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Pelatihan Praktikum Kimia Sederhana di SMAN 16 Padang Imelda Imelda; Refinel Refinel; Refilda Refilda; Yefrida Yefrida; Hermansyah Aziz; Yulizar Yusuf; Suryati Suryati; Zulkarnain Chaidir; Sumaryati Syukur; Rahmiana Zein; Novesar Jamarun; Safni Safni; Zilfa Zilfa; Yetria Rilda; Norman Ferdinal; Tommi Hermansyah; Fivi Mona Bareno
Warta Pengabdian Andalas Vol 30 No 3 (2023)
Publisher : Lembaga Penelitian dan Pengabdian kepada Masyarakat (LPPM) Universitas Andalas

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.25077/jwa.30.3.562-568.2023

Chemistry is one of the subjects taught in State Senior High Schools (SMAN), especially in Natural Sciences (IPA). The problem with chemistry subjects is that it is difficult to practice in the laboratory because laboratory facilities such as space, equipment and chemicals are expensive. As a result, chemical laboratory practices were only sometimes carried out. Several lecturers and students from the Department of Chemistry, FMIPA Unand Kimia Unand, carried out service activities at SMAN 16 Padang through laboratory practice using materials and equipment that were cheap and readily available in the surrounding environment. This community service aims to train teachers and students to carry out chemistry practicums using simple materials and equipment available around them. The training was given to chemistry subject teachers and students in the science laboratory at SMAN 16 on 17 and 21 November 2022. The material was practised in oxidation and reduction (redox) and electrolysis reactions. The activity went smoothly; the students enthusiastically carried out the practicum. Through the results of this simple chemistry practicum, students can design and carry out chemical experiments using simple tools and materials, conduct direct observations of chemical processes, practice scientific thinking, attitude and work skills and analyze and solve various scientific processes using scientific methods. SMAN 16 hopes that this activity will continue with different topics.

Synthesis of Graphene Oxide Enriched Natural Kaolinite Clay and Its Application For Biodiesel Production Syukri Syukri; Fadhil Ferdian; Yetria Rilda; Yulia Eka Putri; Mai Efdi; Upita Septiani
International Journal of Renewable Energy Development Vol 10, No 2 (2021): May 2021
Publisher : Center of Biomass & Renewable Energy, Diponegoro University

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.14710/ijred.2021.32915

A heterogeneous catalyst is one type of catalyst which is very effective for biodiesel production; thus, in this study, a novel heterogeneous bifunctional catalyst was prepared by kaolinite clay obtained from Padang of West Sumatera and impregnated with graphene oxide and potassium hydroxide (KOH) for the simultaneous esterification and transesterification reactions of palm oil into biodiesel. For comparison, two other catalysts were also prepared. The first catalyst was the same clay which was heated at 450ºC for 4 hours, and the second catalyst was the same clay which was impregnated with potassium hydroxide (KOH) only. The three catalysts were characterized using X-Ray Fluorescence (XRF), X-Ray Diffraction (XRD), and Fourier Transform Infra-Red (FTIR). XRF analysis showed that the clay sample’s main composition consisted of 54% silica, 35% alumina, and 7% hematite. The XRD analysis results showed that the most dominant crystal composition was quartz, kaolinite, and hematite. The analysis results using FTIR showed a change in intensity and shift in wave numbers indicating a cation exchange. The catalytic activity test was carried out with a ratio of oil and methanol 1:6, catalyst amount 5%, 60ºC reaction temperature, and 4 hours of reaction time.The results showed that the catalytic activity of clays impregnated with graphene oxide and potassium hydroxide was better with a yield of 58% compared to clays without impregnation and other clays that were only impregnated with KOH under the yields of 0.8% and 0.4%, respectively

EFEK DOPING Ni (II) PADA AKTIFITAS FOTOKATALITIK DARI TiO2 UNTUK INHIBISI BAKTERI PATOGENIK Rilda, Yetria; Dharma, Abdi; Arief, Syukri; Shaleh, Baharuddin
Makara Journal of Science Vol. 14, No. 1
Publisher : UI Scholars Hub

Show Abstract | Download Original | Original Source | Check in Google Scholar

Influence of Co-Doping of Ni (II) on Photocatalytic Activity of TiO2 for Pathogenic Bacteria Inhibition. Nanoparticle titanium dioxide (TiO2) has most attention in the past decade, since it can be applied as alternative material on sterilization photocatalyst process. This research focused on increasing performance of titania such as structure, particles size and surface area through Ni ion doped on TiO2 surface by sol-gel technique. Product were used to design of a photobioreactor for sterilization process from pathogenic bacteria such as Escherichia coli, Staphylococcus aureus and Bacillus subtilis. Product were characterized using Thermogravimetric-Differential Thermal Analysis (TG-DTA), X-ray Diffraction (XRD), Transmition Electron Microscopy (TEM), Scanning Electron Microscopes-Energy Dispersive X-Ray Spectroscopy (SEM-EDX) dan Brunauer-Emmet-Teller (BET). Titanium dioxide with anatase structure have 12.1 nm in particles size and surface area 49.6 m2 / g that have higher inhibition rate to bacteria cell. Photobiocatalytic reaction was carried out in various TiO2-Ni concentration and UV irradiation times. The anti bacteria from TiO2-Ni to all bacteria cell suspension after UV irradiated at λm : 365 nm has good synergistic effect. Effect of mechanical treatment by sonicator showed the increasing inhibition rate around 4% for 120 minute irradiation. Inhibition rate optimization for each bacteria gave different efficiency inhibition to TiO2-Ni concentration 1.5-2.0 g/L. TiO2-Ni powder inhibited growth of Escherichia coli, Staphylococcus aureus around ≥ 95% for 120 minute irradiation, while Bacillus subtilis resistance with inhibition percentage rate only 88.1%.

Separation of Kaolinite from Clay Minerals and Its Catalytic Activity in Transesterification Reactions Rahayu, Rahayu; Nengsih, Zarnida Widia; Arief, Syukri; Rilda, Yetria; Alif, Matlal Fajri; Syukri, Syukri
Hydrogen: Jurnal Kependidikan Kimia Vol 12, No 1 (2024): February 2024
Publisher : Universitas Pendidikan Mandalika

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.33394/hjkk.v12i1.10600

Kaolinite is a type of clay mineral that has the potential to be used as a heterogeneous catalyst in transesterification reactions. However, natural clay still contains a mixture of minerals that occur together. Therefore, as an effort to search for cheaper catalysts to reduce the price of biodiesel production, this study carried out the separation of kaolinite from natural clay and tested its performance as a catalyst in biodiesel production from Waste Cooking Oil (WCO). Separation of the kaolinite fraction was carried out with the help of NH4Cl as a dispersing agent. The main mineral composition of clay as quartz, kaolinite, montmorillonite and hematite. After the separation process, the crystallinity of the minerals experienced an increase marked by an increase in the intensity of several kaolinite peaks, namely in the 2θ 12.24° area from 103 to 108 and at 25.00° from 95 to 125. Thermal modification caused the loss of several kaolinite peaks in the area. 2θ 12.17°; 24.94° and 62.39°. The Si/Al ratio decreased after the fractionation and calcination processes. Average particle size of h-clay decreased from 27.61 µm to 21.09 µm in K-clay. The K-clay catalyst produced the highest conversion of palmitic acid at 42%, while c-K-clay produced the highest conversion of oleic acid and stearate at 30%. In addition, the density and water content of biodiesel catalyzed by K-clay and c-k-clay meet SNI standards. This finding has the potential to be further developed as a cost-effective catalyst based on natural resources in biodiesel production.

Pembuatan Teh Daun Kelor untuk Peningkatan Ekonomi Masyarakat di Kecamatan Ulakan Tapakis, Padang Pariaman Matlal Fajri Alif; Yulizar Yusuf; Emriadi Emriadi; Deswati Deswati; Mai Efdi; Novesar Jamarun; Syukri Arief; Adlis Santoni; Bustanul Arifin; Suryati Suryati; Yetria Rilda; Safni Safni; Zilfa Zilfa; Olly Norita Tetra
Warta Pengabdian Andalas Vol 31 No 4 (2024)
Publisher : Lembaga Penelitian dan Pengabdian kepada Masyarakat (LPPM) Universitas Andalas

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.25077/jwa.31.4.682-688.2024

The Moringa plant, a tropical species, exhibits prolific growth and is abundantly present in Indonesia and other tropical regions worldwide. An extended lifespan, continuous flowering, and a high tolerance for elevated temperatures characterize it. Utilizing its components, including leaves, bark, seeds, and roots, this multifaceted plant is renowned for its therapeutic properties. The plant's antioxidants and various nutrients, including vitamins and minerals (iron, magnesium, vitamin B6, vitamin B2, vitamin C, and vitamin A), have led to studies on the plant's potential health benefits. In order to develop the local economy in Ulakan village, Padang Pariaman Regency, Moringa plants were processed by using the plant leaves to manufacture herbal tea, which can then be sold. This community service program was significant given the widespread presence and ease of cultivation of Moringa plants within the local region. The program involved the planning and selection of the activity site, the implementation of training sessions, and the assessment of the program's outcomes. The result of this community engagement initiative was the demonstrated interest of many participants in producing Moringa leaf tea.

Pembuatan Teh Daun Kelor untuk Peningkatan Ekonomi Masyarakat di Kecamatan Ulakan Tapakis, Padang Pariaman Matlal Fajri Alif; Yulizar Yusuf; Emriadi Emriadi; Deswati Deswati; Mai Efdi; Novesar Jamarun; Syukri Arief; Adlis Santoni; Bustanul Arifin; Suryati Suryati; Yetria Rilda; Safni Safni; Zilfa Zilfa; Olly Norita Tetra
Warta Pengabdian Andalas Vol 31 No 4 (2024)
Publisher : Lembaga Penelitian dan Pengabdian kepada Masyarakat (LPPM) Universitas Andalas

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.25077/jwa.31.4.682-688.2024

The Moringa plant, a tropical species, exhibits prolific growth and is abundantly present in Indonesia and other tropical regions worldwide. An extended lifespan, continuous flowering, and a high tolerance for elevated temperatures characterize it. Utilizing its components, including leaves, bark, seeds, and roots, this multifaceted plant is renowned for its therapeutic properties. The plant's antioxidants and various nutrients, including vitamins and minerals (iron, magnesium, vitamin B6, vitamin B2, vitamin C, and vitamin A), have led to studies on the plant's potential health benefits. In order to develop the local economy in Ulakan village, Padang Pariaman Regency, Moringa plants were processed by using the plant leaves to manufacture herbal tea, which can then be sold. This community service program was significant given the widespread presence and ease of cultivation of Moringa plants within the local region. The program involved the planning and selection of the activity site, the implementation of training sessions, and the assessment of the program's outcomes. The result of this community engagement initiative was the demonstrated interest of many participants in producing Moringa leaf tea.

Overcoming Stunting in Children with VCO-prebiotic as a Nutritional Supplement with Housewives from the DASHAT Program Armaini; Sumaryati Syukur; Rahmiana Zein; Yetria Rilda; Upita Septiani; Tio Putra Wendari
Warta Pengabdian Andalas Vol 32 No 2 (2025)
Publisher : Lembaga Penelitian dan Pengabdian kepada Masyarakat (LPPM) Universitas Andalas

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.25077/jwa.32.2.147-158.2025

Stunting in children is a chronic malnutrition problem caused by a lack of nutritional intake for a long time, especially in the first 1,000 days of life. The prevalence of stunted children in West Sumatra is 25.2%, and in Padang City it is 19.5%, which shows a high stunting rate in Padang City. The Community service activities empower housewives to produce VCO with prebiotics as a nutritional supplement for stunted children in Bukik Karan Rawang Village, Padang City. Providing VCO supplements that contain good fats, prebiotics, and antioxidants improves children's digestive systems, increases their immunity, prevents them from infectious diseases, and supports the development of their brains and nervous systems. Technology transfer provides skills for mothers of stunted children to make their own VCO, and can also improve the family economy. The growth and development of stunted children improve, as indicated by measurable parameters such as increased height and weight, after they are given VCO with prebiotics. Weight gain between 1-1.8 kg, an average of 1.47 kg, and height between 2.2-7 cm, an average of 4.38 cm in stunted children. Education on diet and Parenting Patterns for stunted children is carried out by providing knowledge, training, nutritional counseling, and parenting to increase insight among mothers of stunted children about nutrition supplements and healthy and nutritious foods to achieve improved health. Providing VCO with prebiotics can enhance children's growth and development and improve their nutritional status to help overcome stunting.

Pengaruh Modifikasi Fisika pada Komposisi, Struktur Kristal dan Sifat Katalitik Lempung Solok Admi, Admi; Angellika, Florencia Tri; Rilda, Yetria; Syukri, Syukri
Jurnal Fisika Unand Vol 11 No 4 (2022)
Publisher : Universitas Andalas

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.25077/jfu.11.4.548-555.2022

Mineral lempung yang diperoleh dari Kabupaten Solok, Sumatera Barat, telah dimodifikasi secara fisika melalui pemanasan pada 105Â°C, 450Â°C dan 850Â°C. Aktivitas katalitiknya telah diuji dalam transesterifikasi minyak jelantah untuk menghasilkan metil ester asam lemak. Komposisi utama lempung ditemukan terdiri dari Si, Al dan Fe serta unsur-unsur minor lainnya seperti K, Ti, Na, Ca Mg, dan Mn (pengukuran XRF). Jenis mineral utama sampel lempung adalah kaolinite dan illite (karakterisasi XRD). Kalsinasi pada suhu 850 Â°C mengakibatkan penurunan fasa kaolinit yang menandakan telah terjadi transformasi parsial menjadi metakaolin (analisis XRD). Pengujian aktivitas katalitik di bawah kondisi reaksi tertentu dari semua lempung menunjukkan bahwa lempung yang dikalsinasi pada 850Â°C menghasilkan dua jenis senyawa biodiesel yaitu metil ester asam palmitat dan metil ester asam oleat (analisis GC-MS). Tanah liat yang dipanaskan pada suhu 110 dan 450 oC sama sekali tidak menunjukkan aktivitas katalitik

Separation of Kaolinite from Clay Minerals and Its Catalytic Activity in Transesterification Reactions Rahayu, Rahayu; Nengsih, Zarnida Widia; Arief, Syukri; Rilda, Yetria; Alif, Matlal Fajri; Syukri, Syukri
Hydrogen: Jurnal Kependidikan Kimia Vol. 12 No. 1 (2024): February 2024
Publisher : Universitas Pendidikan Mandalika

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.33394/hjkk.v12i1.10600

Kaolinite is a type of clay mineral that has the potential to be used as a heterogeneous catalyst in transesterification reactions. However, natural clay still contains a mixture of minerals that occur together. Therefore, as an effort to search for cheaper catalysts to reduce the price of biodiesel production, this study carried out the separation of kaolinite from natural clay and tested its performance as a catalyst in biodiesel production from Waste Cooking Oil (WCO). Separation of the kaolinite fraction was carried out with the help of NH4Cl as a dispersing agent. The main mineral composition of clay as quartz, kaolinite, montmorillonite and hematite. After the separation process, the crystallinity of the minerals experienced an increase marked by an increase in the intensity of several kaolinite peaks, namely in the 2Î¸ 12.24Â° area from 103 to 108 and at 25.00Â° from 95 to 125. Thermal modification caused the loss of several kaolinite peaks in the area. 2Î¸ 12.17Â°; 24.94Â° and 62.39Â°. The Si/Al ratio decreased after the fractionation and calcination processes. Average particle size of h-clay decreased from 27.61 Âµm to 21.09 Âµm in K-clay. The K-clay catalyst produced the highest conversion of palmitic acid at 42%, while c-K-clay produced the highest conversion of oleic acid and stearate at 30%. In addition, the density and water content of biodiesel catalyzed by K-clay and c-k-clay meet SNI standards. This finding has the potential to be further developed as a cost-effective catalyst based on natural resources in biodiesel production.

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