Freundlich isotherm model with maximum adsorption capacity calculated 2.006 g water/g adsorbent.   Keywords: elephant foot yam; starch; sodium hydroxide; water adsorption Abstrak PATI UMBI AMORPHOPHALLUS CAMPANULATUS TERMODIFIKASI SEBAGAI ADSORBEN BARU UNTUK ADSORPSI AIR.Adsorben baru berhasil dibentuk dari pati umbi Amorphophallus campanulatus (Porang atau Suweg) yang kemudian digunakan untuk mengadsorp air dari udara lembab. Penelitian berfokus kepada pengaruh penambahan variasi konsentrasi dari natrium hidroksida (NaOH) (10:1, 10:2,5, 10:5, 10:10, 10:20, 10:30, 10:40 mmol pati/mmol NaOH) atas pembentukan morfologi serta ikatan kimia dari adsorben baru. Data eksperimen kemudian dicocokkan dengan beberapa model isoterm serta kinetika adsorpsi. Analisis dengan menggunakan FTIR dan SEM menunjukkan bahwa sampel C7 (perbandingan pati modifikasi dengan NaOH 40:10 mol) adalah adsorben yang dapat menjerab air lebih banyak dibandingkan dengan adsorben yang lainnya. Hal ini menunjukkan bahwa adsorben dapat menjerab air dari udara lembab dan membuktikan bahwa umbi porang ini layak untuk dijadikan sebuah sumber adsorben alami yang baru. Hasil juga menunjukkan bahwa data eksperimen menunjukkan kesesuaian dengan model kinetika semu orde dua dan model isoterm Freundlich dengan kapasitas adsorpsi maksimal 2,006 g air/g adsorben Kata kunci: umbi Suweg; pati; NaOH; adsorpsi air
ANALISA ENERGI DAN EKSERGI PADA PENGERINGAN TEPUNG TAPIOKA MENGGUNAKAN PENGERING KONTINYU UNGGUN FLUIDISASI GETAR Suherman Suherman; Rona Trisnaningtyas
Reaktor Volume 16 No.1 Maret 2016
Publisher : Dept. of Chemical Engineering, Diponegoro University

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (760.418 KB) | DOI: 10.14710/reaktor.16.1.24-31

Abstract

Energy and exergy analysis of cassava starch drying in continuous vibrated fluidized bed dryer were carried out to assess the performance of the system in terms of energy utilization ratio, energy efficiency, exergy inflow and outflow, exergy loss, and exergetic efficiency. The results showed cassava starch has starch content 87%, degree of whiteness 95%, negative fiber content, sperichal granula with average diameter12.32 μm, orthorhombic crystal structure and crystal size 47.467 nm . Energy utilization and energy utilization ratio increased from 0.08 to 0.20 J/s and 0.35 to 0.4 as the drying temperature  increased from 50 to 70 oC. Energy efficiency increased from 13.80 % to 23.31 %, while exergy inflow, outflow, and losses increased from 4.701 to 14.678, 2.277 to 6.344, and 2.424 to 8.334 J/s respectively in the above temperature range. Exergetic efficiency decreased with increase in drying air temperature, while exergetic improvement potential increased with increased drying air temperature. Keywords: Cassava starch, continuous drying, energy and exergy analysis, vibrated fluidized bed Abstrak Analisis energi dan eksergi pengeringan pati tapioka menggunakan pengering kontinu unggun fluidisasi getar, telah dilakukan untuk menilai kinerja sistem dalam bentuk utilisasi energi, efisiensi energi, eksergi masuk dan keluar, eksergi hilang dan efisiensi eksergi. Hasil analisis pati memiliki kandungan starch 87%, tingkat keputihan 95%, kandungan serat negatif, bentuk partikel granular spherical dengan diameter 12,32 μm, struktur kristal orthorhombic dan ukuran kristal sebesar 47,467 nm. Peningkatan suhu pengering dari 50 menjadi 70 0C akan meningkatkan utilisasi energi dan rasio utilisasi energi dari 0,08 menjadi 0,20 J/s dan 0,35 menjadi 0,4. Efisiensi energi meningkat dari 13,80% hingga 23,31%, sedangkan eksergi masuk dan keluar, eksergi hilang meningkat dari 4,701 menjadi 14,678, 2,277 menjadi 6,344, dan 2,424 menjadi 8,334 J/s. Efisiensi eksergi menurun dengan naiknya suhu sedangkan potensi pengembangan eksergi meningkat dengan naiknya suhu. Kata kunci:. Analisis energi dan eksergi, pati tapioka, pengeringan kontinu, unggun fluidisasi getar
Pemanfaatan Limbah Pretreatment Dalam Produksi Bioetanol Dari Lignoselulosa Untuk Me-Recovery Fine Chemicals Dengan Proses Pirolisa Dieni Mansur; Sabar Pangihutan Simanungkalit; Nino Rinaldi
Reaktor Volume 16 No.1 Maret 2016
Publisher : Dept. of Chemical Engineering, Diponegoro University

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (25.711 KB) | DOI: 10.14710/reaktor.16.1.17-23

Abstract

UTILIZATION OF PRETREATMENT WASTE DURING PRODUCTION OF BIOETHANOL FROM LIGNOCELLULOSIC MATERIALS FOR RECOVERY FINE CHEMICALS BY PYROLYSIS. In production of second generation bioethanol by utilizing lignocelluloses as raw material, black liquor was produced from its pretreatment process. As waste of pretreatment process, the black liquor was rich in lignin. Therefore, the black liquor has potential to be proceeded to produce fine chemicals. In this study, black liquor powder was pyrolyzed at 450-600°C for 15 minutes using a fixed bed type reactor. Pyrolysis process produced four types of products thal called as liquid tar, heavy tar, char and gas. Liquid tar was condensable volatile product in condenser and uncondensable ones was called gas. Heavy tar was heavier volatile product that stick to reactor wall on bed of feed and unable to enter a condenser. Whereas, char was deposited carbon left in the pyrolizer. The liquid tar consisted of several chemical compounds that classified into groups of chemicals based on similar functional groups. In a range of temperatures process, higher yield of liquid tar was produced after treated at 550°C compared to other conditions. The main chemical compounds in the liquid tar were phenol, alcohols and alkyl phenols that mainly predicted derived from decomposition of lignin and represented as the fine chemicals from black liquor powder.  Keywords: bioethanol; black liquor powder; fine chemicals; lignocelluloses; pyrolysis Abstrak Dalam produksi bioetanol generasi kedua dengan memanfaatkan lignocellulosa sebagai bahan baku, akan menghasilkan black liquor pada saat proses pretreatment. Sebagai limbah proses pretreatment, black liquor ini kaya akan lignin. Oleh karena itu, black liquor berpotensi diolah untuk menghasilkan fine chemicals. Pada penelitian ini, bubuk black liquor diproses secara pirolisa pada suhu 450-600°C selama 15 menit menggunakan reaktor jenis fixed bed. Proses pirolisa menghasilkan produk yang dapat digolongkan menjadi empat jenis yaitu liquid tar, heavy tar, char dan gas. Liquid tar merupakan volatile product yang terkondensasi di kondensor dan yang tidak dapat terkondensasi disebut sebagai gas. Heavy tar adalah volatile product yang lebih berat dan terlebih dahulu menempel di dinding reaktor pirolisa di atas bed umpan dan tidak sampai masuk ke kondensor. Sementara char adalah deposit karbon yang tertinggal di dalam reaktor pirolisa. Liquid tar tersusun oleh berbagai macam senyawa kimia yang bisa dikelompokkan menjadi grup-grup berdasarkan kesamaan gugus fungsi. Dari rentang suhu proses tersebut, liquid tar paling banyak dihasilkan pada suhu 550°C. Liquid tar tersebut banyak mengandung fenol, alkohol dan alkil fenol yang diprediksi umumnya berasal dari dekomposisi lignin dan menjadi fine chemicals yang dapat di-recovery dari bubuk black liquor Kata kunci: bioetanol; bubuk black liquor; fine chemicals; lignoselulosa; pirolisa.

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