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All Journal Tunas Geografi Jurnal Teknik Kimia USU Majalah Kulit, Karet, dan Plastik Abdimas Talenta : Jurnal Pengabdian Kepada Masyarakat Chemistry Indonesian Journal of Chemical Research Jurnal Abdimas Madani dan Lestari (JAMALI) Jurnal Teknik Kimia USU Jurnal Green Growth dan Manajemen Lingkungan Sewagati

Hamidah Harahap, Hamidah

Departemen Teknik Kimia, Fakultas Teknik Universitas Sumatera Utara

Author-ID : 489454

Agriculture, Biological Sciences & Forestry Arts Humanities Astronomy Biochemistry, Genetics & Molecular Biology Chemical Engineering, Chemistry & Bioengineering Chemistry Civil Engineering, Building, Construction & Architecture Computer Science & IT Earth & Planetary Sciences Education Energy Engineering Environmental Science Industrial & Manufacturing Engineering Languange, Linguistic, Communication & Media Law, Crime, Criminology & Criminal Justice Materials Science & Nanotechnology Nursing Public Health Social Sciences Other

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PENGARUH SUHU VULKANISASI DAN KOMPOSISI BENTONITE CLAY YANG DIMODIFIKASI DENGAN ALKANOLAMIDA DARI BAHAN BAKU RBDPKO PADA PRODUK LATEKS KARET ALAM Friska Erdiana Tambunan, Hamidah Harahap
Jurnal Teknik Kimia USU Vol 4, No 4 (2015)
Publisher : Universitas Sumatera Utara

The is research aims to determine the effect of vulcanization temperature and composition of bentonite clay as good filler on mechanical properties of natural rubber latex product. In this study, we use bentonite clay as filler and alkanolamide as compatibilizer. The material used in this study are high ammonia latex 60%, curative agents such as sulfur, ZnO, ZDEC, AO, KOH, bentonite clay and alkanolamide. Alkanolamide is synthesized from amidation reaction between Refined Bleached Deodorized Palm Kernel Oil and diethanolamine. The methodology includes pre-vulcanizing natural rubber latex with certain formulation, then vulcanized using dipping method. The variable used in this study is filler loading, from 5, 10, 15, 20, and 25 gram, and vulcanization time 10 minutes. The products were then tested in order to observe its mechanical properties, FTIR characterization, SEM characterization and crosslink density. The results show that the synthesized alkanolamide possess the functional group desired. Alkanolamide modified bentonite clay loading is capable of increasing crosslink density and mechanical properties of the products. Optimum filler loading is reported on 10 gram and optimum vulcanization at 120oC.

PENGARUH AGING PADA KEKUATAN TARIK (TENSILE STRENGTH) FILM LATEKS KARET ALAM BERPENGISI NANOKRISTALIN SELULOSA DAN PENYERASI ALKANOLAMIDA Marfuah Lubis; Nuim Hayat; Hamidah Harahap
Jurnal Teknik Kimia USU Vol 5, No 2 (2016)
Publisher : Universitas Sumatera Utara

Nanocrystalline cellulose is nano sized filler with high crystallinity and obtanained by hydrolysis of alpha cellulose from sugarcane bagasse. Tensile test of natural rubber latex film filled nanocrystalline cellulose and alkanolamide as compatibilizer after aging treatment have been done. Natural rubber latex films were prepared by coagulant dipping method and followed by vulcanization process at temperature 100 oC and 20 minutes. Aging treatment of natural rubber latex films have done at temperature 70 oC for 24 hours. Tensile test result of natural rubber latex filled nanocrystalline cellulose showed the tensile strength value of aged natural rubber latex film were lower than unaged one. However, tensile strength value of aged natural rubber latex film filled nanocrystalline cellulose modified alkanolamide were higher than unaged film.

PEMANFAATAN GLISERIN DARI RESIDU GLISERIN SEBAGAI PLASTICIZER UNTUK PEMBUATAN BIOPLASTIK DENGAN BAHAN BAKU PATI BONGGOL PISANG KEPOK Azaria Robiana, M. Yashin Nahar, Hamidah Harahap
Jurnal Teknik Kimia USU Vol 5, No 4 (2016)
Publisher : Universitas Sumatera Utara

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.32734/jutek.v5i4.15193

Glycerin residue is waste oleochemical industry that still contain glycerin. To produce quality and maximum quantity of glycerin, then research the effect of pH acidification using phosphoric acid. Glycerin analysis includes the analysis of pH, Fatty Acid and Ester (FAE), and analysis of the levels of glycerin. The maximum yield obtained at pH acidification 2 is grading 91,60% glycerin and Fatty Acid and Ester (FAE) 3,63 meq/100 g. Glycerin obtained is used as a plasticizer in the manufacture of bioplastics. Manufacture of bioplastics using the method of pouring a solution with varying concentrations of starch banana weevil (5% w/v and 7% w/v), variations of the addition of glycerin (1 ml, 3 ml, 5 ml and 7 ml), and a variety of gelatinization temperature (60°C, 70°C, and 80°C). Analysis of bioplastics include FTIR testing, tensile strength that is supported by SEM analysis. The results obtained in the analysis of FTIR does not form a new cluster on bioplastics starch banana weevil, but only a shift in the recharge area only, it is due to the addition of O-H groups originating from water molecules that enter the polysaccharide through a mechanism gelatinitation that generates interaction hydrogen bonding strengthened. The maximum tensile strength of bioplastics produced at a concentration of starch 7% w/v, 1 ml glycerine and gelatinization temperature of 80°C is 3,430 MPa. While the tensile strength bioplastic decreased with increasing glycerin which can be shown from the results of SEM where there is a crack, indentations and lumps of starch insoluble.

PENGARUH PERLAKUAN LEACHING TERHADAP SIFAT MEKANIK FILM LATEKS KARET ALAM BERPENGISI SELULOSA MIKROKRISTAL DARI AMPAS TEBU Rismadhani Elita, Rojiyatul Ikhwani Lubis, Hamidah Harahap
Jurnal Teknik Kimia USU Vol 5, No 4 (2016)
Publisher : Universitas Sumatera Utara

Leaching process is one of many factors to raise up the mechanical properties of latex products. Studies on the effect of leaching on film natural rubber latex with the filler microcrystalline cellulose from bagasse with alkanolamide using different temperatures and times vulcanization has been done to produce the better mechanical properties such as strenght tensile and elongation at break. Filming of natural rubber latex is done by coagulants dyeing techniques. The study started with the process of pre-vulcanised natural rubber latex at 70 °C with a loading filler by 0 phr, 5 phr, 10 phr and 15 phr and followed by a vulcanization process at a temperature of 100 °C and 150 °C for 10 minutes and 20 minutes. The film result will be have leaching treatment using a solution of water and ammonia 1%. Test results of tensile strength of natural rubber latex film howed that the tensile strength of natural rubber latex film with microcrystalline cellulose as filler and alkanolamides after leaching less than the tensile strength of natural rubber lateks film before leaching

PENGARUH BIODEGRADASI DENGAN TEKNIK PENANAMAN TERHADAP PRODUK LATEKS KARET ALAM BERPENGISI TEPUNG KULIT PISANG YANG DIPUTIHKAN DENGAN HIDROGEN PEROKSIDA Erick Kamil; Emelya Khoesoema; Hamidah Harahap
Jurnal Teknik Kimia USU Vol. 1 No. 2 (2012): Jurnal Teknik Kimia USU
Publisher : Talenta Publisher (Universitas Sumatera Utara)

Natural rubber latex products filled with bleached banana skin powder were identified by burying samples in soil. Soil burial was carried out by adding NPK fertilizer and without fertilizer. One of the tests which was carried out was weight loss calculation. Weight loss calculation showed that natural rubber latex products filled with bleached banana skin powder biodegraded faster than natural rubber latex products without filler. The addition of fertilizer also contributed to biodegradability of samples. The other test was FTIR (Fourier Transform Infrared Spectroscopy) test. The results of FTIR test showed there were structure changes in natural rubber latex which indicated natural rubber latex had been biodegraded.

PENGARUH PENCUACAAN ALAMI TERHADAP PRODUK LATEKS KARET ALAM BERPENGISI TEPUNG KULIT PISANG YANG DIPUTIHKAN DENGAN HIDROGEN PEROKSIDA Emelya Khoesoema; Erick Kamil; Hamidah Harahap
Jurnal Teknik Kimia USU Vol. 1 No. 2 (2012): Jurnal Teknik Kimia USU
Publisher : Talenta Publisher (Universitas Sumatera Utara)

The effect of exposing bleached banana skin powder-filled natural rubber products to sun light and weather with variation of bleached banana skin powder filler loading. Banana skin powder was dried and bleached with hydrogen peroxide and made into disperse system. Natural rubber latex was compounded with bleached banana skin powder with filler loading of 0 to 20 phr (per hundred rubber). Natural rubber latex products, which were produced, were hung in air and exposed to sun light and weather. The degradation of bleached banana skin powder-filled natural rubber products were evaluated by calculating weight loss of samples and performing Fourier transform infrared spectroscopy (FTIR) test. Natural rubber latex lost weight after exposure to sun light and weather from 1 to 16 weeks due to photo-oxidation process.

KEMAMPUAN ADSORBEN LIMBAH LATEKS KARET ALAM TERHADAP MINYAK PELUMAS DALAM AIR Edward Tandy; Ismail Fahmi Hasibuan; Hamidah Harahap
Jurnal Teknik Kimia USU Vol. 1 No. 2 (2012): Jurnal Teknik Kimia USU
Publisher : Talenta Publisher (Universitas Sumatera Utara)

Natural rubber latex waste usually throw away to be unused materials and caused environment issue. One of the ways to handle this environment issue by using natural rubber latex waste as oil adsorbent. Natural rubber latex waste also had oleophilic and hydrophobic properties that are suitable to being used as oil adsorbent. In this research, researchers found out adsorption capacity of natural rubber latex waste to oil and oil from water, also the characteristics of it’s adsorption with Langmuir and Freundlich isoterm adsorption model. The adsorption characteristics of lubricant oil from water with natural rubber latex waste more fitted well with Langmuir isotherm equation model and the maximum adsorption ability of lubricant oil from water with natural rubber latex waste also significantly increased with the contact time till reached the equilibrium. The results of this study concluded that natural rubber latex waste had a great adsorption capacity and suitabled for being used as oil adsorbent.

PEMANFAATAN LIMBAH LATEKS KARET ALAM DENGAN PENGISI BUBUK PELEPAH PISANG SEBAGAI ADSORBEN MINYAK Ismail Fahmi Hasibuan; Edward Tandy; Hamidah Harahap
Jurnal Teknik Kimia USU Vol. 1 No. 2 (2012): Jurnal Teknik Kimia USU
Publisher : Talenta Publisher (Universitas Sumatera Utara)

The use of waste of natural rubber latex with banana sheats powder filler to serve as a more useful product that is used as adsorbent of oil. The process begins with drying the adsorbent manufacture banana and polished up to 100 mesh size. Then the banana powder mixed with waste latex with variations of 10 and 20% (w / w). The analysis of the ability of the adsorbent adsorption isotherms using the Langmuir equation and Freundlich isotherm equation. Research carried out by the batch process and the use of lubricating oil as the adsorbate. The results obtained showed the addition of banana powder as filler waste adsorbent adsorption of latex increases the ability of the oil adsorbent. The conclusion of the analysis showed an increase in the number of characteristics adsroben banana powder can enhance the adsorption of adsorbent.

PENGARUH WAKTU SIMPAN FILM PLASTIK BIODEGRADASI DARI PATI KULIT SINGKONG TERHADAP SIFAT MEKANIKALNYA Fauzi Akbar; Zulisma Anita; Hamidah Harahap
Jurnal Teknik Kimia USU Vol. 2 No. 2 (2013): Jurnal Teknik Kimia USU
Publisher : Talenta Publisher (Universitas Sumatera Utara)

Biodegradable plastics are plastics that will decompose in nature with the help of microorganisms. The use of starch as the main material of plastic manufacturing has great potential because in Indonesia there are different starch crops. To obtain bioplastics, starch is added to the plasticizer glycerol, in order to obtain a more flexible plastic and elastic. This study reviews the use of cassava starch and glycerol skin as a base for the manufacture of biodegradable plastics. The purpose of this research is to know the effect of storage time on the mechanical properties of plastic film biodegradation of starch cassava peel. The results obtained in the form of a thin sheet plastic film that have been tested mechanical properties such as tensile strength, elongation at break, and elasticity. Mechanical properties of plastic films will decrease every week due to the absorption of moisture and plasticizer migration occurs in a matrix of plastic films for storage.

PENGARUH PENAMBAHAN GLISEROL TERHADAP SIFAT MEKANIK FILM PLASTIK BIODEGRADASI DARI PATI KULIT SINGKONG Zulisma Anita; Fauzi Akbar; Hamidah Harahap
Jurnal Teknik Kimia USU Vol. 2 No. 2 (2013): Jurnal Teknik Kimia USU
Publisher : Talenta Publisher (Universitas Sumatera Utara)

Biodegradable plastics are plastics that will decompose in nature with the help of microorganisms. The use of starch as the main material of plastic manufacturing has great potential because in Indonesia there are different starch crops. To obtain bioplastics, starch is added to the glycerol, in order to obtain a more flexible plastic and elastic. This study reviews the use of cassava starch and glycerol skin asa base for the manufacture of biodegradable plastics. The purpose of this research is to know the effect of adding glycerol in the process of making biodegradable plastic from cassava peel waste. In this research, the study of bioplastic manufacturing mixed starch with glycerol as a plastisizer to do variations of the glycerol. The results obtained in the form of a thin sheet of plastic (plastic film) that have been tested mechanical properties obtained optimum data variables namely cassava starch composition 3,5%, and the power og pull 0,02122Mpa, and plastic film storage time for 14 days.

Co-Authors Adrian Hartanto Adrian Hartanto, Adrian Al Fath, Muhammad Thoriq Amir Husin, Amir Ansari, Wan Rizki Aththorick, T Alief Ayuni Yustira Azaria Robiana Bangun, Vega Valentine Barus, Alexander Ternala Batu Bara, Fachreza Amri Dalimunthe, Nisaul Fadilah Edward Tandy Elmer Surya Elmer Surya, Elmer Emelya Khoesoema Erick Kamil Fadhila Fadhila fahmi, Aliyah - Fauzi Akbar Friska Erdiana Tambunan Fujian Junaidi, Ilhamdi Harfansah Nst, Azwin Ida Ayu Putu Sri Widnyani Indra Jaya PAndia, Indra Jaya Indra Surya, Indra Iriani Iriani Ismail Fahmi Hasibuan Kadreni, Emilia Kelvin Hadinatan Kelvin Hadinatan, Kelvin M. Yashin Nahar Marfuah Lubis Marfuah Lubis Muhammad Hendra S Ginting Mukhlis Mukhlis Mulia, Ahmad Perwira Nasution, Halimatuddahliana Nuim Hayat Nuim Hayat Nurdin, Ahmad Pratama, Muhammad A. Renita Manurung Rismadhani Elita Rizky Dharmawan Rojiyatul Ikhwani Lubis Said Muzambiq Satriaji Sudigdo Supriharti, Denny Wahyu, Evita Zuhrina Masyithah Zulhaji Sam, Taufik Zulisma Anita

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