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All Journal KOVALEN: Jurnal Riset Kimia Jurnal Penelitian Sains Indonesian Journal of Pure and Applied Chemistry SPIN: Jurnal Kimia & Pendidikan Kimia CHEDS: Journal of Chemistry, Education, and Science Jurna Beta Kimia
Widiyanto, Holisha
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Biochemistry, Genetics & Molecular Biology Chemical Engineering, Chemistry & Bioengineering Chemistry Education Materials Science & Nanotechnology Mathematics Physics

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Skrining Fitokimia dan Aktivitas Antioksidan Ekstrak Metanol Biji Buah Pare (Momordica charantia L.) Sriwijayanti, Sriwijayanti; Situmeang, Boima; Yulianti, Nani; Susvira, Dian; Widiyanto, Holisha
Jurnal Beta Kimia Vol 4 No 1 (2024): Volume 4, Nomor 1: Mei 2024
Publisher : Universitas Nusa Cendana

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.35508/jbk.v4i1.15487

Abstract

Antioksidan merupakan senyawa yang dapat merangkat radikal bebas. Salah satu tanaman yang diduga dapat merangkat senyawa radikal bebas adalah biji buah pare (Momordica charantia L.). Masyarakat telah menggunakan pare sebagai makanan sehari-hari dan juga telah lama dipercaya sebagai obat tradisional untuk mengobati berbagai macam penyakit. Tujuan dari penelitian ini adalah uji skrining fitokimia dan uji aktivitas antioksidan ekstrak metanol biji buah pare. Ekstraksi dilakukan dengan menggunakan metode maserasi. Uji skrining fitokimia dilakukan dengan menggunakan berbagai reagent kimia untuk analisis senyawa golongan alkaloid, fenoli, flavonoid, tannin, triterpenoid dan steroid. Uji Aktivitas antioksidan dengan menggunakan metode DPPH. Hasil uji skrining fitokimia didapatkan bahwa ekstrak metanol biji buah pare positif mengandung senyawa golongan alkaloid, flavonoid, fenolik, triterpenoid, steroid dan tanin. Hasil uji aktivitas antioksidan didapatkan nilai IC50 sebesar 137,99 ppm yang termasuk dalam kategori sedang.
ETHANOL EXTRACT OF MATOA (Pometia pinnata) AS NATURAL ANTIOXIDANT TO INHIBIT OXIDATION REACTION OF CRUDE PALM OIL: EKSTRAK ETANOL DAUN MATOA (Pometia pinnata) SEBAGAI ANTIOKSIDAN ALAMI UNTUK MENGHAMBAT REAKSI OKSIDASI PADA CRUDE PALM OIL Sriwijayanti; Hidayatullah, Ryan; Musa, Weny JA; Bialangi, Nurhayati; Situmeang, Boima; Widiyanto, Holisha; Lailatussholihah, Isna
SPIN JURNAL KIMIA & PENDIDIKAN KIMIA Vol. 6 No. 1 (2024): Januari - Juni 2024
Publisher : UIN Mataram

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.20414/spin.v6i1.9797

Abstract

Indonesia is the 2nd largest country in the world in terms of palm oil production. The demand for Crude Palm Oil increases every year. For this reason, Indonesia is expected to be able to compete at the international industry level in producing palm oil, with the aim of being able to produce good quality palm oil among industries in other countries. The problem that often occurs in CPO factories is a decrease in the quality of CPO caused by an increase in Free Fatty Acid (FFA) levels and Peroxide Numbers. Antioxidants are substances that can delay or prevent the occurrence of free radical anti-oxidation reactions in the oxidation of fats or oils. Natural antioxidants are antioxidants that are obtained directly from nature. Natural antioxidants are antioxidants that are obtained directly from nature. One of them is the leaf of the matoa plant (Pometia pinnata). Based on the results of this study, the antioxidants of the ethanol extract of the matoa plant can reduce levels of FFA and peroxide numbers depending on the length of time the antioxidant mixture is given to CPO. In this study, a decrease in FFA levels and peroxide numbers was obtained from samples on day - 10 with the addition of 5000 ppm antioxidants, namely 2.71%. while the peroxide number is 0.83%.
Optimalisasi Limbah Serbuk Gergaji Kayu Jati (Tectona grandis L.f) Sebagai Adsorben Logam Berat Kobalt (Co) dengan Metode Aktivasi Kimia: Optimization of Teak Wood Sawdust Waste (Tectona grandis L.f) as Heavy Metal Adsorbent of Cobalt (Co) by Chemical Activation Method Faradin, Faradin; Muharti, Asti; Dinafa, Nazwa Jinanti; Widiyanto, Holisha
KOVALEN: Jurnal Riset Kimia Vol. 10 No. 2 (2024): August Edition
Publisher : Chemistry Department, Mathematics and Natural Science Faculty, Tadulako University

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.22487/kovalen.2024.v10.i2.16629

Abstract

Teak wood (Tectona grandis L.f.), a high-quality wood commonly used in Indonesia, specifically in the Cilegon area, has the potential to be used as an alternative to reduce environmental pollution. This research aimed to test teak wood sawdust waste as an adsorbent for cobalt heavy metal, create activated charcoal from the sawdust waste for the same purpose, and determine the optimal conditions for treatment with and without chemical activation. Industrial waste samples were found to contain 50.7 ppm of cobalt metal through ICPS testing. Activated chemical adsorption, without activation and with industrial wastewater mixture, resulted in a decrease in cobalt metal concentration by 78.2% or 11.08 ppm. The optimal conditions for activated chemical adsorption were found at a pH of 5, an adsorbent mass of 600 mg, and a time of 40 minutes, resulting in decreases of 60.9% (21.2751 ppm), 71% (15.7821 ppm) and 67.7% (17.5812 ppm), respectively. The results show that teak wood sawdust waste can effectively adsorb cobalt heavy metal, providing a potential solution for industrial wastewater treatment.
Efektivitas Perendaman Larutan Nanas Queen Victoria sebagai Pereduksi Logam Fe pada Kerang Hijau (Perna viridis) Widiyanto, Holisha; Julianti, Julianti; Sriwijayanti, Sriwijayanti; Sari, Puspita; Situmeang, Boima; Susvira, Dian
Jurnal Beta Kimia Vol 4 No 2 (2024): Volume 4, Nomor 2: November 2024
Publisher : Universitas Nusa Cendana

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.35508/jbk.v4i2.18673

Abstract

Excessive Fe heavy metal contamination cause health problems for humans. One of the marine biota that is susceptible to heavy metal contamination is green mussels. Green mussels (Perna viridis) are a food that is very often consumed by humans. This Fe metal which derived with materials that are chelating agents such as citric acid, one of the fruits that contain citric acid is the Queen Victoria pineapple. The research aims to determine the effectiveness of soaking Queen Victoria pineapple solution in reduces Fe metal in green mussels. The pineapple solution immersion test was carried out with varying concentrations of 25, 50 and 75% with soaking times of 15, 30 and 45 minutes which were analyzed using inductively coupled plasma (ICP). The highest reduction results were at a concentration of 25% with a soaking time of 30 minutes, amounting to 60.58%.
Pemanfaatan Ekstrak Kulit Batang Kesambi (Schleichera oleosa) dalam Sintesis dan Karakterisasi Nanopartikel Perak dengan FTIR Susvira, Dian; Akbar, Muhammad; Situmeang, Boima; Widiyanto, Holisha
CHEDS: Journal of Chemistry, Education, and Science Vol 9, No 1 (2025)
Publisher : Universitas Islam Sumatera Utara

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.30743/cheds.v9i1.11263

Abstract

Penelitian ini bertujuan untuk mensintesis dan mengkarakterisasi nanopartikel perak menggunakan ekstrak kulit kayu kesambi serta menentukan gugus fungsi dalam ekstrak yang berperan sebagai bioreduktor. Ekstraksi kulit kayu kesambi dilakukan dengan metode maserasi menggunakan pelarut etanol. Pembentukan nanopartikel perak dilakukan dengan menambahkan ekstrak kulit kayu kesambi 4% ke dalam larutan AgNO₃ 0,01 M. Nanopartikel disintesis dengan tiga perbandingan yang berbeda, yaitu: 1:3, 1:5, dan 1:7. Analisis instrumental menggunakan Spektrofotometer dan FTIR. Absorbansi maksimum dari analisis spektrofotometer UV-Vis untuk sampel dengan perbandingan 1:3, 1:5, dan 1:7 diamati pada panjang gelombang 440 nm. Nilai absorbansi tertinggi diperoleh pada perbandingan 1:3. Spektrum FTIR nanopartikel yang berasal dari ekstrak kulit kayu kesambi menunjukkan puncak yang lebar dan kuat pada bilangan gelombang 3385 cm⁻¹, yang menunjukkan adanya vibrasi peregangan OH pada senyawa fenolik, yang berfungsi sebagai agen pereduksi dalam sintesis nanopartikel perak.
Perbandingan Aktivitas Antioksidan Ekstrak Etil asetat dan Metanol Daun Tumbuhan Matoa (Pometia pinnata) Situmeang, Boima; Musa, Weny JA; Mulyadi, Agus; Ibrahim, Agus Malik; Widiyanto, Holisha; Bialangi, Nurhayati
Jurnal Penelitian Sains Vol 26, No 1 (2024)
Publisher : Faculty of Mathtmatics and Natural Sciences

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.56064/jps.v26i1.919

Abstract

Matoa (Pometia pinnata) is a plant from the Sapindaceae family that is widely distributed throughout the Asia-Pacific region, including Indonesia, Malaysia, Thailand, and Sri Lanka. In Indonesia, the Matoa plant is commonly found in Java, Sumatra, and Papua. Empirically, the leaves of the Matoa plant have been utilized by the community as a traditional remedy for treating hypertension, fever, and diarrhea. The aim of this study was to test the antioxidant activity of ethyl acetate extract and methanol extract of Matoa leaves. Extraction was performed using the maceration method. The antioxidant activity was evaluated using UV-Visible spectroscopy. The free radical used was DPPH at a concentration of 50 ppm. The absorbance was measured at a wavelength of 517 nm. The antioxidant activity of the ethyl acetate extract of Matoa leaves was 38.87 ppm and 37.73 ppm. The antioxidant activity of the methanol extract of Matoa leaves was 27.99 ppm and 33.25 ppm. Based on the antioxidant activity values, both the ethyl acetate and methanol extracts of Matoa leaves have the potential as a source of natural antioxidants. 
Analysis of Total Polyhenolic Content and Antioxidant Activity from n-hexane, Ethyl acetate and Ethanol Extract of Kitolod (Hipobbroma longiflora) Leaf Situmeang, Boima; Faradin, Faradin; Susvira, Dian; Bialangi, Nurhayati; Widiyanto, Holisha; Yulianti, Nani; Jinanti, Nazwa
Jurnal Penelitian Sains Vol 27, No 2 (2025)
Publisher : Faculty of Mathtmatics and Natural Sciences

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.56064/jps.v27i2.1182

Abstract

Isotoma longiflora, commonly known as Kitolod, has been traditionally used as a medicinal plant for treating various ailments. This study aims to extract Kitolod leaves using three different solvents with varying polarities: n-hexane (non-polar), ethyl acetate (semi-polar), and ethanol (polar). The total phenolic content, total flavonoid content, and antioxidant activity were analyzed using a spectrophotometer. The trends observed in both TFC and TPC results indicate that ethyl acetate is the most effective solvent for extracting bioactive compounds from Kitolod leaves. The ethyl acetate extract of Kitolod leaves exhibited the highest antioxidant activity (150.542 ± 3.917 ppm), followed by the ethanol (157.235±0.858 ppm) and n-hexane (217.345 ± 1.749 ppm) extracts. This suggests that ethyl acetate is the most effective solvent for extracting bioactive compounds with antioxidant properties from Kitolod leaves.
Penurunan Logam Fe dan Co Pada Kerang Hijau (Perna viridis) dengan Metode Perendaman Larutan Belimbing Wuluh: Reduction Fe and Co Metals in Green Mussels (Perna viridis) by Soaking in Starfruit Solution Widiyanto, Holisha; Asad, Hafidz Al; Sriwijayanti; Susvira, Dian; Situmeang, Boima
KOVALEN: Jurnal Riset Kimia Vol. 9 No. 3 (2023): December Edition
Publisher : Chemistry Department, Mathematics and Natural Science Faculty, Tadulako University

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.22487/kovalen.2023.v9.i3.16586

Abstract

Green mussels with the Latin name Perna viridis are an animal that lives in the ocean and is a type of shellfish that is widely consumed by the public. Along with time, the emergence of factories that can pollute the oceans can cause contamination of marine life in it, one of the pollutants is the heavy metals of Fe and Co. The accumulation of heavy metals Fe and Co in green mussels can be toxic to people who consume them. This study aims to determine the concentration of heavy metals Fe and Co in green mussels before and after immersion in starfruit solution. Tests for immersion of the starfruit solution were carried out at 15, 30, and 45 minutes, then the destruction results were analyzed using inductively coupled plasma (ICP) with the calibration curve method. The Fe content in the green mussel sample before treatment was 2.946 mg/kg and the Co content in the green mussel sample before treatment was 2.6081 mg/kg. After soaking in starfruit solution for 15, 30, and 45 minutes, the Fe metal was 1.572 mg/kg, 1.275 mg/kg, and 1.035 mg/kg and the Co metal was 1.572 mg/kg, 1.275 mg/kg, and 0.683mg/kg. Research of immersing starfruit solution with soaking for 15, 30, and 45 minutes is effective in reducing levels of heavy metals Fe and Co in green mussels. The highest reduction was observed during a 45-minute immersion, with a decrease of 64.87% for Fe and 73.81% for Co, respectively.
PENGARUH PENAMBAHAN KOAGULAN BIJI KELOR TERHADAP PENURUNAN KADAR LOGAM KROMIUM (Cr), MANGAN (Mn), DAN TIMBAL (Pb) MENGGUNAKAN ICP-OES (THE ADDITION EFFECT OF KELOR SEEDS COAGULANT ON THE DECREASING OF CHROMIUM (Cr), MANGANESE (Mn), AND LEAD (Pb) LEVELS USING ICP-OES) Susvira, Dian; Ramadhan, Muhammad Bagus; Susparini, Ninik Triayu; Situmeang, Boima; Widiyanto, Holisha; Bialangi, Nurhayati; Musa, Weny JA
Indonesian Journal of Pure and Applied Chemistry Vol 7, No 1 (2024)
Publisher : Tanjungpura University

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.26418/indonesian.v7i1.63599

Abstract

Electroplating process has a negative effect in form metal ions waste. Today, industrial wastewater treatment widely using aluminum sulfate or alum as synthetic coagulants, although hazardous and expensive. This study was conducted to discover the activity of Moringa seeds (Moringa oleifera) as natural coagulants to substitute synthetic coagulants. Trapped metal ions detected by ICP-OES. The results showed that moringa seed coagulants could reduce 53% Cr, 64.56% Mn, and 92.89% Pb in the addition of 15 grams of moringa seed coagulants.
Co-Authors Asad, Hafidz Al Dinafa, Nazwa Jinanti Faradin, Faradin Hidayatullah, Ryan Ibrahim, Agus Malik Jinanti, Nazwa Julianti Julianti, Julianti Lailatussholihah, Isna Muhammad Akbar Muharti, Asti Mulyadi, Agus Nani Yulianti Ninik Triayu Susparini, Ninik Triayu Nurhayati Bialangi Puspita Sari Ramadhan, Muhammad Bagus Situmeang, Boima Sriwijayanti Sriwijayanti, Sriwijayanti Susvira, Dian