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PROTEKSI KATODIK DENGAN ANODA TUMBAL SEBAGAI PENGENDALIAN KOROSI BAJA DALAM LINGKUNGAN AQUEOUS UTAMI, ISNI
Jurnal Teknik Kimia Vol 3, No 2 (2009): JURNAL TEKNIK KIMIA
Publisher : Program Studi Teknik Kimia

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.33005/jurnal_tekkim.v3i2.112

Cathodic Protection is one of the method to Control Corrosion rate thermodynamically by applying steel as cathode. Application of this methode is by flow the DC current through electrolite to steel so that potential interface between steel and electrolite goes to immun area or until paricular value which corrosion speed allowed (minimum).Cathodic Protection using sacrificial anode methode was researched in electrochemistry way.Experiment was done to AISI SAE 1018 steel in NaCl environtment 3.5% within 168 to 840 hours using sacrificial anode Al and Zn.From analysis data using mass loss methode, Al anode able to decrease steel corrosion speed untill 82% and Zn for 50. %Keyward :Cathodic protection, sacrificial anode

AKTIVASI ZEOLIT SEBAGAI ADSORBEN GAS CO2 Utami, Isni
Jurnal Teknik Kimia Vol 11, No 2 (2017): JURNAL TEKNIK KIMIA
Publisher : Program Studi Teknik Kimia

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.33005/jurnal_tekkim.v11i2.831

Aktivasi zeolit sebagai adsorben gas CO2 dari biogas dilakukan secara kimia dan fisika dengan tujuan menghilangkan pengotor organik untuk mendapatkan bentuk kation dan kerangka zeolit yang berbeda,Aktivasi zeolit ditujukan untuk modifikasi zeolit dan memperbaiki karakter zeolit.Secara kimia sebagai activator digunakan H2SO4 dengan konsentrasi bervariasi pada rentang 5% s/d 30% dan secara fisika dilakukan kalsinasi pada suhu 500 OC selama 4 jam. Proses adsorpsi dilakukan dengan mengalirkan gas CO2 sintetis 98,86% dari bagian bawah kolom adsorber berdiameter 5 cm dan tinggi 30 cm dengan rate 0,0022 lt/menit s/d 0,0058 lt/menit, tinggi adsorben dalam kolom 28 cm dan ukuran butir zeolit -20/+28 mesh .Penelitian menghasilkan kondisi terbaik pada aktivasi kimia H2SO4 25% dan kalsinasi meningkatkan perbandingan Si/Al 76,95% dan peningkatan daya serap gas CO2 75,5 % pada rate gas masuk adsorber 0,0022lt/menit.

MODEL ROTATING CYLINDER ELEKTRODE UNTUK MENENTUKAN KEPERLUAN RAPAT ARUS PROTEKSI KATODIK Utami, Isni
JURNAL TEKNOLOGI TECHNOSCIENTIA Technoscentia Vol 1 No 1 Agustus 2008
Publisher : Lembaga Penelitian & Pengabdian Kepada Masyarakat (LPPM), IST AKPRIND Yogyakarta

Effect of fluids flow rate onto necessity of current density cathodic protection which characterized using Rotating cylinder electrode (RCE) model has been researched on an electrochemistry manner. This research was done to AISI 1018 steel as the electrode spinning cylinder-shaped inside aerated dissolvable NaCl 3.5%. using variation spinning rate 0-2000rpm and 25-75 0C temperature. Current density cathodice protection necessity determined from the steel interface potential -800mV with reference anode Ag/AgCl. Experiment result shows as the increasing of electrode rate, cathode protection current density needs increased due to diffusion layer tare faction and also because corrosion potential become more positive. Higher temperature would increasing cathode protection current density needs and makes corrosion potential more negative. Oxygen activation energy value to be diffused onto electrode surface support the corrodibility AISI 1018 toward temperature increment, because cathode reaction controlled by transfer mass of dissolved oxygen. With un-dimensioned number analysis and data experiment calculation, empiric formula which is functional relation between electrode rate/fluids flow rate characterized as turbulence flow toward cathodic protection current density is mentioned below: iPRCE = 0,0841 0,6539 0,4976

Model Pengendalian Katodik Dalam Elektrode Disk Pemutar Sistem Korosi Utami, Isni
Jurnal Teknik Industri Vol 12, No 1 (2011): Februari
Publisher : Department Industrial Engineering, University of Muhammadiyah Malang

The effect of fluids flow rate onto necessity of current density cathodic protection which characterized using RotatingÂ disk electrode (RDE) model has been researched on an electrochemistry manner. This research was done to AISI 1018 steel as the electrode spinning cylinder-shaped inside aerated dissolvable NaCl 3.5%. using variation spinning rate 0â€“2000rpm and 25â€“75Â° C temperature. Current density cathodic protection necessity determined from the steel interface potential - 800mV with reference anode Ag/AgCl. Experiment result shows that the increasing of electrode rate, cathodic protection current density needs increased due to diffusion layer tare faction and also because corrosion potential become more positive. Higher temperature would increase cathode protection current density needs and makes corrosion potential more negative. Oxygen activation energy value to be diffused onto electrode surface support the corrodibility AISI 1018 toward temperature increment, because cathodic reaction controlled by transfer mass of dissolved oxygen.

MODEL ROTATING CYLINDER ELEKTRODE UNTUK MENENTUKAN KEPERLUAN RAPAT ARUS PROTEKSI KATODIK Utami, Isni
JURNAL TEKNOLOGI TECHNOSCIENTIA Technoscentia Vol 1 No 1 Agustus 2008
Publisher : Lembaga Penelitian & Pengabdian Kepada Masyarakat (LPPM), IST AKPRIND Yogyakarta

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.34151/technoscientia.v1i1.380

Effect of fluids flow rate onto necessity of current density cathodic protection which characterized using Rotating cylinder electrode (RCE) model has been researched on an electrochemistry manner. This research was done to AISI 1018 steel as the electrode spinning cylinder-shaped inside aerated dissolvable NaCl 3.5%. using variation spinning rate 0-2000rpm and 25-75 0C temperature. Current density cathodice protection necessity determined from the steel interface potential -800mV with reference anode Ag/AgCl. Experiment result shows as the increasing of electrode rate, cathode protection current density needs increased due to diffusion layer tare faction and also because corrosion potential become more positive. Higher temperature would increasing cathode protection current density needs and makes corrosion potential more negative. Oxygen activation energy value to be diffused onto electrode surface support the corrodibility AISI 1018 toward temperature increment, because cathode reaction controlled by transfer mass of dissolved oxygen. With un-dimensioned number analysis and data experiment calculation, empiric formula which is functional relation between electrode rate/fluids flow rate characterized as turbulence flow toward cathodic protection current density is mentioned below: iPRCE = 0,0841 0,6539 0,4976

DEMINERALISASI AIR AC DENGAN MEMBRANE REVERSE OSMOSIS Akbar, Dika Restu; Kuspambudijaya, Akbar Dwi; Utami, Isni
Jurnal Teknik Kimia Vol 15, No 1 (2020): JURNAL TEKNIK KIMIA
Publisher : Program Studi Teknik Kimia

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.33005/jurnal_tekkim.v15i1.2300

Proses demineralisasi merupakan proses penghilangan garam mineral di udara, sehingga udara yang dihasilkan memiliki kemurnian yang tinggi. Air demin merupakan produk air yang memiliki kandungan mineral olahan di dalamnya atau air yang tidak mengandung mineral. Penelitian ini menggunakan proses Reverse Osmosis. Membrane reverse osmosis adalah membran semi berpori yang melepaskan molekul menggunakan tekanan lebih besar dari tekanan osmotik yang dilakukan secara alami untuk menghilangkan udara yang terkontaminasi dalam prosesnya. Peneliti menggunakan air limbah AC sebagai bahan utama, dan menggunakan membrane reverse osmosis, jenis membran spiral, bahan membran poliamida, komposit film tipis. Penelitian dilakukan dengan tekanan 30, 50, 70psi dan waktu operasi 20, 40, 60, 80, 100menit. Hasil penelitian yang diperoleh dapat disimpulkan bahwa, kadar udara AC yang memenuhi baku mutu air demineralisasi adalah nilai TDS pada tekanan 50psi dengan waktu operasi 100menit, total coliform terbaik pada tekanan 50psi dengan waktu operasi 100menit yang tidak menghasilkan total coliform, dan kadar timbal (Pb) pada 30psi dengan waktu operasi 80menit. DOI : https://doi.org/10.33005/jurnal_tekkim.v15i1.2300

Model Pengendalian Katodik Dalam Elektrode Disk Pemutar Sistem Korosi Isni Utami
Jurnal Teknik Industri Vol. 12 No. 1 (2011): Februari
Publisher : Department Industrial Engineering, University of Muhammadiyah Malang

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.22219/JTIUMM.Vol12.No1.65-70

The effect of fluids flow rate onto necessity of current density cathodic protection which characterized using Rotating disk electrode (RDE) model has been researched on an electrochemistry manner. This research was done to AISI 1018 steel as the electrode spinning cylinder-shaped inside aerated dissolvable NaCl 3.5%. using variation spinning rate 0–2000rpm and 25–75° C temperature. Current density cathodic protection necessity determined from the steel interface potential - 800mV with reference anode Ag/AgCl. Experiment result shows that the increasing of electrode rate, cathodic protection current density needs increased due to diffusion layer tare faction and also because corrosion potential become more positive. Higher temperature would increase cathode protection current density needs and makes corrosion potential more negative. Oxygen activation energy value to be diffused onto electrode surface support the corrodibility AISI 1018 toward temperature increment, because cathodic reaction controlled by transfer mass of dissolved oxygen.

Synthesis and Modification of Nano-Precipitated Calcium Carbonate (PCC) with Addition of Ethylene Glycol Sani; Mega Rosilina; Mochamad Titus Maulana; A. R Yelvia Sunarti; Srie Muljani; Dwi Hery Astuti; Isni Utami
International Journal of Eco-Innovation in Science and Engineering Vol. 3 No. 01 (2022): IJEISE
Publisher : Engineering Faculty, University of Pembangunan Nasional Jawa Timur

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.33005/ijeise.v3i01.57

ZA fertilizer waste (Ammonium sulfate) is waste generated from the industrial process of producing ZA fertilizer. The waste contains very high calcium and has the potential to be used as a raw material in the manufacture of Precipitated Calcium Carbonate (PCC). PCC with certain qualities can be developed in the field of advanced materials, with size modification into nanoparticles. One method to produce nanoparticles is using the coprecipitation method, with the help of a polymer solution. This study aims to produce Nano-PCC by finding the best conditions of CaCl2: Ethylene Glycol mole ratio and stirring speed. Nano-PCC is synthesized by reacting fertilizer waste with HCl to form a CaCl2 solution. Then, the solution is mixed with ethylene glycol to prevent particle agglomeration so that the size obtained will be smaller. The mixture is then reacted with Na2CO3 to form precipitated calcium carbonate (PCC). In this study, the variables were the mole ratio of CaCl2: ethylene glycol (1:12, 1:14, 1:18, 1:20) and stirring speed (350, 500, 650, 800, and 950 rpm). Based on PSA analysis, the Nano-PCC obtained at the smallest CaCl2: ethylene glycol ratio 1:12, stirring speed 950 rpm was 51.83 nm. Based on Scherrer’s calculations with XRD, the particle size obtained was 48.25 nm. SEM analysis showed that the crystals formed were dominated by vaterite crystals, with a size range of 55.71-607.79 nm.

Corrosion Control of Metal Alloy Using Inhibitor Synergy: Phospate – Carbohydrazide Fachrul Nurcholis; Aditya Irfansyah; Isni Utami; Lilik Suprianti
Nusantara Science and Technology Proceedings 3rd International Conference Eco-Innovation in Science, Engineering, and Technology
Publisher : Future Science

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.11594/nstp.2022.2756

Stainless steel is a kind of metal alloy that is widely used in industrial equipment. The problem faced by all metals that come into contact with corrosive medium is corrosion. Corrosion or metal deterioration can not be avoided since it is a spontaneous reaction between the metal with its environment. One method to control the corrosion of metal alloy is by adding the inhibitor into the medium. The addition of inhibitors in synergy is discussed. The addition of a phosphate inhibitor as a film-forming role on the metal surface is assisted by the addition of carbohydrazide components in controlling dissolved oxygen levels in seawater. The addition of inhibitors in synergy is expected to increase the efficiency of the inhibitor’s performance in a single work. This research aims to determine the best composition for phosphate and carbohydrazide inhibitors due to the effect of synergy in controlling the corrosion rate of metal alloys in seawater. The synthetic seawater medium was the 3.5% NaCl dilution prepared by diluting the NaCl crystal into the demineralized water. The phosphate inhibitor was added into the medium with various compositions (100, 200, 300, 400, and 500 ppm). Then, the carbohydrazide was added into the medium with the multiple compositions 5, 7.5, 10 and 15. The corrosion rate measurement was done by using Electrochemical Impedance Spectroscopy Instrument. The Stainless steel sample was prepared by cutting the stainless steel plate with a size 1cm x 1 cm and a thickness of around 2- 3 mm. The measurement process was done by putting the specimen in the working electrode and dipping into the medium with and without the inhibitors. The results show that the addition of inhibitor effectively decreases the corrosion rate. The best result is obtained when the ratio between phosphate and carbohydrazide is 100:10 ppm, which reduces the corrosion rate from 0.40128 mpy to 0.008 mpy

The Effect of Resin and NH4OH Addition in The Making of Ammonium Silica Fertilizer from Geothermal Sludge Kindriari Nurma Wahyusi; Atika Nandini; Lucky Indrati Utami; Siswanto; Isni Utami; Nurul Mardhiyah; Dian Nofita
International Journal of Eco-Innovation in Science and Engineering (IJEISE) Vol. 2 No. 1 (2021): IJEISE
Publisher : International Journal of Eco-Innovation in Science and Engineering (IJEISE)

Show Abstract | Download Original | Original Source | Check in Google Scholar

Geothermal sludge is a waste product from geothermal where it contains SiO2 which can be used as fertilizer. In this study, the making of silica ammonium fertilizer was carried out by taking salicy acid from geothermal sludge by extracting and adding resin which was then modified with NH4OH addition. Extraction was done using 1000 ml of KOH 1 N to dissolve 60 grams of Geothermal Sludge. Resins are added with variations in resin weight, namely, 5, 10, 20, 30, and 40 grams. NH4OH was added with variations in concentrations namely 3, 6, 9, 12 and 15% with a ratio of filtrate and NH4OH solution of 1: 1. The resulting ammonium silica inorganic liquid fertilizer products were analyzed for free silica and ammonia levels. The results of this study indicate that the levels of free silica and ammonia are influenced by the weight of the resin used and the concentration of ammonium hydroxide mixed. From the results of the research, it was found that inorganic silica liquid fertilizer with the highest SiO2 content in ammonium silica liquid fertilizer occurred when adding 20 grams of resin with the addition of NH4OH with a concentration of 15% which was 1,831.87 mg / L while the highest NH3 content in fertilizer liquid ammonium silica occurs when adding 40 grams of resin with the addition of NH4OH with a concentration of 15% which is equal to 252,312.80 mg / L.

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