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All Journal IPTEK The Journal for Technology and Science Indonesian Journal of Chemistry Jurnal Purifikasi Reka Buana : Jurnal Ilmiah Teknik Sipil dan Teknik Kimia Jurnal Instrumentasi Jurnal Teknik Kimia Indonesia Makara Journal of Technology Scientific Contribution Oil and Gas
Setijo Bismo
Departemen Teknik Kimia, Fakultas Teknik, Universitas Indonesia, Depok 16424, Indonesia
Agriculture, Biological Sciences & Forestry Chemical Engineering, Chemistry & Bioengineering Chemistry Civil Engineering, Building, Construction & Architecture Computer Science & IT Earth & Planetary Sciences Electrical & Electronics Engineering Energy Engineering Environmental Science Industrial & Manufacturing Engineering Materials Science & Nanotechnology Mechanical Engineering

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Effects of Ph on Calcium Carbonate Precipitation Under Magnetic Field Saksono, Nelson; Yuliusman, Yuliusman; Bismo, Setijo; Soemantojo, Roekmijati W.; Manaf, Azwar
Makara Journal of Technology Vol. 13, No. 2
Publisher : UI Scholars Hub

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Abstract

Magnetic field effect on CaCO3 precipitation is the key parameter in evaluating the effectiveness of Anti-scale Magnetic Treatment (AMT). The purpose of this study was to investigate magnetic fields influence on CaCO3 precipitation in high and low super-saturated CaCO3 solution by varied pH CaCO3 solution using circulation flow fluid system. The observation results in the high super saturated solution (pH 8.5) showed the increase of precipited CaCO3 in magnetized solutions compared to those in non-magnetic solution during circulation process. In the low super-saturated CaCO3 solution (pH 6.4) it was found that magnetic treatment increased CaCO3 precipitation after circulation process. In high super-saturated solution, magnetic field strengthens ion interactions, which reduce precipitation during circulation process. However, in low super-saturated CaCO3 solution, magnetic field weakens hydrate ion interaction which indicated by decreasing of the conductivity of solution. It increases the precipitation of CaCO3 after the circulation of magnetization process has completed.
Formation of CaCO3 Particle and Conductivity of Na2CO3 and CaCl2 Solution Under Magnetic Field on Dynamic Fluid System Saksono, Nelson; Bismo, Setijo; Widaningroem, Roekmijati; Manaf, Azwar
Makara Journal of Technology Vol. 15, No. 1
Publisher : UI Scholars Hub

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Abstract

Hard water causes the CaCO3 scale formation on the pipe walls and heat exchanger equipments in industrial or domestic water processes. A great number of experimental researches on the prevention of the CaCO3 precipitation process by magnetic field have been carried out. In this research, Na2CO3 and CaCl2 solutions was magnetized in the circulated flow condition (dynamic fluid system). The velocity of fluid and the circulation time was modified to examine its influences to the magnetization process. CaCO3 content was measured by titration method of EDTA complexometry. Conductivity test was conducted to find out hydrate ion bonding. The results showed that magnetization increased the CaCO3 formation and the optimum process reaches for 10 minutes circulation on 0.554 m/s of flow rate. Magnetic field decreases the conductivities of Na2CO3 and CaCl2 solution, hence reduced the ion hydrate bonding. These results showed that magnetization on Na2CO3 and CaCl2 ionic solution was effective in controlling the CaCO3 formation by increasing CaCO3 precipitation.
The Plasma Electrolysis Phenomenon in a Two-Compartment Reactor for Chlor-Alkali Production Saksono, Nelson; Abqari, Fakhrian; Bismo, Setijo
Makara Journal of Technology Vol. 17, No. 2
Publisher : UI Scholars Hub

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Chlor-alkali is one of the most important processes in the chemical industry. It produces chlorine and caustic soda, which become the main feedstock of daily products. The aim of this study is to report the phenomenon of plasma electrolysis and how it can be used in chlor-alkali production for more efficient energy consumption. When the plasma is formed, the current fluctuates and gradually declines. Plasma electrolysis begins with the process of electrolysis itself. Due to Joule heating, gas bubbles are formed and a sheath is made on both electrodes, resulting in the plasma field. Plasma electrolysis can be identified by its radical production. The higher the voltage and concentration, the greater the production of radicals. In 10 minutes or less, the number of OH radicals produced can reach 4 ppm at 400 V and 0.1 M. This amount is relatively small and is caused by other reactions consuming OH radicals to form other radicals such as chlorine. The energy consumption of plasma electrolysis in this study can reach 16 kJ/mmol Cl2 at 0.5 M NaCl solution.
Ozone Plasma Nanobubble (OPN) Reactor Combined with Coagulation-Flocculation Process: A Promising Technology for Leachate Treatment Zahra, Habiibatuz; Azzahra, Ken; Putri, Azizka Inneke; Luvita, Veny; Bismo, Setijo
Indonesian Journal of Chemistry Vol 24, No 5 (2024)
Publisher : Universitas Gadjah Mada

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.22146/ijc.94559

Abstract

According to World Bank data, approximately 2.01 billion tons of urban waste is produced annually, with approximately 33% of waste being improperly managed, leading to concentrated and toxic leachate. This poses a global challenge due to its varied characteristics influenced by climate, landfill age, and waste composition, resulting in groundwater and surface water pollution with severe impacts on human health, ecosystems, and biodiversity, necessitating stringent treatment measures. To address this, a study integrated coagulation-flocculation and advanced oxidation processes (AOPs) using a dielectric barrier discharge (DBD) ozone plasma nanobubble (OPN) reactor to degrade leachate. Gas flow rate, plasma voltage, and gas sources are variated. This research uses O2 or air as a gas source that produces plasma. The leachate is fed into the DBD reactor, so the bubble will burst and produce further ROS. Optimal results were observed after 60 min, with oxygen gas feed reducing total suspended solids (TSS), chemical oxygen demand (COD), and biological oxygen demand (BOD) by 100, 93.93, and 74.12%, respectively, alongside a decrease in pH. This study indicates the promising potential of this technology for leachate treatment and demonstrates the potential for nitrate production using both types of gas feed.
BIODEGRADATION ENHANCEMENT OF OILY WASTEWATER BY OZONATION METHOD Syafrizal; Zulkifliani; Fami Adetyas Maulana Pratama; Setijo Bismo
Scientific Contributions Oil and Gas Vol. 38 No. 2 (2015): SCOG
Publisher : Testing Center for Oil and Gas LEMIGAS

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.29017/scog.38.2.239

Abstract

This research is aimed at improving the ability of oily wastewater biodegradation through the ozonation method, where ozone will oxidize organic compounds in the oily wastewater that are diffi cult to be degraded by bacteria so that the structure becomes simpler. The ozonation process is done by using a corona-discharge ozonator and semi-batch reactor, and the process is varied by ozone dose and pH value. The ozonation process is then followed by a biodegradation process, where the bacteria that is used is Pseudomonas sp. This study also observed the effect of surfactants in supporting the biodegradation processes. An indicator of research success is the increase in the biodegradation percentage of the sample, followed by an increase in the value of the constant rate of bacterial growth. The research results shows that the ozonation method and the use of surfactant can support the oily wastewater biodegradation process. This is shown by the value of the biodegradation percentage and the constant rate of bacterial growth results, in which respective values are able to reach 86,787% and 0,339 at the optimal operating conditions (ozone dose of 0.53 g/h; pH 7; Bios-H surfactant concentration 500 ppm).
The Application of Catalytic Ozonation Technique using UV and Granular Activated Carbon (GAC) for Eliminating in Waste Phenol, COD, and 1,1,2,2-Tetrachloroethane Ikhsandy, Ferry; Bismo, Setijo; Karamah, Eva Fathul
Reka Buana : Jurnal Ilmiah Teknik Sipil dan Teknik Kimia Vol 7, No 1 (2022): EDISI MARET 2022
Publisher : Universitas Tribhuwana Tunggadewi Malang

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.33366/rekabuana.v7i1.2854

Abstract

Process eliminating compounds of phenol, Chemical Oxygen Demand (COD), and 1,1,2,2-tetrachloroethane using catalytic ozonation technique with catalyst Granular Activated Carbon (GAC) combination with Ultra Violet (UV) light emission performed in this study. This study aimed to obtain the effectiveness of applications catalytic ozonation technique using system configuration Ozone/GAC and Ozone/UV/GAC to eliminate waste phenol 1,1,2,2-tetrachloroethane COD with circulation time (0, 15, 30, 45, 60, and 120 minutes). The wastewater was derived from the wastewater Laboratory of Polyester Industrial in Bogor. The results were analyzed, comprised of COD with Ferrous Ammonium Sulphate (FAS) method, phenol using aminoantipirin method, and 1,1,2,2-tetrachloroethane with Gas Chromatography-Flame Ionization Detector (GC-FID) method. The result of study shown that the configuration of the Ozone/ UV/GAC with an initial concentration of phenol 58,00 mg/L, COD 72,00 mg/L and 1,1,2,2-tetrachloroethane 32,96 mg/L resulted in the percentage of eliminating phenol 57,76%, COD 66,67% and 1,1,2,2-tetrachloroethane 98,74% while the configuration of Ozone/GAC with an initial concentration of phenol 55,00 mg/L, COD 72,00 mg/L and 1,1,2,2-tetrachloroethane 37,70 mg/L resulted in percentage of eliminating phenol 50,91%, COD 55,56% and 1,1,2,2-tetrachloroethane 100%ABSTRAKProses penyisihan senyawa fenol, Chemical Oxygen Demand (COD) dan 1,1,2,2-tetrakloroetana menggunakan teknik ozonasi katalitik dengan katalis Granular Activated Carbon (GAC) yang dikombinasikan dengan emisi sinar Ultra Violet (UV) dilakukan dalam penelitian ini. Tujuan dari penelitian ini untuk memperoleh efektivitas aplikasi teknik ozonasi katalitik menggunakan sistem konfigurasi, yaitu: Ozon/GAC dan Ozon/UV/GAC dalam penyisihan limbah fenol, COD dan 1,1,2,2-tetrakloroetana dengan waktu sirkulasi (0, 15, 30, 45, 60, dan 120 menit). Limbah cair yang digunakan berasal dari limbah cair Laboratorium Industri Polyester di daerah Bogor. Analisis yang dilakukan meliputi analisis COD dengan metode Ferro Ammonium Sulfat (FAS), analisis Fenol dengan menggunakan metode aminoantipirin dan analisis 1,1,2,2-tetrakloroetana dengan metode Gas Chromatography-Flame Ionization Detector (GC-FID). Setelah dilakukan penelitian, diketahui bahwa konfigurasi Ozon/UV/GAC dengan konsentrasi awal fenol 58,00 mg/L, COD 72,00 mg/L dan 1,1,2,2-tetrakloroetana 32,96 mg/L menghasilkan persentase penyisihan senyawa fenol 57,76%, COD 66,67% dan 1,1,2,2-tetrakloroetana 98,74% sedangkan konfigurasi Ozon/GAC dengan konsentrasi awal fenol 55,00 mg/L, COD 72,00 mg/L dan 1,1,2,2-tetrakloroetana 37,70 mg/L menghasilkan persentase penyisihan senyawa fenol 50,91%, COD 55,56% dan 1,1,2,2-tetrakloroetana 100%.
Co-Authors Ade Putera Adi Cifriadi, Adi Asep Handaya Saputra Asep Handaya Saputra, Asep Azwar Manaf Azzahra, Ken Bondan Ariawan, Bondan Dadi R. Maspanger, Dadi E. Kristanti Elsa Krisanti Eva Fathul Karamah Eva Karamah Eva Karamah, Eva Fakhrian Abqari Fakhrian Abqari Fakhrian Abqari, Fakhrian Fami Adetyas Maulana Pratama Ferry Ikhsandy Hotdi Simbolon Hotdi Simbolon, Hotdi Johan Johan L Linda Laksono, Nelson Luvita, Veny Milasari Herdiana Putri Nelson Saksono Nelson Saksono Pratama, Fami Adetyas Maulana Putri, Azizka Inneke Rahma Muthia, Rahma Ratih Tien Seratri, Ratih Roekmijati Soemantojo Roekmijati Soemantojo, Roekmijati Roekmijati W. Soemantojo, Roekmijati W. Roekmijati Widaningroem Roekmijati Widaningroem, Roekmijati Roekmijati Widaningrum Roekmijati Widaningrum, Roekmijati Simbolon, Hotdi M. Slamet Slamet Sofia Loren Butarbutar Sugiarto, Anto Tri Sutrasno Kartohardjono syafrizal Syafrizal Syafrizal Tuti Indah Sari, Tuti Tuti Indah Sari, Tuti Indah Veny Luvita, Veny Widiatmini Sih Winanti Widodo Wahyu Purwanto Yuliusman Yuliusman Yuliusman Yuliusman Zahra, Habiibatuz Zulkifliani Zulkifliani, Zulkifliani