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All Journal Jurnal Matematika & Sains Bulletin of Chemical Reaction Engineering & Catalysis The Journal of Pure and Applied Chemistry Research Journal of Mathematical and Fundamental Sciences Journal of Engineering and Technological Sciences World Chemical Engineering Journal EduChemia: Jurnal Kimia dan Pendidikan PENELITIAN DAN KARYA ILMIAH PROSIDING SEMINAR NASIONAL CENDEKIAWAN Indonesian Journal of Chemistry Prosiding Seminar Nasional Pakar CHEESA: Chemical Engineering Research Articles JURNAL PENELITIAN DAN KARYA ILMIAH LEMBAGA PENELITIAN UNIVERSITAS TRISAKTI Tedc Jurnal Penelitian dan Karya Ilmiah Lembaga Penelitian Universitas Trisakti Bulletin of Chemical Reaction Engineering & Catalysis al Kimiya : Jurnal Ilmu Kimia dan Terapan
Deana Wahyuningrum
Institut Teknologi Bandung
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 1 
SINTESIS KOMPLEKS NIKEL(II) DENGAN LIGAN TURUNAN SALISILIDEN ANILIN SEBAGAI SENYAWA POTENSIAL OLED Irma Nuril Maryam; Deana Wahyuningrum; Irma Mulyani
Jurnal TEDC Vol 10 No 1 (2016): Jurnal TEDC
Publisher : UPPM Politeknik TEDC Bandung

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Abstract

Senyawa kompleks Nikel(II) dengan ligan turunan salisiliden anilin berhasil disintesis dengan metode MAOS(Microwave Assisted Organic Synthesis) dan di pelajari aktivitasnya sebagai senyawa potensial OLED(Organic Light-Emitting Diode). Senyawa-senyawa imina (E)-2-((4-chlorophenylimino)methyl)phenol (L1) dan(E)-2-((p-tolylimino)methyl)phenol (L2) disintesis dengan pelarut etil l-laktat:air (9:1), rendemen masing-masing97% (Tl: 98-100°C) dan 96% (92-94°C). Berdasarkan analisis spektrum IR, 1H NMR, 13C NMR, dan MSmenunjukkan senyawa L1 dan L2 sudah terbentuk. Kompleks Nikel (II) hasil sintesis berwarna hijau mudauntuk K1 (terdekomposisi pada 190°C) dan hijau tua untuk K2 (terdekomposisi pada 170°C). Analisis IR danUV/Vis pada K1 dan K2 menunjukkan ikatan C-O-M telah terbentuk. Berdasarkan spektrum emisi antara K1dan K2, menunjukkan K2 merupakan senyawa yang lebih berpotensi sebagai OLED daripada K1.Kata kunci : Nikel(II), salisiliden anilin, OLED, MAOS
Co-Authors Bambang Ariwahjoedi Buchari Buchari Bunbun Bundjali Bunbun Bundjali Bunbun Bundjali Bunbun Bundjali Bunbun Bundjali Cynthia Linaya Radiman Cynthia Linaya Radiman Damar Nurwahyu Bima Dian Asfriany Nurfalah Doddy Abdassah Herayati, Herayati I Made ARCANA I Made Arcana I Made Arcana I Putu Parwata Irma Mulyani Irma Mulyani Irma Nuril Maryam Iwan Syahjoko Saputra Khusna Widhyahrini Lucy Arianie M. Taufik Fathaddin M. Taufik Fathaddin, M. Taufik Muhamad Jalil Baari Muhammad Ali Zulfikar Ndruru, Sun Theo Constan Lotebulo Ni Ketut Ketis Nila Tanyela Berghuis Nora Idiawati Novriana Sumarti Nuning Nuraini Nurrahmi Handayani Pertiwi, Annisa Mustika Rani Kurnia Rani Kurnia Rini Setiati RUKMAN HERTADI Sadijah Achmad Sadijah Achmad Santi Nurbaiti Septoratno Siregar Septoratno Siregar Septoratno Siregar Sony Suhandono Sugiatmo Kasmungin Sun Theo Constan Lotebulo Ndruru Sun Theo Constan Lotebulo Ndruru Taufan Marhaendrajana Taufan Marhaendrajana, Taufan Tikarahayu Putri Utin Dewi Pebriyana Utjok W.R Siagian Yana Maolana Syah Yudiansyah Yudiansyah Yuliana, Cut Yulyani Nur Azizah