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INDONESIA
Seminar Nasional Teknik Kimia Kejuangan
Published by Universitas Pembangunan Nasional Veteran Yogyakarta
ISSN : -     EISSN : -     DOI : -
Core Subject : Science, Social, Engineering,
Biochemistry, Genetics & Molecular Biology Chemical Engineering, Chemistry & Bioengineering Engineering Environmental Science
Prosiding Seminar Nasional Teknik Kimia Kejuangan adalah media online dari makalah yang telah diseminarkan pada acara Seminar Nasional Teknik Kimia “Kejuangan” (SNTKK). SNTKK merupakan agenda tahunan yang diselenggarakan oleh Program Studi Teknik Kimia FTI UPN ”Veteran” Yogyakarta. Seminar ini merupakan sarana komunikasi bagi para peneliti dari perguruan tinggi, institusi pendidikan, serta lembaga penelitian maupun industri, dalam mengembangkan teknologi kimia untuk pengolahan sumber daya alam Indonesia.
Arjuna Subject : -
Articles 588 Documents
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The Effect of Complexity of Fuel Oil Composition Compounds on Desulphurization Degrees in Oxidative Desulphurization Processes Rofii, Mochammad; Nasikin, Mohammad
Prosiding Seminar Nasional Teknik Kimia "Kejuangan" 2023: PROSIDING SNTKK 2023
Publisher : Seminar Nasional Teknik Kimia "Kejuangan"

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Abstract

Oxidative Desulfurization is an alternative process to reduce sulfur content in fuel. ODS is an oxidation reaction of sulfur compounds in fuel, which contains various hydrocarbon compounds, using an oxidizing agent with the help of a catalyst. The polarity of fuel, sulfur compounds and catalysts is a critical success factor for ODS. This study aims to determine the effect of the complexity of the model fuel used in the ODS process on the degree of sulfur reduction. The complexity variable is considered by polarity, which is determined based on the dielectric constant of the compound using the mixed concentration average of the dielectric constant of the pure compound. The model fuel used in this study is a mixture of hydrocarbon compounds having 6 C atoms in the form of n-hexane, cyclohexane, and benzene. Dibenzothiophena is used as a representative of sulfur compounds with an initial concentration of 300 ppm in each sample. The independent variables that were varied were the composition of the model fuel and the ODS reaction time. Sulfur content in model fuel before and after ODS was analyzed using UV-Vis. Meanwhile, the dielectric constants of fuel and catalyst are determined using empirical equations. The results showed that the polarity of the model fuel changed depending on the composition of the constituent compounds. The ODS process resulted a decrease in DBT levels as a function of increasing the time reaction of ODS. Changes in the polarity of the model fuel solvent give different desulphurization results. The highest degree of desulphurization was obtained at 21% with the use of model fuel with a catalyst which had a dielectrict constant of 1.995.
Preparasi Katalisator Berbasis Biochar dari Ampas Buah Merah untuk Reaksi Transesterifikasi Minyak Jelantah Rahmah, Puspa; Yuliansyah, Ahmad Tawfiequrrahman; Wintoko, Joko
Prosiding Seminar Nasional Teknik Kimia "Kejuangan" 2023: PROSIDING SNTKK 2023
Publisher : Seminar Nasional Teknik Kimia "Kejuangan"

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Abstract

Biodiesel can be produced from plant and animal oils by transesterification reaction using homogeneous or heterogeneous catalysts. In this study, we prepare a biochar-based catalyst, as a heterogeneous catalyst, for transesterification of used cooking oil. The biochar was made by the pyrolysis of the solid waste from the oil extraction of Papuan red fruit (Pandanus conoideus). After the pyrolysis, the solid was immersed in KOH solution to provide the kalium in the produced biochar. The biochar was then sulfonated by H2SO4 5M for 15h at 120°C. Afterwards, the catalysts were characterized by BET for surface area measurement, FTIR for functional groups on the catalyst surface determination and XRD for successive crystallography characterization. The catalytic performance was studied by conducting transesterification of used cooking oil using methanol with the prepared biochar-based catalysts. The transesterification optimum conditions were found to be oil to methanol molar ratio of 1:15, temperature of 60°C, reaction time of 2 hours and the catalyst amount of 3% of the oil weight. Furthermore, the highest biodiesel yield was obtained by the catalyst prepared from biochar that was sulfonated with 5M H2SO4 solution
Sintesis Asil Gliserol Melalui Reaksi Esterifikasi Asam Oleat dengan Gliserol Husada, Caesar Purnama; Sulistyo, Hary; Sediawan, Wahyudi Budi
Prosiding Seminar Nasional Teknik Kimia "Kejuangan" 2023: PROSIDING SNTKK 2023
Publisher : Seminar Nasional Teknik Kimia "Kejuangan"

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Abstract

Acyl glycerol derivatives from oleic acid, especially monoacylglycerol (MAG) and diacylglycerol (DAG), are products that is widely used in the food, lubricant, and cosmetic industries. Acyl glycerol can be obtained through esterification reaction of glycerol with fatty acids.  This study aims to determine the effect of temperature on the conversion and amount of acyl glycerol produced. This research was conducted using a batch system with temperature variations of 80°C, 100°C, and 120°C with HCl 1%wt as catalyst and 1:1 reactant mole ratio (glycerol: oleic acid) for 2 hours reaction time. Samples were taken every 10 minutes, then the samples were analyzed using Thin Layer Chromatography (TLC) to determine the fraction of the product produced. The experimental results showed that increasing the temperature will produce higher conversions and acyl glycerols. The highest conversion of oleic acid occurred at 120°C (43.016%), with mole percentage of 1,796% monoacylglycerol (MAG), 3,820% diacylglycerol (DAG), and 5,813% triacylglycerol (TAG).
Sintesis Surfaktan Non-ionik Berbasis Asam Palmitat Melalui Reaksi Esterifikasi dengan Gliserol Purbaningdyah, Emma; Sulistyo, Hary; Sediawan, Wahyudi Budi
Prosiding Seminar Nasional Teknik Kimia "Kejuangan" 2023: PROSIDING SNTKK 2023
Publisher : Seminar Nasional Teknik Kimia "Kejuangan"

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Abstract

Esterification of glycerol using the fatty acids is one of methods that is widely used in the conversion of glycerol to synthesize products containing monoacylglycerol (MAG) and diacylglycerol (DAG). Among the various types of surfactants, monoacylglycerol (MAG) and diacylglycerol (DAG) are the most widely used of non-ionic surfactants in many industries such as food, pharmacy and cosmetic. This study aims to determine the effect of temperature on the conversion of palmitic acid and the concentration fraction of products. This research was conducted in a batch system with the temperature variations of 80°C, 100°C and 120°C; using 1% HCl catalyst concentration of palmitic acid mass, and reactant mole ratio of 1:1 (glycerol: palmitic acid). Samples were taken every 10 min during 120 min of reaction, to be analyzed by Thin Layer Chromatography (TLC) to determine the concentration fraction of products. The experimental results showed that increasing temperature enhanced the products formation, thus, increased the fraction concentration of products. However, the highest conversion of palmitic acid (80.14%) was obtained at 120°C, with concentration fraction of 1.67% monoacylglycerol (MAG), 10.96% diacylglycerol (DAG) and 6.01% triacylglycerol (TAG).
Potensi Mikroorganisme Indigen Perairan Teluk Lampung sebagai Pendegradasi Masker Sekali Pakai (Disposable Face Mask) Deviany, Deviany; Achmad, Feerzet; Purwanti, Millennia Rischa; Yudhanti, Tri Febri
Prosiding Seminar Nasional Teknik Kimia "Kejuangan" 2023: PROSIDING SNTKK 2023
Publisher : Seminar Nasional Teknik Kimia "Kejuangan"

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Abstract

To prevent the transmission of COVID-19, the World Health Organization recommends the implementation of health protocols including using disposable masks. The use of disposable face masks has an impact on the emergence of mask waste in aquatic environments which results in pollution of water sources by microfibers. Degradation by indigenous microorganisms can be one of the solutions for handling waste that is environmentally friendly and cost effective. In this study, bacteria were isolated from the coast of Lampung Bay which was polluted with plastic waste and masks. Bacterial isolates were characterized by morphological and biochemical tests before the selected one being used for degradation. After seven days of incubation, gravimetric analysis showed that the mask pieces increased in weight when compared to the control. However, the degradation process can be shown by the results of Scanning Electron Microscope (SEM) analysis which shows damage in the form of holes on the surface of the mask when compared to the new mask and the control. SEM images also showed the presence of bacterial biomass remnants attached to the surface of the mask. Based on the results of this study, Lampung Bay indigenous microorganism isolate showed potential as a degrader of disposable face masks.
Degradasi Masker Sekali Pakai dengan Vermiremediasi dan Penambahan Isolat Bakteri Teluk Lampung Deviany, Deviany; Achmad, Feerzet; Rosafira, Adela; Aini, Syarifah
Prosiding Seminar Nasional Teknik Kimia "Kejuangan" 2023: PROSIDING SNTKK 2023
Publisher : Seminar Nasional Teknik Kimia "Kejuangan"

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Abstract

The use of disposable face masks during the Covid-19 pandemic has resulted in the emergence of mask waste polluting aquatic environments due to poor management. This waste will decompose into microfibers which accumulate in aquatic organisms. The combination of vermiremediation with the addition of degrading microorganisms can be one of the solutions for treating disposable mask waste. In this study, Eudrilus eugeniae, an earthworm species, was used in vermiremediation with variations in the treatment by adding indigenous bacterial isolate from the waters of Lampung Bay which has been proven able to degrade disposable masks. The results showed that the vermiremediation technique can be used to degrade disposable masks, indicated by a decrease in mask weight after incubation for two months in the amount of 0.03 grams and 0.05 grams for the treatment with the Eudrilus eugeniae and a combination of bacterial isolate respectively against the initial weight. Lampung Bay indigenous bacterial isolate helped accelerate the mask degradation process in the combined vermiremediation technique. The carbon, nitrogen, phosphorus, and potassium contents of the compost produced by the vermiremediation process have met the SNI for compost from domestic organic waste.
Biodegradable Wet Wipes dari Sabut Kelapa Sawit (Palm Fiber) dengan Ekstrak Flavonoid Daun Kelapa Sawit Sebagai Bahan Antibakteri Fadilah, Fadilah; Ningtyas, Divanda Sekar Rahayu; Dewi, Audrey Vista Candra; Krisnawati, Anita Budi; Putra, Reyza Fachrezy
Prosiding Seminar Nasional Teknik Kimia "Kejuangan" 2023: PROSIDING SNTKK 2023
Publisher : Seminar Nasional Teknik Kimia "Kejuangan"

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Abstract

The wet tissue currently circulating in the market is made of synthetic fibers consisting of 30% viscose fibers and 70% polyester fibers, and 90% of the wet tissue contains plastic. Indonesia's palm oil industry grows annually, however. Palm fiber waste has high cellulose, useful as wet tissue raw material substitute. This study used flavonoids from palm leaves as an antibacterial material to create biodegradable wet wipes from palm fiber and evaluate their antibacterial and antiseptic effectiveness. The best characteristics of biodegradable wet wipes are obtained with a composition of 91.5% (w/w) palm coconut fiber cellulose, and a ratio (w/w) of PVA:tapioca:chitosan at every 10 mL of used VCO of 2:3:6 (1.5%:2.25%:4.5%) with variations in pulp bleaching and the method of applying the binder solution by being spread onto semi-dry tissue paper. The evaluation of wet tissue includes tests for tensile strength, color, biodegradability, phytochemical analysis, antibacterial testing, antiseptic testing, irritation testing, and pH testing. The test results showed that biodegradable wet wipes made of palm coconut fiber and flavonoid extract from palm coconut leaf at concentrations of 10%, 15%, and 20%, which have been adjusted to SNI 8526:2018 standard, have bacterial reduction effectiveness of 68.09%, 79.06%, and 89.94%, respectively.
Pengaruh Morfologi Anionik Flokulan terhadap Performa Koagulasi Nira PG. Krembong PTPN X Taji, Lulu Sekar; Ardiansyah, Erlangga; Ningrum, Eva Oktavia
Prosiding Seminar Nasional Teknik Kimia "Kejuangan" 2023: PROSIDING SNTKK 2023
Publisher : Seminar Nasional Teknik Kimia "Kejuangan"

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Abstract

The problem that occurs in Indonesia is the consumption of sugar that is greater than its production which causes the inability of the sugar industry to supply the demand of all consumers. One of the problems that occured is caused by the large number of raw materials that are still imported, including the flocculant used in this case, namely Anionic Polyacrylamide flocculant. Anionic Polyacrylamide (APAM) was first developed using an alkaline hydrolysis process. Until now, APAM manufacturing technology has undergone many developments. However, there are only few research conducted on Anionic poly flocculant (SA-co-A) regarding the influence of polymer properties and the efficiency of its use in the sugar refining process, therefore research was conducted on the influence of Anionic flocculant morphology on the coagulation-flocculation performance of sap at Krembong PTPN X sugar factory to reduce costs in the sugar production process. In this study, poly (SA-co-A) synthesis was carried out as a flocculant to be used in the sugar refining process. The steps used are adding acrylic acid, acrylamide and sodium carbonate which are then added with the NaOH solution. The next step is the synthesis of poly(SA-co-A), the synthesis process is carried out with a nitrogen atmosphere for 3 hours which has previously been added with ammonium persulfate. This study was conducted on the concentration ratio between acrylic acid and acrylamide which uses 40:60, 50:50, 60:40 variables. The resulting flocculants will be tested for flocculant FTIR test, flocculant SEM test, NMR test, settling speed test, mud volume test, pH test, TDS test, turbidity test on sugar’s sap to determine the effect of adding the flocculant. Based on the research that has been done, optimal flocculant performance was obtained, namely on the variable of poly(SA-co-A) 60:40 dose 2.5 ppm, whereas the results are almost equal or even better than commercial flocculant performance. With the removal percentage for the speed of precipitation and the volume of precipitation increases up to 4.5 and 2 times. Then for TDS and turbidity dropped to 14% and 86%.
Sintesis dan Karakterisasi Hidroksiapatit Cangkang Rajungan dengan Variasi Suhu Kalsinasi dan Konsentasi KH2PO4 menggunakan Metode Presipitasi Sebagai Sediaan Biomaterial Implan Tulang Romadhona, Novelia Gita; Syafira, Nesha Permata; Gumelar, Tobing; Rizqiyah, Vita Fatichah; Ningrum, Eva Oktavia
Prosiding Seminar Nasional Teknik Kimia "Kejuangan" 2023: PROSIDING SNTKK 2023
Publisher : Seminar Nasional Teknik Kimia "Kejuangan"

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Abstract

Bone implants are mostly made of non-degradable metal materials that are toxic to the body. An alternative biodegradable material being developed is Poly-L-Lactic Acid (PLLA). However, PLLA has the disadvantage of being incompatible with bone tissue. So, materials that are biodegradable and biocompatible are needed, such as hydroxyapatite, which has similarities with the minerals in bone and teeth, it suitable as an alternative biomaterial in the biomedical. This research aims to determine the effect of synthesis conditions, with calcination temperature (850, 900, 950, 1000°C) and KH2PO4 concentration (0.25, 0.5, 0.75, 1 M), on the production of hydroxyapatite using raw materials from local blue crab shells, in terms of calcium content, functional group presence, and conformity of hydroxyapatite peaks with JCPDS 09-0432. The synthesized product was characterized using XRF, which showed a relatively high calcium in crab shells of 94.89% at calcination temperature 850°C. The FTIR test results after the mixing of KH2PO4 with CaO showed the formation of hydroxyapatite functional groups, namely OH- and PO43-, in all variables. The XRD test results showed that at 850°C and KH2PO4 concentration of 0.75 M the main peak of hydroxyapatite was closest to JCPDS 09-0432, at a diffraction angle (2θ) of 31.7634.
Sintesis Nanohidroksiapatit Berbahan Cangkang Keong Sawah (Pila ampullacea) dengan Variasi Konsentrasi H3PO4 Menggunakan Metode Ultrasound Assisted Precipitation Karisma, Achmad Dwitama; Kriswanto, Oktavianus Nugroho; Rachmaningtrias, Renda
Prosiding Seminar Nasional Teknik Kimia "Kejuangan" 2023: PROSIDING SNTKK 2023
Publisher : Seminar Nasional Teknik Kimia "Kejuangan"

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Abstract

Nanohydroxyapatite with the molecular formula Ca10(PO4)6(OH)2 is a calcium phosphate compound that is most widely used in biomedical applications such as bone and dental implants due to its high biocompatibility. The synthesis of nanohydroxyapatite can be carried out using CaCO3 rich materials such rice field snail shell (Pila ampullacea) with a composition of 93.4% CaCO3. The nanohydroxyapatite synthesis method used is Ultrasound Assisted Precipitation. Calcium obtained from the natural material of rice field snail shell (Pila ampullacea) was reacted with H3PO4 precursor at variable 0.3; 0.5; 0.8; 1; 1.3 M until a precipitate of nanohydroxyapatite particles was formed. To determine the effect of H3PO4 concentration, analysis was conducted on the characteristics of the synthesized nanohydroxyapatite. The SEM-EDX analysis revealed a Ca/P ratio of 1.59-1.72 with spherical particle morphology. The FTIR analysis indicated the presence of hydroxyapatite in the sample through the P-O and O-H functional groups.

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