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Reaktor
Published by Universitas Diponegoro
ISSN : 08520798     EISSN : 24075973     DOI : https://doi.org/10.14710/reaktor.xx.x.xx-xx
Core Subject : Science, Engineering,
Chemical Engineering, Chemistry & Bioengineering Control & Systems Engineering Energy Materials Science & Nanotechnology
Reaktor invites contributions of original and novel fundamental research. Reaktor publishes scientific study/ research papers, industrial problem solving related to Chemical Engineering field as well as review papers. The journal presents paper dealing with the topic related to Chemical Engineering including: Transport Phenomena and Chemical Engineering Operating Unit Chemical Reaction Technique, Chemical Kinetics, and Catalysis Designing, Modeling, and Process Optimization Energy and Conversion Technology Thermodynamics Process System Engineering and products Particulate and emulsion technologies Membrane Technology Material Development Food Technology and Bioprocess Waste Treatment Technology
Arjuna Subject : Teknik (semua kategori) - Teknik (Lain-Lain)
Articles 530 Documents
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Removal of COD & NH3 from Produced Water using Modified Horizontal Subsurface Flow Constructed Wetlands (HSCW) Agus Jatnika Effendi; Regi Risman Sandi
Reaktor Volume 18 No. 3 September 2018
Publisher : Dept. of Chemical Engineering, Diponegoro University

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (541.664 KB) | DOI: 10.14710/reaktor.18.03.166-170

Abstract

It is very common that COD and NH3 are found in Produced Water with elevated concentration. One proven technology that is capable in removing organic substances and nutrients, is Horizontal Subsurface Flow Constructed Wetland (HSCW). Based on characterization of produced water from one oil field in Indonesia, it was shown that COD and NH3 were found to exceed the threshold limit stated in Ministry of Environmental Decree no. 19 Year 2010. Modified HSCWs were developed in order to treat produced water containing high concentration of COD and NH3 and allowing anaerobic process to occur in the reactor. The HSCWs were planted by three different species; they were Sagittaria palaefolia (Jasmine Water), Scirpus grossus (Mensiang), and Typha latifolia (Walingi). Organic loading rates (OLRs) to the HSCWs reactor were varied from 7.2 to 72 gr COD/m2.day. It was found that HSCW planted with Typha latifolia had the highest removal efficiency for both COD and NH3 when the OLR was set at 14.4 gr COD/m2.day. Anaerobic bacteria were found in high number indicating that these bacteria involved actively in removing pollutants containing in produced water. However, further microbiology study should be performed in order to determine the role of anaerobic bacteria.
ANALISA PEMANFAATAN KOMPOS SEBAGAI MEDIA BIOCOVER DI TEMPAT PEMROSESAN AKHIR SAMPAH: Studi Kasus Kota Depok, Jawa Barat Gabriel Andari Kristanto; Dwi Rahayu; Evy Novita
Reaktor Volume 15, No.2, OKTOBER 2014
Publisher : Dept. of Chemical Engineering, Diponegoro University

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (605.087 KB) | DOI: 10.14710/reaktor.15.2.117-125

Abstract

High percentage of organic waste in urban areas makes composting as good alternative in waste processing. However, composting has not been effectively used and the result is not optimal. Previous studies found compost can be used as biocover media to reduce methane emission landfill. The objective of the study is to identify the characteristic of produced at temporary waste unit Depok, West Java and the effect of compaction toward the amount of methane removal in the landfill. Before applied as biocover media, compost was characterized followed by maturation process. Study on methane removal efficiency was conducted as batches in four reactors for 35 days with compaction rate varying from 750, 800, 850 dan 900 kg/m3. Composting media used in the research had 80 cm thickness with artificial gas consisting of 50% CH4 dan 50% CO2. Initially, compost did not meet criteria as mature compost based on SNI 19-7030-2004, and as media biocover hence a pre-treatment was needed to improve the quality compost to meet the requirements. Compaction rate of 900 kg/m3has highest elimination capacity of methane i.e. 98,31%±3,6% and 13,98±4,32 g/m3/hour.
Absorpsi Gas SO2 dengan Larutan Ca(OH)2 Dalam Reaktor Berpengaduk Mahfud mahfud; A. Mintarto; A. Indriyaswati
Reaktor Volume 07 No. 1 Juni 2003
Publisher : Dept. of Chemical Engineering, Diponegoro University

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (3750.458 KB) | DOI: 10.14710/reaktor.7.1.22-26

Abstract

Penelitian ini bertujuan untuk mempelajari proses absorbs gas SO2 ke dalam larutan Ca(OH)2 dalam reaktor berpengaduk dan untuk mempelajari pengaruh berbagai kondisi operasi pada proses absorbsi SO2  kedalam larutan Ca(OH)2. Penelitian dilakukan dengan mereaksikan gas SO2 dengan larutan Ca(OH)2 dalam reaktor berpengaduk. Reaktor yang digunakan terbuat dari acrylic dengan kapasitas 1000 ml, diameter 10 cm, tinggi 14 cm, dilengkapi dengan 4 buah bafel, dan sebuah pengaduk dengan impeler dished blade turbin. Gas yang digunakan adalah campuran gas SO2   dan udara. Percobaan dilakukan pada suhu kamar (30 0C)  dan tekanan atmosferik serta laju alir 24. 10-6 m3/s dengan variabel percobaan sebagai berikut : ph larutan awal larutan 10-14, kecepatan putaran  pengaduk 550, 780, 1030 rpm. konsentrasi Ca(OH)2 :0,7-2 gr/liter larutan fraksi gas SO2  masuk 1-3%. Hasil penelitian menujukkan bahwa laju absorbs sedikit meningkat dengan kecepatan putar pengaduk dan meningkat secara signifikan  dengan naiknya konsentrasi gas SO2. Perubahan konsentrasi Ca(OH)2 tidak signifikan terhadap perubahan laju absorbs. Data laju absorbs hasil percobaan dibandingkan dengan 2 macam model. Dan hasil perbandingan ini menunjukkan hasil percobaan lebih mendekati padaa model 2, dimana perpindahan massa sisi cair tidak bias diabaikan dan reaksi terjadi pada film liquid atau dengan kata lain perpindahan massa sisi cair yang mengendalikan proses absorbs, dan dari perbandingan laju absorbs model dan laju absorbs eksperiment didapatkan kesalahan rata-rata ±10%.Kata kunci : absorbs, gas SO2 , larutan Ca(OH)2, reaktor berpengaduk
SINTESIS LIPIDA TERSTRUKTUR DARI ASAM LAURAT DAN GLISEROL DALAM PELARUT ISOOKTANA DENGAN BIOKATALIS LIPASE Candida rugosa Sriyono Poerwanto; Chusnul Hidayat; Supriyadi Supriyadi
Reaktor Volume 13, Nomor 1, Juni 2010
Publisher : Dept. of Chemical Engineering, Diponegoro University

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (262.848 KB) | DOI: 10.14710/reaktor.13.1.44-50

Abstract

Lipida terstruktur (LS) yang mengandung asam lemak rantai medium mempunyai keuntungan untuk kesehatan dan banyak dipelajari kegunaannya untuk keperluan medis, fungsional nutrisi, dan makanan. Dalam penelitian ini dikaji sintesis enzimatik LS rantai medium dari asam laurat dan gliserol menggunakan lipase Candida rugosa. Berbagai pengaruh parameter reaksi seperti konsentrasi enzim, lama reaksi, suhu, penambahan molecular sieve, dan perbandingan molar substrat (mmol asam laurat/mmol gliserol telah dikaji). Hasil yang diperoleh menunjukkan bahwa kondisi terbaik untuk sintesis gliserida rantai medium dicapai pada suhu reaksi 37°C selama 24 jam dengan  jumlah lipase sebanyak 80 mg, penambahan molecular sieve 0,1 mg, dan perbandingan molar substrat asam laurat/gliserol 3:1. Analisa produk reaksi menggunakan kromatografi gas menunjukkan bahwa lipase Candida rugosa dapat menghasilkan gliserida dengan komposisi persentase molar 15,55% monolaurin, 10,29% dilaurin, dan 1,41% trilaurin
DAMPAK RANGKAIAN SEL ELEKTRODA AL-C DALAM ELEKTROKIMIAUNTUK MENDEGRADASI LIMBAH TEKSTIL Ni Made Wiratini; Ngadiran Kartowasono
Reaktor Volume 16 No. 2 Juni 2016
Publisher : Dept. of Chemical Engineering, Diponegoro University

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (348.16 KB) | DOI: 10.14710/reaktor.16.2.65-71

Abstract

Abstract IMPACT OF AL-C ELECTRODE CELL CIRCUIT IN ELECTROCHEMISTRY FOR TEXTILES WASTE DEGRADATION. The purpose of this study was to determine the impact circuit of Al-C electrode cell in electrochemical to degrade textile waste. To achieve these goals, 1) cells that were developed using 3 electrode by varying the electrochemical cell circuit  such as: cell circuit 1(anode: Al-C series, cathode C), cell circuit 2 ( anode: Al-C parallel, cathode C), cell circuit 3(anode: Al-C series, cathode: Al), and cell circuit 4 ( anode: Al-C parallel, cathode: Al); 2) varying the electrode spacing, ie: 3, 6, 9 and 12 cm; and 3) varying the voltage, which is 3, 6, 9, and 13, 5 V. BOD, DO, COD, pH, and absorbance were  measured before and after degradation in every varying cell circuit, electrode spacing, and voltage.  The results showed: black textile waste, odor, COD 2540 mg / L, DO 0 mg / L, BOD 0 mg / L, pH 11, and the absorbance was 0.92. While  best cells circuit is cell circuit 2 (anode: Al-C parallel and c in cathodes), best electrode spacing for processing textile waste is 3 cm, and the best voltage to degrade textile waste is 13.5 V. Key words: degradation, electrochemical, set of cells, textile waste Abstrak Tujuan penelitian ini adalah mengetahui dampak rangkaian sel elektroda Al-C dalam elektrokimia untuk mendegradasi limbah tekstil. Untuk mencapai tujuan tersebut, 1) sel yang dikembangkan menggunakan 3 elektroda dengan memvariasikan rangkaian sel elektrokimia  yaitu: rangkaian 1 (anoda: Al-C seri, katoda C), rangkaian 2(anoda: Al-C paralel, katoda C), rangkaian 3( anoda: Al-C seri, katoda: Al), dan rangkaian 4( anoda: Al-C paralel, katoda: Al); 2) memvariasikan jarak elektroda, yaitu: 3,6, 9, dan 12 cm; dan 3) memvariasikan voltase, yaitu 3, 6, 9, dan 13, 5 V. BOD, DO, COD, pH dan absorbansi diukur sebelum dan sesudah degradasi pada setiap variasi rangkaian sel, jarak, dan voltase. Hasil penelitian menunjukkan: limbah tekstil berwarna hitam, berbau, COD 2540 mg/L, DO 0 mg/L, BOD 0 mg/L, pH 11, dan absorbansi 0,92. Sedangkan rangkaian sel yang paling baik adalah rangkaian sell 2 (anoda: Al-C parallel dan katoda: C), jarak elektroda terbaik untuk pengolahan limbah tekstil adalah 3 cm, dan voltase yang terbaik untuk mendegradasi limbah tekstil 13,5 V. Kata-kata kunci: degradasi, elektrokimia, limbah tekstil,  rangkaian sel
MODEL ADSORPSI LANGMUIR GAS DINITROGEN MONOKSIDA DALAM SISTEM BIOFILTER DENGAN MEDIUM PUPUK KOMPOS Tania Surya Utami; Josia Simanjuntak; Heri Hermansyah; Mohamad Nasikin
Reaktor Volume 13, Nomor 3, Juni 2011
Publisher : Dept. of Chemical Engineering, Diponegoro University

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (911.146 KB) | DOI: 10.14710/reaktor.13.3.172-177

Abstract

 LANGMUIR ADSORPTION MODEL FOR DINITROGEN MONOXIDE IN BIOFILTER SYSTEM USING COMPOST FERTILIZER MEDIUM. Nitrous oxide (N2O) is mostly emitted from various industrial processes and agricultural activities. This gas causes serious environmental problems and is considered as a dangerous pollutant. In the past, traditional control technologies, such as Selective Catalytic Reduction (SCR) and Selective Non-Catalytic Reduction (SNCR), were applied to control N2O emissions in some industries. However, these two processes required high temperatures and the use of catalysts. Economic and technical constraints in SCR and SNCR methods motivated researchers to develop new, cost-effective processes to remove N2O. Biofiltration is an emerging technology that offers a number of advantages over traditional methods of air pollution control. The purpose of this research is to modelise the biofiltration experimental results into the Langmuir adsorption model. This research is conducted in laboratory scale biofilter column, with parameters studied are effect of biofilter length and N2O gas flowrate. The result of the model is simulated into sensitivity analysis. The average Langmuir constant obtained in the model of the research is 16.006 liter/mol. Dinitrogen Monoksida (N2O) merupakan emisi dari proses industri dan kegiatan pertanian. Gas tersebut merupakan gas polutan berbahaya dan menyebabkan masalah lingkungan yang serius. Sebelumnya, teknologi kontrol tradisional seperti Selective Catalytic Reduction (SCR) dan Selective Non-Catalytic Reduction (SNCR) digunakan untuk mengontrol emisi N2O pada kegiatan-kegiatan industri. Akan tetapi, kedua proses ini membutuhkan suhu yang tinggi dan penggunaan katalis. Adanya masalah dari segi ekonomi dan teknis memotivasi peneliti untuk mengembangkan teknologi baru yang lebih murah dan efisien untuk menghilangkan N2O dari gas buangan. Pengolahan N2O secara biologis dalam proses biofiltrasi adalah salah satu alternatif ramah lingkungan yang dapat digunakan dalam pengelolaan emisi industri. Penelitian ini bertujuan untuk menggambarkan hasil biofiltrasi gas N2O dengan medium pupuk kompos dalam bentuk model adsorpsi Langmuir. Penelitian dilakukan dalam kolom biofilter skala laboratorium, dan parameter-parameter yang diteliti adalah pengaruh dari ketinggian biofilter dan laju alir gas N2O. Hasil dari pemodelan kemudian disimulasikan dalam analisis sensitivitas. Nilai konstanta Langmuir rata-rata yang didapatkan dari pemodelan penelitian ini adalah 16,006 liter/mol.
Kinetika Release Mikrokapsul Oleoresin Jahe Merah Jayanudin Jayanudin; R Rochmadi; Meri Yulvianti; Ahmad Imanudin; Tri Rina Sari
Reaktor Volume 16 No.3 September 2016
Publisher : Dept. of Chemical Engineering, Diponegoro University

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (730.468 KB) | DOI: 10.14710/reaktor.16.3.128--140

Abstract

Abstract RELEASE KINETICS OF RED GINGER OLEORESIN MICROCAPSULES. Red ginger oleoresin microcapsule is used to protect the active component of medicine against the negative effect of the environment, thus the microcapsule can be applied in the pharmaceutical industries. Kinetic release is used to determine the rate of red ginger oleoresin microcapsule release in human body system. The models used for this purpose are zero order, first order, Higuchi, and Korsmeyer-Peppas. These models were completed by using graphical method to get the determination coefficient (R2). The aims of this research are to determine the effect of Tripolyphosphate (TPP) concentration towards microcapsule release, to determine the red ginger oleoresin microcapsule kinetic release, and to characterize the morphology and particle sizes of red ginger oleoresin microcapsule using the Scanning Electron Microscopy (SEM). The encapsulation method was started by emulsifying process of chitosan-alginate, with various ratios of Chitosan-Alginate such as 1:2, 1:1, 2:1, and 20 gram red ginger oleoresin, and also the addition of TPP, with various concentrations for as much as 3%, 4 %, and 5%, as the crosslinking agent. The emulsion was forwarded to the spray dryer machine to produce the red ginger oleoresin microcapsule. Then, the microcapsule was treated with the mixture of KH2PO4 and NaOH (pH 6.8) for 1 hour, and sample was taken for every 10 minutes for the dissolution test. The result showed that the increase of TPP concentration will reduce the release velocity of the active compound. Kinetic model with the highest value of R2 was the Korsmeyer-Peppas model. Keywords: alginate; encapsulation; release kinetics; chitosan red ginger oleoresin;   Abstrak Mikrokapsul digunakan untuk melindungi oleoresin jahe merah yang sensitif terhadap pengaruh lingkungan, sehingga dapat diaplikasikan dalam bidang farmasi. Kinetika release digunakan untuk menentukan kecepatan release mikrokapsul oleoresin jahe merah, model yang digunakan adalah model order nol, order satu, model Higuchi, dan Model Korsmeyer-Peppas. Penyelesaian model-model ini menggunakan metode grafis dengan menentukan koefisien determinasi (R2). Tujuan penelitian ini adalah menentukan pengaruh konsentrasi sodium tripolifosfat (TPP) dan rasio berat antara kitosan dan alginate sebagai penyalut terhadap kinetika release dan karakterisasi morfologi mikrokapsul oleoresin jahe merah.  Metode enkapsulasi dimulai dengan pembentukan emulsi dari penyalut kitosan-alginat dengan rasio 1:2; 1:1; 2:1 dan 20 gram oleoresin jahe merah, penambahan TPP 3%, 4% dan 5% untuk cross-link. Emulsi dialirkan ke spray dryer untuk menghasilkan mikrokapsul oleoresin jahe merah. Uji disolusi menggunakan medium basa dengan mencampurkan KH2PO4 dan NaOH (pH 6,8) sampel diambil tiap 10 menit selama 1 jam. Hasil penelitian yang telah dilakukan didapat peningkatan konsentrasi TPP akan menurunkan kecepatan releasenya, model model kinetika dengan nilai R2 terbesar adalah model Korsmeyer-Peppas. Kata kunci: alginat; enkapsulasi; kinetika release; kitosan; oleoresin jahe merah
PENAMBAHAN POTASSIUM CHLORIDE PADA BIOPLASTIK PATI SAGU DENGAN BERPENGUAT MIKROFIBRIL SELULOSA BAMBU BERBANTUKAN SONIKASI Silviana Silviana; Puji Rahayu
Reaktor Volume 17 No. 3 September 2017
Publisher : Dept. of Chemical Engineering, Diponegoro University

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (244.355 KB) | DOI: 10.14710/reaktor.17.3.152-158

Abstract

Sago starch based bioplastics as food packaging have drawbacks such as soft, and easily broken. This paper explains improvement of sago starch-based bioplastics reinforced with bamboo microfibrillated cellulose (MFC). Furthermore, this paper investigates effect of dispersing agent on mechanical property by using of potassium chloride (KCl) assisted by ultrasonic homogenizer. Variable used experiments were bamboo MFC concentration of 1%; 3% and 5% w/w and KCl concentration of 1%; 2% dan 3% w/v. Sago starch-based solution was prepared from 4% w/v of commercial sago starch. The mixed solution was gelatinized at temperature of 90 oC. The result showed that the 5% of bamboo MFC increased tensile strength of sago starch-based bioplastics due to purpose of bamboo MFC as reinforcement of sago starch. Further, additional of KCl reduced the dispersing time for 1 hour. Optimum result in this preliminary experiment was obtained at bamboo MFC of 5% w/w and KCl concentration of 1% w/v resulting tensile strength of 17.99 MPa.
OPTIMASI PRODUKSI METIL ESTER SULFONAT DARI METIL ESTER MINYAK JELANTAH Sri Hidayati; Natalia Gultom; Hestuti Eni
Reaktor Volume 14, Nomor 2, Oktober 2012
Publisher : Dept. of Chemical Engineering, Diponegoro University

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (193.905 KB) | DOI: 10.14710/reaktor.14.2.165-172

Abstract

OPTIMATION OF METHYL ESTER SULFONATES PRODUCTION FROM WASTE COOKING METHYL ESTER. An experiment of sulfonation process of methyl ester to produce methyl ester sulfonates (MES) was caried out using waste palm methyl ester and sulfuric acid as sulfonating agent with variation of H2SO4 concentration (60% (K1), 70% (K2), dan 80% (K3)) and sulfonation time (60 minute (L1), 75 minute (L2) and 90 minute (L3)) using factorial on Randomized Complete Design Block. The experiment result showed the best sulfonation condition present in 80% H2SO4 concentration and sulfonation time of 90 minutes.  The best characteristic of MES is produced showed surface tension of 27.35 dyne/cm, emulsion stability of 89.44%, acid value of 17.72 mg KOH/g and interfacial tension of 0.0361 dyne/cm at MES concentration of 2% in 10,000 ppm salinity water. Sebuah penelitian tentang proses produksi metil ester sulfonat menggunakan minyak bekas kelapa sawit dilakukan dengan menggunakan H2SO4 sebagai agen pensulfonasi dengan variasi konsentrasi H2SO4 (60% (K1), 70% (K2), dan 80% (K3)) dan lama sulfonasi (60 menit (L1), 75 menit (L2) and 90 menit (L3)) dengan menggunakan faktorial dalam Rancangan Kelompok Teracak Lengkap. Hasil penelitian menunjukkan bahwa kondisi proses sulfonasi terbaik terdapat pada konsentrasi H2SO4 80% dan lama reaksi 90 menit. Karakteristik Metil Ester Sulfonat (MES) terbaik yang dihasilkan memperlihatkan nilai tegangan permukaan 27,35 dyne/cm, stabilitas emulsi 89,44%, nilai bilangan asam antara 17,72 mg KOH/g dan nilai tegangan antar muka pada konsentrasi MES 2% di dalam air dengan salinitas 10.000 ppm yaitu 0,0361 dyne/cm.
Preparasi dan karakterisasi zeolit dari abu laying batu bara secara alkali hidrotermal Jumaeri Jumaeri; w. Astuti; w. T.P. Lestari
Reaktor Volume 11, Nomor 1, Juni 2007
Publisher : Dept. of Chemical Engineering, Diponegoro University

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (5614.919 KB) | DOI: 10.14710/reaktor.11.1.38-44

Abstract

Preparasi zeolit dari abu laying batu bara PLTU Suralaya secara alkali hidrotermal telah dilakukan. Preparasi dilakukan terhadap abu laying yang telah direfluks dengan HCl 1M dan tanpa refluks. Larutan NaOH dengan konsentrasi tertentu (1, 2 dan 3 M) dicampur dengan abu laying batu bara dengan rasio 10 ml larutan tiap 1 gram abu laying, ke dalam tabung Teflon 100 ml dalam suatu auto clave stainless-steel. Autoclave kemudian dipanaskan pada temperatur 80-16 0C selama 3 hari. Zeolit sintesis yang dihasilkan selanjutnya diuji secara kualitatif dengan menggunakan spektroskopi inframerah., dan Difraksi Sinar-X. Hasil penelitian menunjukkan bahwa aktivasi abu laying dengan proses alkali hidrotermal dapat material yang mempunyai struktur mirip zeolit (zeolit-like). Produk hidrotermal terdiri dari campuran zeolit ( Zeolit P, Zeolit Y) serta Kristal sodalit dan mulit. Pada temperatur 160 0C, diperoleh zeolit dengan kristalinitas lebih tinggi daripada 100 0C, baik melalui refluks atau tanpa refluks. Karakteristik zeolit yang terbentuk sangat ditentukan oleh kondisi proses, yang meliputi konsentrasi NaOH, waktu dan temperatur.Kata kunci : abu layang batu bara, alkali hidrotermal, preparasi, karakterisasi, zeolit

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