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Reaktor
Published by Universitas Diponegoro
ISSN : 08520798     EISSN : 24075973     DOI : https://doi.org/10.14710/reaktor.xx.x.xx-xx
Core Subject : Science, Engineering,
Chemical Engineering, Chemistry & Bioengineering Control & Systems Engineering Energy Materials Science & Nanotechnology
Reaktor invites contributions of original and novel fundamental research. Reaktor publishes scientific study/ research papers, industrial problem solving related to Chemical Engineering field as well as review papers. The journal presents paper dealing with the topic related to Chemical Engineering including: Transport Phenomena and Chemical Engineering Operating Unit Chemical Reaction Technique, Chemical Kinetics, and Catalysis Designing, Modeling, and Process Optimization Energy and Conversion Technology Thermodynamics Process System Engineering and products Particulate and emulsion technologies Membrane Technology Material Development Food Technology and Bioprocess Waste Treatment Technology
Arjuna Subject : Teknik (semua kategori) - Teknik (Lain-Lain)
Articles 530 Documents
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Numerical Solution Of Electrokinetics Mass Transfer Model For Protein Recovery Through Membrane Electrofilter Syaubari syaubari; S. Nurdin
Reaktor Volume 07 No.2 Desember 2003
Publisher : Dept. of Chemical Engineering, Diponegoro University

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (3098.872 KB) | DOI: 10.14710/reaktor.7.02.66-69

Abstract

Separation based on electrophoresis and electroosmosis (electrokinetics) of binary mixture of proteins (bovine serum albumin-hemoglobin) was studied on a membrane electrofilter. The mixture was separated using ionic polycarbonate membrane with variable studied consist of voltage, current, protein diffusivity, and electrophoresis mobility. Operation parameters were varied to investigate hemoglobin concentration, which pass semi permeable membrane. A model was been derived based on mass transfer principle for the case of unsteady state. For simplification, the model has been modified using Cramer Method with pseudo steady state approach to give the dimentionless form. A program for computer simulation has een written in C/C+ + language. This programming language was shown to have more effective computing ability. Furthermore, using a model and simulation on computer, the result indicates that initial mechanism of electrofilter can also be used to separate and to concentrate protein on their buffer solution.Keywords : electrophoresis, electroosmosis, protein, membrane, electrofilter
DIRECT ETHOXYLATION OF GLYCEROL MONO OLEATE FROM PALM OIL DERIVATE AS A NOVEL NON-IONIC POLYMERIC SURFACTANT Joddy Arya Laksmono; Indri Badria Adilina; Egi Agustian
Reaktor Volume 12, Nomor 2, Desember 2008
Publisher : Dept. of Chemical Engineering, Diponegoro University

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (528.658 KB) | DOI: 10.14710/reaktor.12.2.102-106

Abstract

The work investigates ethoxylation of glycerol mono oleate (GMO) performed in the presence of an alkaline catalyst. Glycerol mono oleate applied was derivated from Indonesian palm oil. The reaction was conducted with variation of Glycerol mono oleate : ethylene oxide ratio, temperature, and catalyst concentration. Forier Transform Infra Red (FTIR) and Nuclear Magnetic Resonance (NMR) analysis showed products with degrees of ethoxylation n=2 and n=3. FTIR analysis of products gave a new peak at 1570 cm-1 supporting that C-O-C bond was formed. New peaks were also observed in 13-C-NMR analysis of run 2 and run 3 with chemical shift of (δ) 61.3385; 61.9108; 62.5117; 63.8566; 66.0982; 72.6127 and 61.2172; 63.2393; 65.9100; 72.5201, respectively. Glycerol mono oleate ethoxylated was yielded and could be useful for a novel non-ionic polymeric surfactant.
Effect of Intermittent Spray Pyrolysis on the Characteristics of Fluorine-Doped Tin Oxide Conductive Glass for Dye Sensitized Solar Cell Isdiriayani Nurdin; Pramujo Widiatmoko; Hary Devianto; Anastasia Yuandy; Rendy Rendy
Reaktor Volume 19 No. 4 December 2019
Publisher : Dept. of Chemical Engineering, Diponegoro University

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (804.925 KB) | DOI: 10.14710/reaktor.19.4.180-186

Abstract

One of dye sensitized solar cell’s (DSSC) component is conductive glass, a transparent glass substrate covered with semiconductor oxide, usually fluorine-doped tin oxide (FTO). An economic and scalable method used to deposit the FTO film is spray pyrolysis. A research conducted by Fukano et al. (2004) showed that introducing intermittence in spray pyrolysis using batch atomizer improves the glass’ characteristics. This research aims to observe the effect of intermittence on spray pyrolysis method using nebulizer. A compressor nebulizer and hotplate were used, where the glass’ surface temperature reached 300oC. Transmittance, conductance, morphology and composition of the glasses produced were analyzed. Deposition time and intermittence were varied. Variation of time were 5; 7.5; 10; 16; and 39 minutes. Deposition time of 7.5 minutes showed the highest figure of merit (FOM) of 7.83×10-3 Ω-1. Intermittence was performed by turning the nebulizer off during deposition, with varying period and amount of intermittence. Periods of intermittence were varied for 10, 20, and 30 seconds, and amounts of intermittence were varied 1, 2, and 3 times. Variation of 3 intermittences at 20 seconds each resulted in the highest FOM of 19.29×10-3 Ω-1. DSSC’s efficiency built using produced conductive glass are 1.9×10-4 % and 5.5×10-4 %.
Prediction Of Solubility Of Solid N-Paraffins In Supercritical Fluids Using Modified Redlich-Kwong Equation Of State Ratnawati Ratnawati
Reaktor Volume 08 No.1 Juni 2004
Publisher : Dept. of Chemical Engineering, Diponegoro University

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (4222.272 KB) | DOI: 10.14710/reaktor.8.1.1-6

Abstract

Three equation of state are used to predict solubilities of solid n-pafaffins in supercritical fluids. The equations are the Redlich-Kwong, the Soave-Redlich-Kwong, and equation proposed by Hartono et.al. (2003; 2004). Both the last two equations were formed by modificating the Redlich-Kwong equqtion of state. With the binary interactions parameter, kif , equals zero, the equations proposed by Hartono et.al. is better than both the Redlich-Kwong and the Soave-Redlich-Kwong equations of state are. Upon optimization with kif as the adjustable parameter, the equation of state proposed by Hartono et.al. is closer to the experimental data than the other equqtions are. For 142 data points of 12 systems the equation proposed by Hartono et. Al. gives the average deviation of 36.6%, while the Redlich-Kwong and the Soave-Redlich-Kwong give 66.7% and 65.8%, respectively.Keywords : equation of state, solubility, supercritical
MODEL KINETIKA REAKSI PEMBENTUKAN POLYOL BERBASIS MINYAK SAWIT La Ifa; Sumarno Sumarno; Susianto Susianto; Mahfud Mahfud
Reaktor Volume 14, Nomor 1, April 2012
Publisher : Dept. of Chemical Engineering, Diponegoro University

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (115.839 KB) | DOI: 10.14710/reaktor.14.1.1-8

Abstract

REACTION KINETIC MODEL OF RBD PALM OIL BASED-POLYOL PRODUCTION. Polyol, a raw material of polyurethane, has successfully been produced from a renewable resource namely RBD palm oil. This polyol was made by firstly adding a peroxyacetic acid formed in situ from H2O2 and CH3COOH with H2SO4 as cataliyst into RBD palm oil to form epoxidized RBD palm oil. The epoxidized palm oil then was added to a mixture of methanol (MeOH), isopropanol (IPA), and H2SO4 for 2 hours at 60oC so that palm oil-based polyol was formed. The main equipment used in this research was a 500 mL three necked flask, equipped with a reflux condeser, thermometer, water bath and magnetic stirrer. The product was analysed using a titration method and Infra Red (IR) Spectroscopy. It was obtained that the produced palm oil-based polyol has a value of hydroxyl number of 150-209 mg KOH/g sample and a viscosity of 740.777 cP. These results are in accordance with other polyol products from other sources. The kinetic of palm oil-based kinetic was studied and the best model of the reaction rate equation was where k’ = 3.399 e-2391.,6/RT.  The unit of  k is L2 mol-2 menit-1 . The average error of the equation is 4,549%.  Polyol, bahan baku polyuretan, telah berhasil dibuat dari bahan baku terbarukan yakni polyol berbasis RBD palm olein. Polyol ini mula-mula dibuat dengan menambahkan asam peroksi asetat yang dibentuk secara in situ dari H2O2 dan CH3COOH dengan katalis H2SO4 kedalam RBD palm olein untuk membentuk RBD palm olein terepoksidasi. RBD palm oil terepoksidasi ditambahkan kedalam campuran metanol (MeOH), isopropanol (IPA) dan sejumlah katalis H2SO4 selama 2 jam pada suhu 60 oC sehingga terbentuk polyol berbasis RBD palm oil. Peralatan utama yang digunakan dalam percobaan pembuatan polyol adalah labu leher tiga 500 mL dilengakapi dengan kondesor reflux, termometer, water bath dan magnetic stirrer. Polyol produk dianalisa bilangan hidroksil dengan cara titrasi dan dianalisis dengan Infra Red (IR) Spectroscopy. Polyol berbasis RBD palm oil yang dihasilkan memiliki bilangan hidroksil 150-209 mg KOH/g sampel dan viskositas 740,777 cP. hasil ini sebanding dengan polyol yang dihasilkan dari sumber minyak yang lain. Kinetika reaksi polyol berbasis RBD palm oil telah dipelajari dan hasil terbaik didekati dengan persamaan laju reaksi yang diperoleh pada penelitian adalah dimana k’ = 3,399 e-23913,6/RT dalam satuan L2 mol-2 menit-1. Kesalahan estimasi rata-rata adalah 4,549%. Kata kunci: model kinetika; RBD palm oil; polyol
Bagian belakang Vol 16 No. 3 September 2016 Widayat, W
Reaktor Volume 16 No.3 September 2016
Publisher : Dept. of Chemical Engineering, Diponegoro University

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (251.711 KB)

Abstract

Bagian belakang yang berisi indeks judul, subyek dan author
The Design of ACE (Aluminum Corrosion and Electrolysis) Reactor and Its Performance to Produce Hydrogen from Beverage Cans Ahmad Zikri; Erlinawati .; Lety Trisnaliani; Daya Wulandari
Reaktor Volume 17 No. 4 Desember 2017
Publisher : Dept. of Chemical Engineering, Diponegoro University

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (450.956 KB) | DOI: 10.14710/reaktor.17.4.210-214

Abstract

AbstractThe reaction of aluminum (Al) with an alkaline solution in producing hydrogen gas has been known for a long time. This aluminum corrosion reaction has a major obstacle in the passivation phenomenon, a formation of aluminum oxide coating on the metal surface that prevents aluminum from collapsing. Integration of electric current to the potassium hydroxide solution could result in electrolysis of water which increases the production of hydrogen. This process was carried out continuously in an ACE (aluminum corrosion and electrolysis) reactor of water. This reactor design enabled to produce hydrogen and oxygen in separating chamber. The use of 10 g of cans, 0.02 M gallium, 12 VDC, and 0.8 M KOH obtained the maximum production rate of hydrogen 162.58 ml/s with a purity of 79.83%. Keywords: aluminum corrosion; hydrogen; water electrolysis
PREPARASI Fe3+/TiO2- MONTMORILLONIT SEBAGAI KATALIS PADA DEGRADASI ZAT WARNA AZO Is Fatimah; Tuty Alawiyah; Iwan Sumarlan
Reaktor Volume 14, No. 4, OKTOBER 2013
Publisher : Dept. of Chemical Engineering, Diponegoro University

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (249.754 KB) | DOI: 10.14710/reaktor.14.4.255-260

Abstract

Dalam penelitian ini dilakukan preparasi material Fe3+/TiO2-Montmorillonit dan uji aktivitasnya sebagai katalis pada degradasi senyawa azo. Keberhasilan preparasi material dipelajari melalui karakterisasi menggunakan X-ray Diffraction, BET surface area analyzer dan Diffuse Reflectance UV-Visible. Peranan katalitik material hasil preparasi pada degradasi senyawa azo: metil jingga(MO) dan metilena biru(MB) dipelajari melalui studi kinetika reaksi dengan mekanisme mirip foto-Fenton (Photo-Fenton like mechanism). Hasil penelitian menunjukkan keberhasilan preparasi material Fe3+/TiO2-Montmorillonit serta tercapainya tujuan penggunaannya sebagai katalis untuk degradasi zat warna azo melalui mekanisme Photo-Fenton like. Simulasi terhadap data kinetika menunjukkan bahwa degradasi kedua zat warna azo dengan katalis hasil preparasi mengikuti  model kinetika Langmuir-Hinshelwood dengan nilai k dan K untuk MO berturut-turut adalah sebesar 8,83x10-7 M/detik dan 328,29 dan untuk MB sebesar 4,56x10-5 M dan 555,60. Nilai konstanta laju reaksi dan konstanta adsorpsi-desorpsi reaksi degradasi kedua zat warna menjelaskan peranan mekanisme interaksi permukaan dalam proses katalisis.
Penghilangan Cemaran Karbon Monoksida Dari Gas Buang Menggunakan Unggun Tetap Tanah Sumarno Sumarno
Reaktor Volume 5 No. 1 Juni 2001
Publisher : Dept. of Chemical Engineering, Diponegoro University

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (3805.119 KB) | DOI: 10.14710/reaktor.5.1.21-26

Abstract

Skala bangku kolom unggun tetap digunakan untuk uji kemampuan menghilangkan karbon monoksida dari gas buang dengan variasi media isian, laju alir gas buang dan tinggi unggun. Efisisiensi penghilangan karbon monoksida rata-rata berkisar 26,5 sampai 98,3 persen pada laju alir 0,2 L/menit, 0,5 L/menit, 0,8 L/menit; tinggi unggun 50 cm dan 75 cm dengan media isian tanah, kompos dan pupuk kandang. Factor pembatas yang menentuakan penghilangan CO dari gas buang dengan unggun tanah adalah adsorpsi CO pada partikel tanah yang lebih lambat disbanding factor oksidasi CO menjadi CO2 secara mikrobiologis.Kata kunci : penghilangan CO, unggun tetap tanah, gas buang
MIGRASI KE SCILAB UNTUK VISUALISASI SERTA PENYELESAIAN MODEL MATEMATIS Setia Budi Sasongko
Reaktor Volume 12, Nomor 1, Juni 2008
Publisher : Dept. of Chemical Engineering, Diponegoro University

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (164.134 KB) | DOI: 10.14710/reaktor.12.1.1-6

Abstract

Perangkat lunak merupakan salah satu komponen yang mutlak diperlukan dalam simulasi komputer. Permasalahan harga menjadi salah satu kendala dalam pengembangan sistem tersebut. Akan tetapi problema tersebut dapat diatasi dengan menggunakan Scilab sebagai “Open Source Software”. Scilab merupakan perangkat lunak berbasis matrik dalam menyelesaian permasalahan matematis dan visualisasi hasilnya.Penyusunan program didasarkan pada model matematis untuk bioreaktor. Validasi hasil dari Scilab dilakukan melalui komparasi hasil visualisasi dengan perangkat lunak Polymath 5 versi pendidikan. Hasil yang diperoleh dari Scilab tidak menunjukkan perbedaan yang signifikan dengan hasil yang diperoleh dengan Polymath 5. Berdasarkan hasil tersebut, perlu dikembangkan lebih lanjut simulasi komputasi dengan menggunakan Scilab.

Page 28 of 53 | Total Record : 530

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