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Journal : FLUIDA

Pemanfaatan Bioadsorben Dari Sekam Padi Untuk Mendegradasi Logam Cu Pada Minyak Pelumas Bekas Jusuf Pratama; Arlin Dini Anindya; Yurike Luckita; Nabila Nur Latiefa; Alfiana Adhitasari
Fluida Vol 15 No 1 (2022): FLUIDA
Publisher : Jurusan Teknik Kimia, Politeknik Negeri Bandung

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.35313/fluida.v15i1.3611

Abstract

Penggunaan minyak pelumas dalam industri sebagai bahan untuk melindungi mesin dari gesekan dengan komponen lain menghasilkan limbah yang sifatnya mudah terbakar dan meledak apabila salah dalam pengelolaan dan pembuangannya, sehingga dapat membahayakan manusia dan lingkungan. Salah satu upaya untuk mengolah minyak pelumas bekas adalah dengan metode asidifikasi-adsorpsi. Metode asidifikasi atau penambahan asam kuat seperti asam sulfat (H2SO4) digunakan untuk menghilangkan pengotor dan mengembalikan beberapa sifat fisik seperti densitas, viskositas dan warna. kemudian untuk menghilangkan kandung logam Cu digunakan metode adsorpsi menggunakan adsorben dari selulosa yang berasal dari sekam padi. Tujuan dari penelitian ini yaitu mengetahui pengaruh penambahan asam sulfat (H2SO4) pada metode asidifikasi, mengetahui pengaruh komposisi massa sekam padi pada metode adsorbsi, serta membandingkan hasil pengujian minyak pelumas bekas sebelum dan setelah diolah ditinjau dari kadar logam berat yang terkandung, viskositas dan Spesific Garivity (SG). Berdasarkan penelitian yang sudah dilakukan penurunan konsentrasi logam Cu tertinggi terjadi pada asidifikasi H2SO4 sebanyak 5% dari volume sampel dengan variasi selusosa-asetat 1:3. Metode asidifikasi-adsorpsi dengan adsorben alami selulosa-kitosan berhasil dilakukan untuk mengubah beberapa sifat fisik dan kadar logam Cu dari minyak pelumas bekas. The use of lubricating oil in industry as a material to protect the machine from friction with other components produces waste that is flammable and explodes if mismanaged and disposed of, so that it can harm humans and the environment. One of the efforts to process used lubricating oil is by acidification-adsorption method. Acidification methods or the addition of strong acids such as sulfuric acid (H2SO4) are used to remove impurities and restore some of the physical properties such as density, viscosity and color. then to remove cu metal bladder used adsorption method using adsorbens from cellulose derived from rice husks The purpose of this study is to find out the effect of sulfuric acid addition (H2SO4) on acidification methods, find out the effect of rice husk mass composition on adsorbtion methods, and compare the results of testing of used lubricant oil before and after processing in view of the levels of heavy metals contained, viscosity and Spesific Garivity (SG). Based on research that has been done the highest reduction in cu metal concentration occurred in the acidification of H2SO4 as much as 5% of the sample volume with a cellulose-acetate variation of 1:3. The acidification-adsorption method with the natural adsorbent cellulose-chitosan was successfully performed to change some of the physical properties and levels of Cu metal from used lubricating oil.
Pemanfaatan Bioadsorben Dari Sekam Padi Untuk Mendegradasi Logam Cu Pada Minyak Pelumas Bekas Jusuf Pratama; Arlin Dini Anindya; Yurike Luckita; Nabila Nur Latiefa; Alfiana Adhitasari
Fluida Vol 15 No 1 (2022): FLUIDA
Publisher : Department of Chemical Engineering, Politeknik Negeri Bandung

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.35313/fluida.v15i1.3611

Abstract

Penggunaan minyak pelumas dalam industri sebagai bahan untuk melindungi mesin dari gesekan dengan komponen lain menghasilkan limbah yang sifatnya mudah terbakar dan meledak apabila salah dalam pengelolaan dan pembuangannya, sehingga dapat membahayakan manusia dan lingkungan. Salah satu upaya untuk mengolah minyak pelumas bekas adalah dengan metode asidifikasi-adsorpsi. Metode asidifikasi atau penambahan asam kuat seperti asam sulfat (H2SO4) digunakan untuk menghilangkan pengotor dan mengembalikan beberapa sifat fisik seperti densitas, viskositas dan warna. kemudian untuk menghilangkan kandung logam Cu digunakan metode adsorpsi menggunakan adsorben dari selulosa yang berasal dari sekam padi. Tujuan dari penelitian ini yaitu mengetahui pengaruh penambahan asam sulfat (H2SO4) pada metode asidifikasi, mengetahui pengaruh komposisi massa sekam padi pada metode adsorbsi, serta membandingkan hasil pengujian minyak pelumas bekas sebelum dan setelah diolah ditinjau dari kadar logam berat yang terkandung, viskositas dan Spesific Garivity (SG). Berdasarkan penelitian yang sudah dilakukan penurunan konsentrasi logam Cu tertinggi terjadi pada asidifikasi H2SO4 sebanyak 5% dari volume sampel dengan variasi selusosa-asetat 1:3. Metode asidifikasi-adsorpsi dengan adsorben alami selulosa-kitosan berhasil dilakukan untuk mengubah beberapa sifat fisik dan kadar logam Cu dari minyak pelumas bekas. The use of lubricating oil in industry as a material to protect the machine from friction with other components produces waste that is flammable and explodes if mismanaged and disposed of, so that it can harm humans and the environment. One of the efforts to process used lubricating oil is by acidification-adsorption method. Acidification methods or the addition of strong acids such as sulfuric acid (H2SO4) are used to remove impurities and restore some of the physical properties such as density, viscosity and color. then to remove cu metal bladder used adsorption method using adsorbens from cellulose derived from rice husks The purpose of this study is to find out the effect of sulfuric acid addition (H2SO4) on acidification methods, find out the effect of rice husk mass composition on adsorbtion methods, and compare the results of testing of used lubricant oil before and after processing in view of the levels of heavy metals contained, viscosity and Spesific Garivity (SG). Based on research that has been done the highest reduction in cu metal concentration occurred in the acidification of H2SO4 as much as 5% of the sample volume with a cellulose-acetate variation of 1:3. The acidification-adsorption method with the natural adsorbent cellulose-chitosan was successfully performed to change some of the physical properties and levels of Cu metal from used lubricating oil.
Determination Of Optimum Drying Condition On Flavonoid Content Of Ficus Carica L. Leaves Using Tray Dryer Emma Hermawati; Yusmardhany Yusuf; Alfiana Adhitasari
Fluida Vol 16 No 1 (2023): FLUIDA
Publisher : Department of Chemical Engineering, Politeknik Negeri Bandung

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.35313/fluida.v16i1.4401

Abstract

This research aims to find out the characteristics of Ficus carica L. drying process using a tray dryer and determine the effect of temperature and drying time on Ficus Carica L. flavonoid content using a tray dryer to obtain Ficus carica L. herbal leaf tea which is high in antioxidants. At the experimental stage, the water content of fresh leaves of Ficus carica L. were determined, so the water content is 74 ± 1.11% (wet base), then dried using a tray dryer at 35; 40; 45; 50; and 55oC, with a variation of the drying air flow rate of 1.3; 1.6; 1.9; 2.2; and 2.4 m/s. The optimum temperature and drying air flow rate are 50oC and 1.9 m/s since the highest flavonoid content was obtained at those condition as much 0.78 ± 0.001 gram QE/100gram extract. Dried products which packaged in tea bags have a content of 23.60% carbohydrate, total fat 3.50%, protein 5.35%,antioxidant 154.25 ppm and calorific value of 1430 Kcal/100 grams. It can be concluded that Ficus carica L. drying process using a tray dryer can be used to produce herbal leaf tea which is high in antioxidants and flavonoid content.
The Impact of Bifunctional Catalyst Synthesis Method Cu/ZnO/ZrO2/Al2O3-HZSM-5 on Dimethyl Ether Production from CO2 and H2 Adhitasari, Alfiana; Yulistiani, Fitria; Jahulan, Tufana Muhallik; Fadhillah, Fauzan
Fluida Vol. 17 No. 1 (2024): FLUIDA
Publisher : Department of Chemical Engineering, Politeknik Negeri Bandung

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.35313/fluida.v17i1.4782

Abstract

Indonesia has initiated a zero-carbon emission plan; one strategy is to replace Liquid Petroleum Gas (LPG) with eco-friendly fuels like Dimethyl Ether (DME). However, high Operational Expenditure (OPEX) for CO2 conversion technology poses a challenge. This research aims to address these techno-economic barriers by examining how catalyst synthesis methods, specifically Ultrasonic (US) and coprecipitation (CP), impact the performance of the bifunctional catalyst Cu/ZnO/Zr/Al2O3 – H+ Zeolite Socony Mobil-5 (CZZA-HZSM-5) in DME synthesis. The catalysts are characterized using the Brunauer-Emmett-Teller (BET) method and tested in a fixed-bed reactor at 240°C and 27.6 bar, followed by a bubble reactor containing methanol. Gas Chromatography-Mass Spectrometry (GC-MS) is used for analysis. The US method produces catalysts with higher surface area, pore volume, and average pore diameter than the CP method, with values of 45.93 m²/g, 0.3822 cc/g, and 1.6646 nm, respectively. Correspondingly, the US catalyst shows higher CO2 conversion and methanol yield, at 13.3% and 59.7%. DME as the final product is undetected in GC-MS analysis, likely due to differences in HZSM5 specifications, high reaction rates, and ΔG values above 1. This study enhances understanding of how catalyst synthesis methods affect CO2 conversion efficiency, crucial for developing sustainable fuel alternatives.