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INDONESIA
JURNAL ATOMIK
Published by Universitas Mulawarman
ISSN : 25490052     EISSN : 25490052     DOI : -
Core Subject : Science, Social, Engineering,
Biochemistry, Genetics & Molecular Biology Chemical Engineering, Chemistry & Bioengineering Chemistry Energy Environmental Science
Jurnal Atomik (JA) is published twice a year (March and August) by Department of Chemistry, Faculty of Mathematics and Natural Sciences, Mulawarman University. Jurnal Atomik is a media for graduate students of Department of Chemistry to publish their research articles in Chemistry field including Analytical Chemistry, Inorganic Chemistry, Physical Chemistry, Organic Chemistry, and Biochemistry. The research articles that be submitted to Jurnal Atomik have to be approved by Editorial Board and in accordance with the rules of writing approved by Editor of Jurnal Atomik.
Arjuna Subject : -
Articles 12 Documents
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Search results for , issue "Vol 5 No 2 (2020)" : 12 Documents clear
RELATIONSHIP OF LOW BIRTH WEIGHT, NUTRITIONAL STATUS AND EXCLUSIVE BREAST-FEEDING WITH ARI IN INFANTS AGED 6–23 MONTHS IN KARANG ASAM PUBLIC HEALTH CENTER, SAMARINDA CITY IN 2018 Magdaleni, Agustina Rahayu; Irawan, Dimas Bagus; Sukemi, Sayidi
JURNAL ATOMIK Vol 5 No 2 (2020)
Publisher : Jurusan Kimia FMIPA UNMUL

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Abstract

Acute respiratory infection (ARI) is one of the main causes of patient visits (40%–60%) in public health centers from year to year and is always on the list of the 10 most diseases each year in health facilities, such as health centers. Populations susceptible to ARI are children less than two years old who have health problems such as malnutrition, have a history of low birth weight (LBW), do not get exclusive breastfeeding. The aim of this research is to find out the relationship between LBW, nutritional status and exclusive breastfeeding with ARI in infants aged 6–23 months in Karang Asam Public Health Center in 2018. This research is quantitative research with a design cross-sectional. The study was conducted on 87 samples, namely toddlers aged 6–23 months who visited and registered at Karang Asam Public Health Center. The sample was taken by accidental sampling. Bivariate analysis using the Chi-Square test showed a significant correlation between nutritional status and ARI in infants aged 6–23 months (0.026) and between exclusive breastfeeding and ARI in infants aged 6–23 months (0.005). Whereas there was no association between LBW and ARI in infants aged 6–23 months at Karang Asam Public Health Center in 2018 (0.078). It can be concluded that there are significant relationships between nutritional status and exclusive breastfeeding with ARI in infants aged 6–23 months. In contrast to LBW, there is no association between LBW and ARI in infants aged 6–23 months in Karang Asam Public Health Center in 2018
ENDOPHYTIC BACTERIA SCREENING FROM THE LEAVES OF OKRA (Abelmoschus esculentus L. Moench) WHICH PRODUCED LIPASE Utami, Nanda Putri; Astuti, Winni; Kartika, Rudi
JURNAL ATOMIK Vol 5 No 2 (2020)
Publisher : Jurusan Kimia FMIPA UNMUL

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Abstract

Endophytic bacteria found in plant tissues can produce enzymes, one of which is lipase. The purpose of this study was to screening endophytic bacteria from the leaves of Okra (Abelmoschus esculentus L. Moench) which produced lipases. The method used in this study is screening with media nutrient agar (NA) containing Rhodamine B and olive oil. The results showed that 4 of bacterial isolates (D1, D2, D3 and D4) from 14 endophytic bacterial isolates had lipase activity. The crude lipase extract was quantitatively tested for lipase activity by the titrimetry method. The highest lipase activity was shown by isolates with a D1 code of 1.50 U/mL.
SYNTHESIS OF ETHYLENEDIAMIDE FROM METHYL ESTER OIL ARABICA COFFEE SEEDS (Coffea arabica. L) WITH ETHYLENEDIAMINE USING NaOCH3 CATALYST BY AMIDATION REACTION Maimunah, Siti; -, Daniel; Saleh, Chairul
JURNAL ATOMIK Vol 5 No 2 (2020)
Publisher : Jurusan Kimia FMIPA UNMUL

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Abstract

Synthesis of ethylenediamide surfactant from coffee bean oil methyl ester (Coffea arabica. L) through an amidation reaction. The synthesis process that has been carried out includes extraction, esterification and amidation of coffee bean oil content by soxhletation of 15.47% with acid number 3.15 mg KOH/g and ALB 1.58%. Coffee bean oil is converted to methyl ester through esterification and acid number is 1.50 mg KOH/g ALB level drops to 0.75% saponification number of 57.11 mg KOH / g. The most dominant composition of the coffee bean oil methyl ester based on GC-MS analysis was 48.0% methyl oleate. The FT-IR spectrum of methyl ester gives a specific absorption peak C = O ester at wave number 1745 cm-1. Methyl esters are converted to ethylenediamide through an amidation process. The resulting ethylenediamide has an acid number of 9.1 mg KOH/g and a saponification number of 3.39 mg KOH/g. The FT-IR spectrum provides specific absorption peaks for groups C=O at wave number 1639 cm1 and C-N at wave number 3302 cm-1. Ethylenediamide HLB values ​​are practically 12.5495 which includes oil in water (O/W) emulsifier surfactants.
APPLICATION OF UV SPECTROPHOTOMETER AND HPLC ON ANALYSIS OF CAFFEINE CONTENT IN ARABICA AND ROBUSTA COFFEES Prasetyo, Dedy; Sitorus, Saibun; Gunawan, Rahmat
JURNAL ATOMIK Vol 5 No 2 (2020)
Publisher : Jurusan Kimia FMIPA UNMUL

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Abstract

Analysis of caffeine content in Arabica coffee and Robusta coffee using Ultra Violet (UV) spectrophotometers and High Performance Liquid Chromatography (HPLC) was carried out. Coffee samples were soxhleted with 96% ethanol with the rotation variation used, namely 4, 6, 8, 10 and 12. The extract was dissolved in 96% ethanol and tested with a UV spectrophotometer. The results obtained caffeine content in arabica coffee for 4, 6, 8, 10 and 12 rotations are 1.347 mg/L, 1.631 mg/L, 1.953 mg/L, 2.868 mg/L and 3.764 mg/L respectively. While the caffeine content obtained by Robusta coffee for 4, 6, 8, 10 and 12 turns are 1.820 mg/L, 2.258 mg/L, 2.741 mg/L, 3.814 mg/L and 4.781 mg/L, respectively. Caffeine content in Arabica and Robusta coffee were analyzed by HPLC. The results obtained in Arabica coffee are retention time of 5.079 minutes, area of 1265348 and height of 56539 and in Robusta coffee the retention time is 5,083 minutes, the area is 1249273 and the height is 55700.
THE MANUFACTURING OF SILICA GEL FROM BAMBOO LEAF ASH (Dendrocalamus asper (Schult. f) Backer ex Heyne) AND THE APPLICATION FOR ADSORPTION Cd (II) ION -, Yasrin; -, Alimuddin; Panggabean, Aman Sentosa
JURNAL ATOMIK Vol 5 No 2 (2020)
Publisher : Jurusan Kimia FMIPA UNMUL

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Abstract

The research about silica gel manufacturing from bamboo leaf ash (Dendrocalamus asper (Schult.) Backer ex Heyne) and the application for Cd (II) ion adsorption has been done. The adsorption of Cd (II) ion done by some varieties, such as pH, concentration, and contact time. The result of the research showed the optimum pH was 8, the optimum concentration was 4 ppm and the contact time was 60 minutes. The adsorption capacity was 0.388 mg/g and the percentage of recovery was 93.44%.
MODIFICATION OF ADSORBEN SILICA FROM RICE HUSK ASH WITH CHITOSAN TO ADSORPTION ION MANGANESE (TOTAL) Fauzi, Akhmad; -, Alimuddin; Widodo, Nanang Tri
JURNAL ATOMIK Vol 5 No 2 (2020)
Publisher : Jurusan Kimia FMIPA UNMUL

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Abstract

Adsorbent silica from rice husk ash supported by chitosan can be used to adsorb Mn (Total) metal. The adsorbent is regulated by adjusting the composition of 65% silica and 35% chitosan. The characteristics of the silica-chitosan adsorbent and the adsorbent interaction with Mn (Total) are believed to be based on Fourier Transform Infared (FTIR) data. The concentration of Mn (Total) ion after adsorption is determined by Atomic Absorption Spectrophotometer (AAS). The results showed optimum pH at pH 5 percentage adsorption 79.45% and optimum contact time at 60 minutes with adsorption percentage 96.78%, and obtained chitosan-silica adsorption capacity of Mn (Total) ions of 1.0349 mg/g.
PHYTOCHEMICAL TEST AND ANTIBACTERIAL ACTIVITY OF METHANOL EXTRACT OF MENTAWA LEAF (Artocarpus anisophyllus Mig.) Pratama, Wahyu; Saleh, Chairul; Astuti, Winni
JURNAL ATOMIK Vol 5 No 2 (2020)
Publisher : Jurusan Kimia FMIPA UNMUL

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Abstract

Phytochemical test and antibacterial activity of methanol extract of Mentawa leaf (Articarpus anisophyllus Mig.) have been done. The extraction of Mentawa leaf samples was carried out by the maceration method using methanol as a solvent. An antibacterial activity test was carried out using the agar diffusion method. Phytochemical tests results show that methanol extract of Mentawa leaf has secondary metabolites of flavonoid, steroid, triterpenoid, phenolic, and quinone compounds. The antibacterial activity test results obtained MIC values for Salmonella typhi bacteria were 1.25-2.5%, Streptococcus mutans bacteria were 0-0,625%, Streptococcus sobrinus bacteria were 1.25-2.5% and for Propionibacterium acnes bacteria were 0.625-1.25%. Methanol extract of Mentawa leaf has broad-spectrum antibacterial activity.
EFFECT OF TIME VARIATION ON XYLENE USING ACTIVE CARBON FROM WASTE OF BANANA STEM (Musa paradisiaca L) Ashari, Ayu Wanti; -, Alimuddin; Sitorus, Saibun
JURNAL ATOMIK Vol 5 No 2 (2020)
Publisher : Jurusan Kimia FMIPA UNMUL

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Abstract

Test of activated carbon adsorption ability of banana stem waste (Musa paradisiaca L) on xylene has been carried out. In the characterization of activated carbon Scanning Electron Microscopy (SEM) was used to show the morphological differences in activated carbon after activation and before activation while xylene adsorption using a UV spectrophotometer with variations in the time of adsorption. The optimum xylene adsorption time was obtained on the weight of 0.4 gram adsorbent, the concentration of xylene 40 ppm was 45 minutes, the adsorption capacity was 1.772 mg/g.
CORRELATION OF Pb METAL ION LEVELS ON PROTEIN CONCENTRATION IN CRUSH CONSTRUCTION (Gafrarium tumidium) TAKEN IN THE COAST OF BONTANG, EAST KALIMANTAN Corebima, Damianus Develistur; Kartika, Rudi; Hindryawati, Noor
JURNAL ATOMIK Vol 5 No 2 (2020)
Publisher : Jurusan Kimia FMIPA UNMUL

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Research on the correlation of Pb metal ion levels to protein content in crush clams (Gafrarium tumidium) taken at the coast of the East Kalimantan Rhino Estuary has been conducted. This study aims to determine the levels of Pb metal ions and protein levels in blood clams based on the size and location of different samples. Correlation of Pb metal ion levels and protein in blood clams was tested using the Least Square method and Pearson product moment. Analysis of Pb metal ion levels using SSA (Atomic Absorption Spectrophotometer) and protein content analysis using the Kjeldahl method. In this study, the Pb metal ion level was obtained at the public port of Tanjung Limau, PPI Tanjung Limau and beach Lallo Sekangat with an average of 0.7474 mg/L, 0.5513 mg/L, and 0.2804 mg/L respectively. Crush clam protein content at Tanjung Limau, PPI Tanjung Limau and beach Lallo Sekangat with an average of 19.6544%, 14.6902%, and 10.9135% respectively. The correlation of Pb metal levels to protein levels in crush clams (Gafrarium tumidium) was stated positively with coefficient correlation results was strong (r = 0.7910).
THE UTILIZATION OF WANYI SEEDS (Mangifera caesia Jack.) IN MAKING ETHANOL BY ENZYMATIC HYDROLYSIS AND FERMENTATION USING Saccharomyces cerevisiae Arissah, Nur; Sitorus, Saibun; Gunawan, Rahmat
JURNAL ATOMIK Vol 5 No 2 (2020)
Publisher : Jurusan Kimia FMIPA UNMUL

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Abstract

The utilization of wanyi seeds (Mangifera caesia Jack.) in making ethanol by enzymatic hydrolysis and fermentation using Saccharomyces cerevisiae has been carried out. The method used is the hydrolysis of α-amylase and gluco-amylase enzymes, fermentation with time variation and yeast concentration as well as the addition of 0.5% urea nutrition and 0.06% NPK, distillation and gas chromatography. Ethanol content 98.508% at 6 days fermentation with yeast concentration 0.23%.

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