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All Journal Jurnal Matematika & Sains The Journal of Pure and Applied Chemistry Research Journal of Mathematical and Fundamental Sciences Journal of Engineering and Technological Sciences World Chemical Engineering Journal Biology, Medicine, & Natural Product Chemistry EduChemia: Jurnal Kimia dan Pendidikan PENELITIAN DAN KARYA ILMIAH PROSIDING SEMINAR NASIONAL CENDEKIAWAN Indonesian Journal of Chemistry Prosiding Seminar Nasional Pakar CHEESA: Chemical Engineering Research Articles JURNAL PENELITIAN DAN KARYA ILMIAH LEMBAGA PENELITIAN UNIVERSITAS TRISAKTI Tedc Jurnal Penelitian dan Karya Ilmiah Lembaga Penelitian Universitas Trisakti Bulletin of Chemical Reaction Engineering & Catalysis al Kimiya : Jurnal Ilmu Kimia dan Terapan Scientific Contributions Oil and Gas
Deana Wahyuningrum
Institut Teknologi Bandung
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Synthesis, Characterization, and Micellar Behavior of Amphiphilic Chitosan Bearing Sulfate and Anisaldehyde Imine Groups Herayati Herayati; Deana Wahyuningrum; Damar Nurwahyu Bima; Indah Puspita Sari
Biology, Medicine, & Natural Product Chemistry Vol 14, No 2 (2025)
Publisher : Sunan Kalijaga State Islamic University & Society for Indonesian Biodiversity

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.14421/biomedich.2025.142.905-909

Abstract

Amphiphilic chitosan derivatives bearing sulfate and anisaldehyde imine (anisimine) groups were successfully synthesized and characterized for potential applications as functional biomaterials. The synthesis involved two key steps: (1) sulfation of chitosan using chlorosulfonic acid to introduce O-sulfate groups, and (2) Schiff base formation via reaction with p-anisaldehyde to generate N-anisimine functionalities. Structural modifications were confirmed by Fourier-transform infrared (FTIR) spectroscopy, which showed characteristic absorption bands at ~1250 cm-¹ and ~820 cm-¹ corresponding to O=S=O stretching of sulfate, and a C=N stretch at ~1640 cm-¹ indicating imine formation. Proton nuclear magnetic resonance (1H-NMR) spectra further verified the successful attachment of aromatic protons from p-anisaldehyde and the disappearance of primary amine peaks, confirming imination. The amphiphilic behavior and micelle-forming ability of the N-anisimine-O-sulfated (NAOS) chitosan were evaluated using pyrene as a hydrophobic fluorescent probe for determining the critical micelle concentration (CMC), which was found to be 0.012 mg/mL. The observed low CMC value indicates strong self-assembly capability in aqueous media. These results suggest that NAOS chitosan possesses promising structural and surface-active properties suitable for advanced applications in drug delivery and cosmetic formulations.
Potential Use of Kepok Banana Peel Waste as Raw Material for Carboxymethyl Cellulose for Oil and Gas Drilling Fluid Applications Wastu, Apriandi Rizkina Rangga; Permadi , Asep Kurnia; Wahyuningrum, Deana; Nugrahanti, Asri
Scientific Contributions Oil and Gas Vol 49 No 2 (2026)
Publisher : Testing Center for Oil and Gas LEMIGAS

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.29017/scog.v49i2.2070

Abstract

This research aims to evaluate the potential of kepok banana peel as a raw material for carboxymethyl cellulose synthesis and to assess its effects on the rheological properties and filtration of bentonite-based drilling mud. CMC is synthesized through a process of delignification, bleaching, alkalization, and carboxymethylation. CMC characterization includes alpha cellulose content, degree of substitution, purity, pH, FTIR, SEM, and EDS. The obtained CMC was added in drilling mud at concentrations of 3 g, 6 g, and 9 g, and the resulting mud was tested for mud rheology and filtrate volume. The results showed that the alpha-cellulose content was 91.60%, the degree of substitution was 1.0, and the purity was 88.17%, meeting the SNI CMC grade II standard. The application of CMC increased plastic viscosity (12–14 cP), yield point (19–21 lb/100 ft²), and gel strength (8–13 lb/100 ft² for 10 seconds; 12–17 lb/100 ft² for 10 minutes) as the concentration increased. The filtrate volume decreased from 15 ml to 13 ml/30 minutes, and the mud cake thickness decreased from 0.5 mm to 0.3 mm. The pH value was stable in the range of 9. It was concluded that CMC derived from kepok banana peel has the potential to serve as an environmentally friendly drilling mud additive.
Co-Authors Abdassah, Doddy Asep Kurnia Permadi Asri Nugrahanti, Asri Bambang Ariwahjoedi Buchari Buchari Bunbun Bundjali Cynthia Linaya Radiman Cynthia Linaya Radiman Damar Nurwahyu Bima Dian Asfriany Nurfalah Herayati Herayati Herayati, Herayati I Made Arcana I Made ARCANA I Made Arcana I Putu Parwata Indah Puspita Sari Irma Mulyani Irma Mulyani Irma Nuril Maryam Iwan Syahjoko Saputra Khusna Widhyahrini Lucy Arianie M. Taufik Fathaddin M. Taufik Fathaddin, M. Taufik Muhamad Jalil Baari Muhammad Ali Zulfikar Ndruru, Sun Theo Constan Lotebulo Ni Ketut Ketis Nila Tanyela Berghuis Nora Idiawati Novriana Sumarti Nuning Nuraini Nurrahmi Handayani Pertiwi, Annisa Mustika Rani Kurnia Rini Setiati RUKMAN HERTADI Sadijah Achmad Sadijah Achmad Santi Nurbaiti Septoratno Siregar Septoratno Siregar Septoratno Siregar Sony Suhandono Sugiatmo Kasmungin Sun Theo Constan Lotebulo Ndruru Sun Theo Constan Lotebulo Ndruru Taufan Marhaendrajana Taufan Marhaendrajana, Taufan Tikarahayu Putri Utin Dewi Pebriyana Utjok W.R Siagian Wastu, Apriandi Rizkina Rangga Yana Maolana Syah Yudiansyah Yudiansyah Yuliana, Cut Yulyani Nur Azizah