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All Journal EKSAKTA: Journal of Sciences and Data Analysis JURNAL KIMIA SAINS DAN APLIKASI Biota: Jurnal Ilmiah Ilmu-Ilmu Hayati Prosiding Seminar Nasional Sains Dan Teknologi Fakultas Teknik Abdimas Indonesian Journal of Cancer Chemoprevention Journal of Degraded and Mining Lands Management The Journal of Pure and Applied Chemistry Research Jurnal Kimia dan Kemasan Agrokreatif Jurnal Ilmiah Pengabdian kepada Masyarakat EduChemia: Jurnal Kimia dan Pendidikan Jurnal Kimia Mulawarman BERITA BIOLOGI Jurnal Bioteknologi & Biosains Indonesia (JBBI) JURNAL KONVERSI Chimica et Natura Acta ALCHEMY Jurnal Penelitian Kimia Akta Kimia Indonesia JKPK (Jurnal Kimia dan Pendidikan Kimia) Berkala Penelitian Hayati Makara Journal of Science Magistrorum et Scholarium: Jurnal Pengabdian Masyarakat Jurnal Manusia dan Lingkungan Molekul: Jurnal Ilmiah Kimia
Hartati Soetjipto
Universitas Kristen Satya Wacana
Agriculture, Biological Sciences & Forestry Arts Humanities Biochemistry, Genetics & Molecular Biology Chemical Engineering, Chemistry & Bioengineering Chemistry Computer Science & IT Earth & Planetary Sciences Education Energy Engineering Environmental Science Immunology & microbiology Industrial & Manufacturing Engineering Languange, Linguistic, Communication & Media Law, Crime, Criminology & Criminal Justice Materials Science & Nanotechnology Medicine & Pharmacology Social Sciences

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Extraction and Chemical Compounds Identification of Red Rice Bran Oil Using Gas Chromatography – Mass Spectrometry (GC-MS) Method Hoo Sheren Hartono; Hartati Soetjipto; A. Ign. Kristijanto
EKSAKTA: Journal of Sciences and Data Analysis VOLUME 17, ISSUE 2, August 2017
Publisher : Fakultas Matematika dan Ilmu Pengetahuan Alam

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.20885/eksakta.vol17.iss2.art2

Abstract

The objectives of the study are to obtain optimum yield of extraction red rice bran oil, to determine the physico-chemical characteristics, and componen coumpounds. Data was analyzed using Nir Parametric Statistics by Friedmann test. The result showed the optimum extraction results was obtained by the ratio of substrate : solvent of 1: 8 and the oil yield was 12.31 ±0.325%. The physico properties of red rice bran oil were greenish brown colour, with a density ranged from 0.908 ± 0.014 to 0.922 ± 0.014 (g/mL), and the water content ranged from 0.87 ± 0.06 to 0.91 ± 0.02 %. The chemical properties of red rice bran oil were: the acid number ranged from 116.41 ± 1.22 to 118.11 ± 2.45 (mg NaOH/g); the saponification number ranged from 193.74 ±21.88 to 199.62 ± 12.63 (mg KOH/g); and the peroxide number ranged from 24.37 ± 2.44 to 26.07 ± 4.88 (mgek/kg), respectively. Oils was analyzed used GC-MS. The chemical components of rice bran oil are oleic acid (46.24%), palmitic acid (18.25%), linoleic acid (13.29%), 9-octadecane(7.76%).
PENGARUH PEMURNIAN TERHADAP MUTU MINYAK BIJI PEPAYA (Carica papaya L.) DITINJAU DARI SIFAT FISIKO KIMIA Riska Cahyaningtyas; Hartati Soetjipto; Cucun Alep Riyanto
Prosiding SNST Fakultas Teknik Vol 1, No 1 (2017): PROSIDING SEMINAR NASIONAL SAINS DAN TEKNOLOGI 8 2017
Publisher : Prosiding SNST Fakultas Teknik

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (182.209 KB)

Abstract

Penelitian ini bertujuan untuk memperoleh rendemen minyak biji pepaya (Carica papaya L.) sebelum dan setelah pemurnian serta menentukan karakteristik sifat fisiko-kimiawinya. Minyak biji pepaya diperoleh secara maserasi selama 18 jam menggunakan n-heksan. Sifat fisiko kimia yang diuji antara lain bilangan asam, bilangan penyabunan, bilangan peroksida, aroma, warna, kadar air dan massa jenis. Pemurnian minyak biji pepaya dilakukan dengan cara degumming dan netralisasi. Rendemen ekstraksi minyak biji pepaya diperoleh sebesar 15.70±1.34% (bk) sedangkan setelah pemurnian diperoleh sebesar 35.78±9.06% (bk). Sifat Fisikokimia sebelum pemurnian memiliki kadar air minyak sebesar 1,06 ± 0,33% ; massa jenis 0,91±0,00g/mL ; bilangan peroksida sebesar  21,77±1,28 mgek/kg ; bilangan asam sebesar 37,47±0,07mg NaOH/g minyak ; dan bilangan penyabunan sebesar 147,55±4,73mg KOH/g minyak.. Sedangkan setelah pemurnian sebagai berikut: loss minyak 64,23± 4,19%. Kadar air 0.88±0.05 ; bilangan Peroksida 12,85±1,56 mgek/kg ; Bilangan asam 29,17±0,47 mg NaOH/g minyak ; Bilangan Penyabunan 91,95±5,62 mg KOH/g minyak..Kata kunci : Carica papaya L., fisikokimia, maserasi, pemurnian 
Pemberdayaan Anggota PKK di Desa Lembu dalam Membuat Kosmetik Sri Hartini; Hartati Soetjipto; Cucun Alep Ryanto; Margareta Novian Cahyanti; Dewi Kurniasih Arum Kusuma Hastuti
Agrokreatif: Jurnal Ilmiah Pengabdian kepada Masyarakat Vol. 2 No. 2 (2016): Agrokreatif Jurnal Ilmiah Pengabdian kepada Masyarakat
Publisher : Institut Pertanian Bogor

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.29244/agrokreatif.2.2.81-86

Abstract

Community Service in the Village Lembu, District of Bancak on 2015/2016 focused on training the manufacture of cosmetic products. The most mothers Household of PKK’s member supplied and trained in one skill, namely the training of cosmetic products, such as soaps, lotions and others. Service activities packaged in the form of community empowerment by methods PRA (Participatory Rural Appraisal) to form the basis of a briefing about the character cosmetic products and training products manufacture. The implementation steps include the stage of awareness of materials, devices used when creating products and maturation/curing of the product before use. The practice of making cosmetic conducted in groups and each group of at least 5 people. Completeness is the continuity of the motivation for the manufacture of cosmetic products which are prepared to serve the needs of the market. From the results of development activities can be concluded that the public powerful of time management and become skilled productive use of household appliances for the production of cosmetics, and does not stutter anymore to make cosmetics with the appropriate technology. Marketing begins with consumers who come from the rural communities Lembu, then slightly extends in the District Bancak. Two excellent products that can meet the needs of the community are soaps and lotions with a sale value of Rp. 10.000/100 ml. Monitoring and evaluation of cosmetic products made in directly consultation with the campus UKSW.
ISOLASI DAN IDENTIFIKASI SENYAWA ANTIBAKTERI MINYAK ATSIRI DAUN KEMBANG BULAN {Tithonia diversifolia (Hemsley) A. Gray} Hartati Soetjipto; Lusiawati Dewi; Sentot Adi Prayitno
BERITA BIOLOGI Vol 9, No 2 (2008)
Publisher : Research Center for Biology-Indonesian Institute of Sciences

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.14203/beritabiologi.v9i2.2024

Abstract

Isolation and identification of chemical compounds and antibacterial compounds of the essential oil of Kembang bulan or Japanese sunflower {Tithonia diversifolia (Hemsley) A. Gray} leaves showed that the essential oil contain 29 components. The main components were caryophyllene (27.76%), nerolidol (21.81%),caryophyllene oxide (7.06%), copaene (6.41%) and bicylogermacrene (4.90%). The oil was screened for their antibacterial activity through bioautography method. Two antibacterial spots which had Rf 0.49 and Rf 0.61were obtained. The spot with Rf 0.49 was a mixture of 21 compounds with main compounds were heneicosane, nonacosane and tetratetracontane, while the spot with Rf 0.61 consisted of 22 compounds, which the main compound was nerolidol.
SKRINING FITOKIMIA DAN UJI TOKSISITAS EKSTRAK DAUN PECUT KUDA (Stachytarpheta jamaicensis L. Vahl) TERHADAP LARVA UDANG Artemia salina Leach Lany Indrayani; Hartati Soetjipto; Lydia Sihasale
JURNAL PENELITIAN BIOLOGI BERKALA PENELITIAN HAYATI Vol 12 No 1 (2006): December 2006
Publisher : The East Java Biological Society

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.23869/399

Abstract

Phytochemical screening and Brine Shrimp lethality test of pecut kuda leaf extract had been done against Artemia salina Leach. The aims of this study is to screen potentially bioactive extract of pecut kuda leaf as an effort ti find out the chemical substances responsible for the toxic effect. The Pecut kuda leaves (Stachytarpheta jamaicensis, L. Vahl) was extracted by methanol 80%, then partitioned successively with hexane, chloroform, and ethyl acetate. Phytochemical screening was done according to Ciulei method (1984). The toxicity effect was tested against A. salina, L (Brine Shrimp Test). The result of phytochemical screening known that compounds in the extract of pecut kuda leaves (S. jamaicensis, L. Vahl), hexane fraction contained of sterol and triterpenes; where the chloroform fraction contained of saponin, sterol, and triterpenes; further more the ethyl acetate fraction contained flavonoid, tannin, saponin, sterol, dan triterpenes. The result of the study shows that several fractions of extract of pecut kuda leaves (S. jamaicensis) hexane fraction, chloroform, and ethyl acetate was toxic because it was able to kill more than 50% larva of A. salina, L at the concentration less than 1000 ppm. The LC50 of all fractions of pecut kuda leaves extract (S. jamaicensis, L. Vahl) were shown from the most toxic to the lowest were as followed: LC50 of hexane fraction = 98.33 ppm, of chloroform raction LC50 = 204.17 ppm, and of ethyl acetate fraction LC50 = 249.80 ppm. Finally results of the TLC profile showed that all fraction (hexane, chloroform, and ethyl acetate) indicated that the pecut kuda leaves extract (S. jamaicensis) contained terpenoid compound.
PENGARUH PEMURNIAN DEGUMMING DAN NETRALISASI TERHADAP PROFIL MINYAK BIJI LABU KUNING (Cucurbita moschata D.) Hartati Soetjipto; Apriyanti Tindage; Margareta Novian Cahyanti
JURNAL KONVERSI Vol 7, No 1 (2018)
Publisher : Universitas Muhammadiyah Jakarta

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.24853/konversi.7.1.8

Abstract

ABSTRACTThe objective of the study were to obtain of pumpkin (C. moschata D.) seed oil yield using hexane soxhlet extraction method and the effect of purification on the profile of pumpkin seed oil fatty acids. The results of the study showed that the yield of pumpkin seed crude oil was 37,98% (b/b), whereas the optimum rendement after purification was 76,27% (w/w) by using 0,15% H3PO4. The GC-MS analysis of pumpkin seed oil showed the presence of three same main components of pumpkin seed oil before and after purification which are: linoleic acid, palmitic acid, and stearic acid, respectively. The content of pumpkin seed oil before purification are as follows: 57,96% of linoleic acid, 24,63% of palmitic acid, dan 6,82% of stearic acid, respectively. In the contrary, the content of pumpkin seed oil after purification are as follows: 48,21% of linoleic acid, 20,70% of palmitic acid, dan 5,27% stearic acid, respectively. The purification processes do not affect on the main components of pumpkin seed oil, but determine the difference percentages of pumpkin seed oil main components.
Synthesis and Determination Level of Calcium-Phosphate Hydroxyapatite (HAp) from Chicken Eggshell Imelda Wadu; Hartati Soetjipto; Margareta Novian Cahyanti
JKPK (Jurnal Kimia dan Pendidikan Kimia) Vol 3, No 1 (2018): JKPK (Jurnal Kimia dan Pendidikan Kimia)
Publisher : Program Studi Pendidikan Kimia FKIP Universitas Sebelas Maret

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (705.472 KB) | DOI: 10.20961/jkpk.v3i1.11860

Abstract

The purpose of this study was to synthesize bio-ceramics hydroxyapatite (HAp) from local chicken eggshell and broiler chicken eggshell. The synthesis was done by using precipitation method with sintering temperature 1000ºC. In addition, to determine the levels of calcium-phosphate contained in HAp bioceramics AAS and Spectrophotometer UV-Vis were used. The results show that of 10 grams of each eggshell powder can produce 8.8-9.8 g of HAp powder. Determination of calcium level in HAp by AAS was about ± 71.23% from local chicken eggshell and ± 78.62% from broiler chicken eggshell. Whereas determination of phosphate level in HAp using Spectrophotometer UV-Vis was about ± 67.22% from local chicken and ± 73.75% from broiler chicken eggshell.
Characterization and Antibacterial Activity Test of Hydroxyapatite (HAp) from Chicken Eggshell against Lactobacillus acidophilus Bacteria Imelda Wadu; Hartati Soetjipto; Margareta Novian Cahyanti
JKPK (Jurnal Kimia dan Pendidikan Kimia) Vol 2, No 3 (2017): JKPK (Jurnal Kimia dan Pendidikan Kimia)
Publisher : Program Studi Pendidikan Kimia FKIP Universitas Sebelas Maret

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (807.354 KB) | DOI: 10.20961/jkpk.v2i3.11862

Abstract

The purposes of this study were to characterize Hydroxyapatite (HAp) bioceramics which synthesized from local chicken and broiler eggshell using FTIR, and to determine HAp antibacterial activity with the highest content of calcium-phosphate (HAp from broiler chicken eggshell) using paper disc method. Characterization of HAp from local chicken eggshell using FTIR showed peaks for PO43- functional group on the wavelength 1040.08, 608.46 and 568.67 cm-1; OH- functional group on the wavelength 3426.39 and 2880.46 cm-1; CO2 functional group on the wavelength 2142.91 cm-1; and CO32- functional group on the wavelength 1653.64 cm-1. Whereas broiler chicken eggshell HAp showed peaks for PO43- functional group on the wavelength 1044.40, 604.13 and 568.66 cm-1; OH- functional group on the wavelength 3419.61 and 2838.35 cm-1; CO2 functional group on the wavelength 2086.69 cm-1; and CO32- functional group on the wavelength 1653.64 cm-1. HAp antibacterial activity test against caries bacteria L. acidophilus gives the positive results either for the lowest test dose (5μg/μL) or the highest test dose (75μg/μL), which was characterized by the formation of diameter inhibitory area 22.93±0,066 and 33.08±0,031 mm (strong category of >20 mm), respectively. The characterization of HAp from local chicken and broiler chicken eggshell using FTIR confirmed the presence of HAp compounds, and the antibacterial activity test result of HAp synthesized from broiler chicken eggshell indicates a positive and strong antibacterial power.
THE EFFECT OF TEMPE FERMENTATION TIME ON THE TOTAL PHENOLIC AND ISOFLAVONE GENISTEIN CONTENTS Kiki Fransiska Suharto; Hartati Soetjipto; Yohanes Martono
ALCHEMY Jurnal Penelitian Kimia Vol 13, No 2 (2017): September
Publisher : UNIVERSITAS SEBELAS MARET (UNS)

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.20961/alchemy.13.2.5094.228-238

Abstract

The objective of this study was to evaluate total phenolic compounds and isoflavone genistein contents during 0 - 9 days of fermentation time. Isoflavone extract were obtained by maceration and fractionation. Total phenolic compounds were measured by Folin ciocalteau method, meanwhile, the isoflavone genistein contents were analyzed by a High Performance Liquid Chromatography. The yield of isoflavone extract and the total phenolic compounds were analyzed using a randomized completely block design and the mean between treatments was compared by the Honestly Significant Difference (HSD) test using significance level of 5 %. The highest amount of total phenolic compounds during the incubation time was obtained on 4 days of fermentation time, i.e., 232.05n ± 7.71 μg/g, while the highest content of isoflavone genistein was obtained on 5 days of fermentation time, i.e., 100.48 μg/g. This research confirms that the fermentation process of tempe induces the total phenolic contents and the production of isoflavone genistein is fluctuating.
Composition of Fatty Acids and Squalene Content of Wild Spinach (Amaranthus dubius Mart) Seed Oil Soetjipto, Hartati; Krisdayanti, Mitra; Aminu, November Rianto
Makara Journal of Science Vol. 25, No. 2
Publisher : UI Scholars Hub

Show Abstract | Download Original | Original Source | Check in Google Scholar

Abstract

This study aims to determine the yield of wild spinach seed oil obtained by continuous extraction methods using Soxhlet apparatus for 10.5 hours in n-hexane solvent, the physio-chemical properties, and the composition of wild spinach seed oil using the Gas Chromatography-Mass Spectrometry (GC-MS) method. Refinement of wild spinach seed oil was done by degumming and neutralization. The yield of wild spinach seed oil extraction before refinement was 4.36 ± 0.29% (w/w) while after refinement was 0.68 ± 0.033% (w/w). Physio-chemical properties of wild spinach seed oil after refinement was as follows: water content 0.37%; peroxide value 9.5 meq/kg; acid value of 0.53 mg KOH/g oil; saponification value 208.9 mg KOH/g oil. The results of GC-MS analysis showed that the wild spinach seeds were composed of 5 main components: dodecanoic acid (0.28%); tetradecanoic acid (0.08%); palmitic acid (1.31%); squalene (94.9%); and linoleic acid (3.34%).
Co-Authors A Ign Kristijanto A. Ign Kristijanto Antonius Rizky Meilano Apriyanti Tindage Asmorowati, Rica Susy Augustinus Ignatius Kristijanto Cucun Alep Riyanto Cucun Alep Ryanto Devina Intan Sari Dewi Kurniasih Arum Kusuma Hastuti Divina Anindya Della Diyonisio Kevin Elisando Febriyanti, Teresa Franciska Alvina Hanny Hafiar Hoo Sheren Hartono I S Jamil Imelda Wadu Indah Tri Susilowati J Winarno KH Timotius Kiki Fransiska Suharto Krisdayanti, Mitra Kristijanto, Agus Ign. Laili Nurrohmah Laili Nurrohmah Lany Indrayani Lusiawati Dewi Lydia Sihasale Margareta Novian Cahyanti Mitra Krisdayanti Murda Pradipta November Rianto Aminu Novena Risnalani Rintank Constani Novenda Pramesti Ayuningtyas Purwoko, Agus R Sudaryanto Riska Cahyaningtyas S Supriyadi Salsabila, Unik Hanifah Sentot Adi Prayitno Sri Hartini Sri Hartini Suprihati Suprihati Suprihati Susanti Pudji Hastuti Teguh Wahyono Teresa Febriyanti Tiffany Febetania Widodo Trisna Anggreini Widhi Nugroho Meindra Yayi Suryo Prabandari Yoga Andika Putra Yoga Andika Putra Yohanes Martono Yuliawati Zulfa Yuniarti