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All Journal Jurnal Teknik Kimia USU ABDI SABHA (Jurnal Pengabdian kepada Masyarakat) Jurnal Teknik Kimia USU

Iriany

Departemen Teknik Kimia, Fakultas Teknik Universitas Sumatera Utara

Author-ID : 4065296

Religion Arts Humanities Chemical Engineering, Chemistry & Bioengineering Chemistry Education Engineering Environmental Science Industrial & Manufacturing Engineering Materials Science & Nanotechnology Social Sciences

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PEMBUATAN BIOBRIKET DARI PELEPAH DAN CANGKANG KELAPA SAWIT: PENGARUH VARIASI KOMPOSISI BAHAN BAKU DAN WAKTU KARBONISASI TERHADAP KUALITAS BRIKET Iriany; Cindy Carnella; Cici Novita Sari
Jurnal Teknik Kimia USU Vol. 5 No. 3 (2016): Jurnal Teknik Kimia USU
Publisher : Talenta Publisher (Universitas Sumatera Utara)

Briquette was a product of the compaction process of biomass residue used as fuel and it is formed using binder. Briquette from biomass has a high heating value. The quality of briquettes influenced by raw material composition and the time of carbonization. The carbonization process in the manufacture of briquettes could improve heating value and reduce smoke produced from burning briquette. This research is aim to study the effect of variations in the composition of raw materials and carbonization time on the heating value and the characteristics of the resulting briquettes. The materials used are palm fronds, palm shells, starch, used oil, H2SO4 and Tri Ethyl Amine (TEA). The ratios of palm frond and palm shell charcoal in this research is 1: 2, 1: 4, 1: 6 and 1: 8 with variation of carbonization time 30 minutes, 60 minutes, 90 minutes and 120 minutes. The research began with the carbonization process of the raw materials. Then charcoal product of carbonization was pressed using an binder starch and used oil as much as 20% based on the weight of raw materials at the ratio of 1: 1. The best quality from this research is obtained at the ratio palm fronds and oil palm shell 1: 8 with carbonization time of 120 minutes, heating value 15107,138 cal/g, moisture content 6%, ash content of 5,185%, volatile matter 39,226%, fixed carbon 70,955%, density 0,442 g/cm3, burning rate 0,273 g/min, and compressive strength 0,046 N / mm2. The result shows the briquettes produced had a strong structure, it was not easily broken and it was not moldy when stored.

PENGARUH PERBANDINGAN TEMPURUNG KELAPA DAN ECENG GONDOK SERTA VARIASI UKURAN PARTIKEL TERHADAP KARAKTERISTIK BRIKET Iriany; Firman Abednego Sarwedi Sibarani; Meliza
Jurnal Teknik Kimia USU Vol. 5 No. 3 (2016): Jurnal Teknik Kimia USU
Publisher : Talenta Publisher (Universitas Sumatera Utara)

This research used raw material water hyacinth and coconut shell. The purpose of this research is to get briquettes with high heating value and to obtain briquettes with good quality. Comparison of the base material mixed water hyacinth and coconut shell in this research is 1:1, 1:2, 1:3, 1:4 with variations in particle size of 10 mesh, 42 mesh and 60 mesh, and using an adhesive tapioca 10% from the weight of raw material. The results of measurement in this research was compared to the quality parameters such as SNI, Japan standard, British, and America. The survey results revealed that the ideal composition made from a mixture of water hyacinth and coconut shell is briquette in comparison 1:4 with particle size 60 mesh and have the highest of heating value is 6.851,3311 cal/g, the lowest ash content is 8,1918%, the lowest of moisture content is 1,0140%, levels of substance evaporates is 13,7890%, the value of density is 0.9836 g/cm3, the firing rate is 2,9x10 -3 g/sec and the compressive strength is 11,3234 kg/cm2. The results are in accordance to SNI, Japan standard, British, and America, while the compression pressure of briquette only accordance to British standard.

DESORPSI β-KAROTEN MINYAK KELAPA SAWIT (CRUDE PALM OIL) DARI KARBON AKTIF MENGGUNAKAN ISOPROPANOL Nurul Aini; Olyvia Putri Wardhani; Iriany
Jurnal Teknik Kimia USU Vol. 5 No. 4 (2016): Jurnal Teknik Kimia USU
Publisher : Talenta Publisher (Universitas Sumatera Utara)

The aim of the research is to study the ability of isopropyl alcohol in the desorption of β-carotene and to obtain kinetic model and desorption isoterm which is suitable in β-carotene desorption. The main material used were isopropyl alcohol and activated carbon containing β-carotene. The variabels used in this research are desorption temperature, activated carbon concentration and parameter observed is concentration of β-carotene in isopropyl alcohol. In the desorption process, activated carbon which adsorp β-carotene was soaked in isopropyl alcohol. To review the desorption kinetics, this research was carried out in various temperature such as 40 oC, 50 oC, and 60 oC. In desorption isoterm process is, various mass of activated carbon was used. Desorption process will be analyzed at spesified time. This research used the first order of desorption kinetics model. The desorption constant rate obtained for 40 oC, 50 oC, and 60 oC are 0,013, 0,014, and 0,036 minute-1 with activation energy is 0,226 kkal/mol. The maximum desorption percentage obtain is 41,94 %. The desorption isoterm model which fit with the β-carotene desorption was Langmuir isoterm model with constanta value 1,2077 L/mg and -0,2218.

PENGARUH PENAMBAHAN BENTONIT TERMODIFIKASI SEBAGAI PENGISI TERHADAP SIFAT MEKANIK DAN PENYERAPAN AIR KOMPOSIT EPOKSI Alvian; Kenrick; Iriany
Jurnal Teknik Kimia USU Vol. 5 No. 4 (2016): Jurnal Teknik Kimia USU
Publisher : Talenta Publisher (Universitas Sumatera Utara)

Research about the application of modified bentonite as filler in epoxy has been done for the purpose of getting the best composition of modified bentonite as filler at epoxy composite to obtain the best mechanical properties such as tensile strength, impact strength and the water absorption. In this research, epoxy resin mixed with bentonite which have been modified using cetyltrimethylammonium bromide (CTAB) surfactant with various concentrations of 0,05M, 0,1M, and 0,15M. Modified bentonite filler and TiO2 then mixed with epoxy resin with various concentration of 5%, 10%, 15%, and 20% of filler from the total mass of the composite and then the composite was produced with hand lay-up method. The result of FTIR characterization showed that the bond between matrix and the filler produced was only interfacial bonding. The result of the mechanical properties test indicated that 5% of filler composition with 0,1M of surfactant concentration obtained the maximum value of tensile strength and mechanical strength respectively 33,667 MPa and 12564,9 J/m2. The result of mechanical properties test was supported by analysis of Scaning Electron Microscopy (SEM). On the test of water absorption, the water absorption capacity increased along with the increased of filler composition.

PEMBUATAN KARBON AKTIF DARI CANGKANG BUAH KARET (Hevea brasilliensis) DENGAN AKTIVATOR H3PO4 DAN APLIKASINYA SEBAGAI PENJERAP Cr(VI) Muhammad Zulfadhli; Iriany
Jurnal Teknik Kimia USU Vol. 6 No. 1 (2017): Jurnal Teknik Kimia USU
Publisher : Talenta Publisher (Universitas Sumatera Utara)

Activated carbon from lignocellulosic materials are renewable, abundant, and inexpesive. Rubber shell activated carbon that activated chemicaly has abilty to adsorp heavy metal. The purpose of this research is to study the effect of phosphoric acid concentration toward characteristics of rubber shell activated carbon, and its ability to adsorp Cr(VI). The materials used in this research are rubber shell, aquadest, and Cr(VI) solution. This research was started by impregnating rubber shell with phosphoric acid at 20%, 40% and 60% for 1 hour and then sample was carbonizated in furnace at 500oC for 1 hour. After that, activated carbon was applied to adsorp Cr(VI). The characteristic of surface area of rubber shell activated carbon are measured by BET method. Furthermore, the residual concentration of Cr(VI) was measured with Atomic Adsortion Spectrophotometer. The result shows that characteristics of rubber shell activated carbon such as moisture content, ash content, volatile matter have fulfilled National Standard of Indonesia (SNI) except ash content of activated carbon that activated by 20% phosphoric acid. Surface area of activated carbon has fulfilled the standard of commercial adsorbent. The largest adsorption capasity is obtained using Rubber shell activated carbon that activated by 40% phosphoric acid with adsorption percentage 96,67%.

PEMBUATAN KARBON AKTIF DARI CANGKANG BUAH KARET DENGAN AKTIVATOR H3PO¬4 DAN APLIKASINYA SEBAGAI PENJERAP Pb(II) Joko Murtono; Iriany
Jurnal Teknik Kimia USU Vol. 6 No. 1 (2017): Jurnal Teknik Kimia USU
Publisher : Talenta Publisher (Universitas Sumatera Utara)

Activated carbon necessity in Indonesia was increasing along with the developments of the industriaization era. Based on natural product in Indonesia, probably activated carbon necessity could be guaranteed by domestic production. Rubber shells were solid waste which has potential for multiple uses such as raw materials for the manufacture of activated carbon. In this researched, rubber shells waste were processed into activated charcoal. The aim of this researhed was to determine the effect of the concentration of phosphoric acid activator toward the characteristics of the activated carbon and activated carbon absorption capacity to Pb(II). Shells rubber that passed by the of 100 mesh sieve was impregnated with phosphoric acid (H3PO4) as activator in the ratio fruit shells rubber: phosphoric acid (b:b) of 1:2 and varying concentrations of H3PO4 at 20%, 40%, and 60% for 1 hour. After immersion in the acid, then material was carbonized in a furnace at temperature 500 oC for 1 hour. Surface area of activated carbon was analyzed by usning Braunanear, Emmelt and Teller and concentration of adsorption of Pb(II) was measured by Atomic Absorption Spectroscopy. The results showed the general characteristics of activated carbon comparable to the Indonesian National Standard. The largest adsorption capasity percentage 74% is obtained using Rubber shell activated carbon that activated by 20% phosphoric acid .

EKSTRAKSI TANIN DARI KULIT KAYU AKASIA DENGAN MENGGUNAKAN MICROWAVE: PENGARUH DAYA MICROWAVE, WAKTU EKSTRAKSI DAN JENIS PELARUT Iriany; Florentina Pandiangan; Christina Eka P
Jurnal Teknik Kimia USU Vol. 6 No. 3 (2017): Jurnal Teknik Kimia USU
Publisher : Talenta Publisher (Universitas Sumatera Utara)

Tannin is one of complex polyphenol compound which soluble in polar solvent. Tannin could be extracted from acacia bark. This study aims to examine microwave-assisted extraction of tannins under influence of microwave power, extraction time, and solvent and its application to adsorb Cd and Cu. Tannin was extracted from acacia bark with feed-to-solvent ratio (1:20 g/ml). Power of microwave was adjusted 100 W, 180 W, 300 W, 450 W, and 600 W for 1 minute, 3 minutes and 5 minutes respectively using aquadest and ethanol as the solvent. The extracts were analyzed using UV-Vis spectrophotometer. Furthermore, the extract with the highest yield of tannins are used as the adsorbent. The concentration of Cd and cu were analyzed using Atomic Absorption Spectrophotometer. The result showed the highest yield of tannin 26.606 mg/g at 100 W and 3 minutes extraction time using ethanol as the solvent. The result showed that the adsorption capacity of adsorbent from tannin was 3.81 mg/g and 2.26 mg/g for Cd and Cu respectively.

MODEL KINETIKA EKSTRAKSI FLAVONOID DARI BAYAM MERAH (Alternanthera amoena voss) Iriany; Irsa Septiawan; Salwa Jody Gustia
Jurnal Teknik Kimia USU Vol. 6 No. 4 (2017): Jurnal Teknik Kimia USU
Publisher : Talenta Publisher (Universitas Sumatera Utara)

Red spinach (Alternanthera amoena voss) contains vitamins, protein, and flavonoids. Flavonoid is polyphenol compounds having properties as a free radical catcher.The purpose of this research is to obtain the kinetic rate of flavonoid mass transfer from red spinach.Extraction is one of the way to take flavonoids contained in solids with the assist of solvents. Mass transfer in liquid solid extraction occurs by diffusion. The determination of mass transfer coefficient (KC) is to conduct the rate of mass transfer of flavonoids from solids. In this study, the effect of temperature on the extraction of flavonoids from red spinach with water solvent is observed. The temperatures extraction in this research are of 50°C, 60°C, and 70°C respectively. Determinationof total flavonoid, mass transfer coefficient, and antioxidant activity carried out using FT-IR Spectrophotometry and UV-VIS Spectrophotometry. This study concluded that the increase in extraction time and temperature will increase the total content of flavonoids and extract rendement.Mass transfer coefficient equation in this study is K = 3078645 . Antioxidants in red spinach are included in the group of very strong antioxidants.

EKSTRAKSI MINYAK ATSIRI BUNGA MELATI DENGAN MENGGUNAKAN PELARUT ISOPROPIL ETER : PENGARUH WAKTU, TEMPERATUR, DAN RASIO MASSA BUNGA MELATI DENGAN VOLUME PELARUT Febrina Iskandar; Michael Dillo Rizki Ginting; Iriany; Okta Bani
Jurnal Teknik Kimia USU Vol. 8 No. 1 (2019): Jurnal Teknik Kimia USU
Publisher : Talenta Publisher (Universitas Sumatera Utara)

Jasmine flower is one of the high value commodities. One of the applications of jasmine flower is jasmine essential oil. Jasmine essential oil is often used to produce high quality parfume. Extraction is one of the methods for extracting jasmine essential oil, usually by the help of solvent. In this study, the effect of extraction time, extraction temperature, and solvent to jasmine flower ratio on jasmine oil extraction was studied. The extraction was carried out at 30oC, 35oC, and 40oC for 2 hours, 3 hours, 4 hours, and 5 hours by using isopropyl ether. The ratio of jasmine flower to isopropyl ether were 1:3; 1:4; and 1:5 (m/v). The resulting jasmine oil was analyzed by GC-MS and its quality was assessed according to SNI 06-2385-2006 which include colour test, refractive index analysis, acid number analysis, and ester number analysis. This experiment showed that increasing of extraction time, extraction temperature, and volume of solvent lead to increase of absolute yield of jasmine essential oil. The highest jasmine oil yield was obtained at 10.63 %. The jasmine oil contained 45.34% benzyl acetate and had yellow color. Its refractive index, acid number, and ester number were 1.485, 26.228 mg KOH/gram jasmine essential oil, and 159.885 mg KOH/gram jasmine essential oil.

EKSTRAKSI MINYAK ATSIRI BUNGA MELATI: PENGARUH RASIO MASSA BUNGA MELATI DENGAN VOLUME PELARUT N-HEKSANA, WAKTU EKSTRAKSI, DAN TEMPERATUR EKSTRAKSI Michael Dillo Rizki Ginting; Febrina Iskandar; Iriany; Okta Bani
Jurnal Teknik Kimia USU Vol. 8 No. 1 (2019): Jurnal Teknik Kimia USU
Publisher : Talenta Publisher (Universitas Sumatera Utara)

Jasmine flower (Jasminum sambac) contains essential oil compounds. Jasmine flower essential oil is a high-quality essential oil. Essential oils are volatile oils that have aroma similar to the original plant. Jasmine flower essential oil is sought due to its calming and anti-depression nature. In this study, the effect of extraction temperature, extraction time and solvent to jasmine flower ratio on jasmine oil was studied. The extraction was carried out at 30oC, 35oC, and 40oC for 2 hours, 3 hours, 4 hours, and 5 hours by using n-hexane. The ratio of jasmine flower to n-hexanes were 1:3; 1:4; and 1:5 (w/v). Resulting jasmine oil was analyzed by GC-MS, and its quality was assessed according to SNI 06-2385-2006 which include colour test, refractive index analysis, acid number analysis, and ester number analysis. This experiment showed that increasing of extraction time, extraction temperature, and volume of solvent lead to increase of absolute yield of jasmine essential oil. The highest jasmine oil yield obtained at 11.69 %. The jasmine oil contained was 47.14 % benzyl acetate and had yellow color. Its refractive index, acid number, and ester number were 1.478, 20.92 mg KOH/gram jasmine essential oil, and 150.27 mg KOH/gram jasmine essential oil respectively.

Co-Authors Akhmad Anugerah S Alvian Andrew Faguh Sitanggang Christina Eka P Cici Novita Sari Cindy Carnella Daniel Reymondo Manurung Dian Halimah Batubara Febrina Iskandar Firman Abednego S. Sibarani Firman Abednego Sarwedi Sibarani Fitri Hariani Nurza Florentina Pandiangan Irsa Septiawan Irvan Jasinda Joko Murtono Josua Manurung Juan Surya Manurung Kenrick Kherliyanda Febriani Krisnawati M. Thoriq Al Fath Meliza Michael Dillo Rizki Ginting Muhammad Zulfadhli Nurul Aini Okta Bani Olyvia Putri Wardhani Rahmad Dennie A. Pohan Ranggita Dwi Nindya Affandi Reni Sutri Reny Arapenta Ginting Rinaldry Sirait Rivaldi Sidabutar Rondang Tambun Salwa Jody Gustia Sari Liza Azura Nst Seri Maulina Tagora Bangkit P.S Taslim Taslim Toni Rizki Aruan Venansia Matondang

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