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Alizar, Alizar
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Journal : Indonesian Journal of Chemical Science and Technology

 1 
Characterization of Molecularly Imprinted Polymers (MIPs) as Cholesterol-Absorbing Materials Nadia, Nadia; Kurniawati, Desy; Alizar, Alizar
Indonesian Journal of Chemical Science and Technology (IJCST) Vol 6, No 2 (2023): JULY 2023
Publisher : Universitas Negeri Medan

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.24114/ijcst.v6i2.49367

Abstract

Molecularly Imprinted Polymer (MIP) membranes as cholesterol absorbers have been successfully synthesized. MIP membranes can absorb cholesterol molecules because they have cavite (pores) and active groups that are selective and sensitive to cholesterol molecules. MIP membranes are synthesized from butyl acrylate monomers, cross-linkers, ethylene glycol dimethacrilate (EGDMA), initiators of 2- 2-dimethoxy-2-phenylacetophenone (DMPP, sodium dodecyl sulfate (SDS) as surfactants, and cholesterol as templates. MIP membranes are synthesized using photopolymerization irradiated with UV light. The results obtained in the form of powder solids can be characterized using UV-Vis spectrophotometry. The results obtained by UV-Vis spectrophotometry showed that the MIP membrane prepared a standard curve with a linear regression equation y = 0.0054x-0.007 with a value of R2 = 0.9982. This suggests that MIP membranes are selective and sensitive to analytes. At optimum absorption of the MIP-cholesterol membrane can absorb cholesterol molecules in the amount of 0.020 grams of cholesterol composition within 20 minutes
Effect Type of Desorption Eluent and Concentration in Desorption of Zn2+ Cation from Sulfonate Modified Silica Gel-GPTMS (Glycydoxypropyltrimethoxysilane) Adsorbent Hafis, Muhamad; Oktavia, Budhi; Alizar, Alizar; Warda Ningsih, Sherly Kasuma
Indonesian Journal of Chemical Science and Technology (IJCST) Vol 7, No 2 (2024): JULY 2024
Publisher : Universitas Negeri Medan

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.24114/ijcst.v7i2.62256

Abstract

Silica has silanol groups contained in it which have low binding ability because it has low acidity, resulting in low absorption effectiveness on silica. In order to improve the properties and to expand the field of utilization, a modification process is carried out on silica gel using GPTMS bridging compounds and sulfonate salts as modifiers. The study explains that CaCl2.2H2O with a desorption percent of 97.25% has a greater ability than NaCl which is only 83.93% in the desorption of Zn2+ cations. The study also explains that the optimum concentration of CaCl2.2H2O eluent in the desorption of Zn2+ cations is at 1mmol/L where the desorption yield is 93.74%.
Characterization of Silica Nanoparticles from Pumice as an Aerogel Adsorbent Hidayah, Rahma; Kurniawati, Desy; Alizar, Alizar
Indonesian Journal of Chemical Science and Technology (IJCST) Vol 7, No 1 (2024): JANUARY 2024
Publisher : Universitas Negeri Medan

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.24114/ijcst.v7i1.56435

Abstract

Pumice is often found around the banks of rivers, this stone is a type of igneous rock formed from volcanic eruptions. One of the compounds contained in pumice is silica. Therefore, the synthesis of silica nanoparticles from pumice using the sol gel method was used because it is simpler and more efficient in terms of cost and processing time. the initial step was by reacting pumice powder and NaOH at 70°C - 80°C then synthesized by adding 2M HCI to form a gel or white precipitate, soaking in ethanol, teos, hexane solutions was then synthesized to become an aerogel. Silica synthesis results into silica aerogels were characterized by FTIR and XRF. From FTIR silanol and siloxane functional groups were found, and the SiO2 composition increased to 93,299% after synthesis.
Characterization of Silica Nanoparticles from Pumice as an Aerogel Adsorbent Hidayah, Rahma; Kurniawati, Desy; Alizar, Alizar
Indonesian Journal of Chemical Science and Technology (IJCST) Vol 6, No 2 (2023): JULY 2023
Publisher : Universitas Negeri Medan

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.24114/ijcst.v6i2.49368

Abstract

Pumice is often found around the banks of rivers, this stone is a type of igneous rock formed from volcanic eruptions. One of the compounds contained in pumice is silica. Therefore, the synthesis of silica nanoparticles from pumice using the sol gel method was used because it is simpler and more efficient in terms of cost and processing time. the initial step was by reacting pumice powder and NaOH at 70°C - 80°C then synthesized by adding 2M HCI to form a gel or white precipitate, soaking in ethanol, teos, hexane solutions was then synthesized to become an aerogel. Silica synthesis results into silica aerogels were characterized by FTIR and XRF. From FTIR silanol and siloxane functional groups were found, and the SiO2 composition increased to 93,299% after synthesis.
Co-Authors Abdillah, Aditya Nur Adam, Wahyu Adi Saputra, Rifaldi Andreas Andreas AYU LESTARI Benti Etika, Sri Berlian, Anggananda Budhi Oktavia Desy Kurniawati Dewi, Marysca Shintya Edi Nasra Fatma, Winda Faulina Fato, Adri Hafifah, Haifa Hafis, Muhamad Hidayah, Rahma Indang Dewata Ira Damayanti, Ira Iryani Iryani Komarudin Komarudin Lestari, Kardina Liza, Yulia Mona Lubis, Andika Marlini, Rahmida Md Isa, Illyas Mulia, Melindra Nadia Nadia Pandiangan, Ronaldo Mulyadi Parbuntari, Hesty Pratama, Aditya Eka Putra, Ananda Putra, Anggih Permata Putri Rinjani, Mitna Sekar Putri, Reza Athia Romy Dwipa Yamesa Away Rosmiyani, Tia Safitri, Tofana Eka Saputra, Yusuf Adi Sari, Trisna Kumala Sherly Kasuma Warda Ningsih Trisna Kumala Sari Utama, Rodika Yerimadesi Yerimadesi Yulkifli Yulkifli Yusri, Wilda Triputri Zonalia Fitriza