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Bulletin of Chemical Reaction Engineering & Catalysis
Published by Masyarakat Katalis Indonesia - Indonesian Catalyst Society
ISSN : -     EISSN : 19782993     DOI : https://doi.org/10.9767/bcrec
Core Subject : Science, Engineering,
Chemical Engineering, Chemistry & Bioengineering Chemistry
Bulletin of Chemical Reaction Engineering & Catalysis, a reputable international journal, provides a forum for publishing the novel technologies related to the catalyst, catalysis, chemical reactor, kinetics, and chemical reaction engineering. Scientific articles dealing with the following topics in chemical reaction engineering, catalysis science, and engineering, catalyst preparation method and characterization, novel innovation of chemical reactor, kinetic studies, etc. are particularly welcome. However, articles concerned on the general chemical engineering process are not covered and out of the scope of this journal. This journal encompasses Original Research Articles, Review Articles (only selected/invited authors), and Short Communications, including: fundamentals of catalyst and catalysis; materials and nano-materials for catalyst; chemistry of catalyst and catalysis; surface chemistry of catalyst; applied catalysis; applied bio-catalysis; applied chemical reaction engineering; catalyst regeneration; catalyst deactivation; photocatalyst and photocatalysis; electrocatalysis for fuel cell application; applied bio-reactor; membrane bioreactor; fundamentals of chemical reaction engineering; kinetics studies of chemical reaction engineering; chemical reactor design (not process parameter optimization); enzymatic catalytic reaction (not process parameter optimization); kinetic studies of enzymatic reaction (not process parameter optimization); the industrial practice of catalyst; the industrial practice of chemical reactor engineering; application of plasma technology in catalysis and chemical reactor; and advanced technology for chemical reactors design. However, articles concerned about the "General Chemical Engineering Process" are not covered and out of the scope of this journal.
Arjuna Subject : Teknik Kimia (semua kategori) - Katalisis
Articles 838 Documents
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Backmatter (Author Guideline, Copyright Transfer Agreement for Publishing Form)
Bulletin of Chemical Reaction Engineering & Catalysis 2009: BCREC Volume 4 Issue 1 Year 2009 (June 2009)
Publisher : Masyarakat Katalis Indonesia - Indonesian Catalyst Society (MKICS)

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.9767/bcrec.19700

Abstract

Backmatter (Author Guideline, Copyright Transfer Agreement for Publishing Form)
Dehydrogenation of Cyclohexanol to Cyclohexanone Over Nitrogen-doped Graphene supported Cu catalyst Alyaa. K. Mageed; Dayang A. B. Radiah; A. Salmiaton; Shamsul Izhar; Musab Abdul Razak; Bamidele Victor Ayodele
Bulletin of Chemical Reaction Engineering & Catalysis 2020: BCREC Volume 15 Issue 2 Year 2020 (August 2020)
Publisher : Masyarakat Katalis Indonesia - Indonesian Catalyst Society (MKICS)

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.9767/bcrec.15.2.6774.568-578

Abstract

In this study, the dehydrogenation of cyclohexanol to cyclohexanone over nitrogen-doped reduced graphene oxide (N-rGO) Cu catalyst has been reported. The N-rGO support was synthesized by chemical reduction of graphite oxide (GO). The synthesized N-rGO was used as a support to prepare the Cu/N-rGO catalyst via an incipient wet impregnation method. The as-prepared support and the Cu/N-rGO catalyst were characterized by FESEM, EDX, XRD, TEM, TGA, and Raman spectroscopy. The various characterization analysis revealed the suitability of the Cu/N-rGO as a heterogeneous catalyst that can be employed for the dehydrogenation of cyclohexanol to cyclohexanone. The catalytic activity of the Cu/N-rGO catalyst was tested in non-oxidative dehydrogenation of cyclohexanol to cyclohexanone using a stainless-steel fixed bed reactor. The effects of temperature, reactant flow rate, and time-on-stream on the activity of the Cu/N-rGO catalyst were examined. The Cu/N-rGO nanosheets show excellent catalytic activity and selectivity to cyclohexanone. The formation of stable Cu nanoparticles on N-rGO support interaction and segregation of Cu were crucial factors for the catalytic activity. The highest cyclohexanol conversion and selectivity of 93.3% and 82.7%, respectively, were obtained at a reaction temperature of 270 °C and cyclohexanol feed rate of 0.1 ml/min. Copyright © 2020 by Authors, Published by BCREC Group. This is an open access article under the CC BY-SA License (https://creativecommons.org/licenses/by-sa/4.0). 
Ethanol Production from Whey by Kluyveromyces marxianus in Batch Fermentation System: Kinetics Parameters Estimation Dessy Ariyanti; Hadiyanto Hadiyanto
Bulletin of Chemical Reaction Engineering & Catalysis 2013: BCREC Volume 7 Issue 3 Year 2013 (March 2013)
Publisher : Masyarakat Katalis Indonesia - Indonesian Catalyst Society (MKICS)

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.9767/bcrec.7.3.4044.179-184

Abstract

Whey is the liquid remaining after milk has been curdled and strained. It is a by-product of the manufacture of cheese or casein and has several commercial uses. In environmental point of view, whey is kind of waste which has high pollution level due to it’s contain high organic compound with BOD and COD value 50 and 80 g/L respectively. On the other side, whey also contain an amount of lactose (4.5%-5%); lactose can be used as carbon source and raw material for producing ethanol via fermentation using yeast strain Kluyveromyces marxianus. The objective of this research is to investigate the ethanol production kinetics from crude whey through fermentation using Kluyveromyces marxianus and to predict the model kinetics parameter. The yeast was able to metabolize most of the lactose within 16 h to give 8.64 g/L ethanol, 4.43 g/L biomass, and remain the 3.122 g/L residual lactose. From the results presented it also can be concluded that common kinetic model for microbial growth, substrate consumption, and product formation is a good alternative to describe an experimental batch fermentation of Kluyveromyces marxianus grown on a medium composed of whey. The model was found to be capable of reflecting all batch culture phases to a certain degree of accuracy, giving the parameter value: μmax, Ks, YX/S, α, β : 0.32, 10.52, 0.095, 1.52, and 0.11 respectively.© 2013 by Authors, Published by BCREC Group. This is an open access article under the CC BY-SA License (https://creativecommons.org/licenses/by-sa/4.0)
Lampung Natural Zeolite Dopped with of ZnO-TiO2 Metal Oxide as Catalyst for Biodiesel Production Al Muttaqii, Muhammad; Marbun, Maja Pranata; Priyanto, Sugeng; Sibuea, Andreas; Simanjuntak, Wasinton; Syafaat AM, Fuad; Silalahi Raja, Havier Samuel Huttur; Alviany, Riza; Maryani, Tri; Sulistyaningsih, Triastuti; Prasetyo, Erik; Sudibyo, Sudibyo; Yati, Indri
Bulletin of Chemical Reaction Engineering & Catalysis 2024: BCREC Volume 19 Issue 1 Year 2024 (April 2024)
Publisher : Masyarakat Katalis Indonesia - Indonesian Catalyst Society (MKICS)

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.9767/bcrec.20038

Abstract

Research has been carried out on making biodiesel from palm oil using natural zeolite catalysts impregnated with metal oxides such as zinc oxide and titanium oxide. This research aims to produce biodiesel using natural zeolite and ZnO-TiO2/NZ catalysts. The catalysts were analyzed using X-Ray Diffraction (XRD), X-Ray Fluorescence (XRF), Scanning Electron Microscope (SEM), and Brunauer-Emmet-Teller (BET). The catalyst was tested in the transesterification reaction to produce biodiesel. The mole oil and methanol ratio varied from 1:15, 1:18, and 1:20. In addition, the biodiesel product was analyzed using Gas Chromatography-Mass Spectroscopy (GC-MS). The results showed the optimum condition for converting triglycerides to 1:18 variation of oil:methanol was 60.53%using a ZnO-TiO2/NZ catalyst. The ZnO-TiO2/NZ catalyst is very promising for use as a catalyst for converting palm oils into biodiesel.
Synthesis of p-Aminophenol from p-Nitrophenol Using CuO-Nanoleaf/g-Al2O3 Catalyst Didik Sudarsono; Eriawan Rismana; Slamet Slamet
Bulletin of Chemical Reaction Engineering & Catalysis 2022: BCREC Volume 17 Issue 4 Year 2022 (December 2022)
Publisher : Masyarakat Katalis Indonesia - Indonesian Catalyst Society (MKICS)

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.9767/bcrec.17.4.16135.850-861

Abstract

The CuO-nanoleaf/g-Al2O3 catalyst was synthesized through wet chemical impregnation and had promising catalytic activity in reducing p-Nitrophenol (PNP) into p-Aminophenol (PAP). The synthesis was conducted in situ with Ethylene Glycol as a stabilizer agent of the CuO-nanoleaf structure and g-Al2O3 as catalyst support with high adsorption ability. Furthermore, the crystal phase, morphology, element composition, and specific surface area were investigated by X-Ray Diffraction (XRD), Field Emission Scanning Electron Microscopy (FESEM), and N2 adsorption-desorption, respectively. The XRD pattern showed the crystal phase of CuO and g-Al2O3 in the composite, and the morphology was successfully reported using FESEM. The increase in the specific surface area of the catalyst indicates that the CuO material was well composited in g-Al2O3. The catalyst has good activity in reducing PNP to PAP with 93.53% PNP conversion within 4 min. In addition, the reduction reaction of PNP with excess NaBH4 could be categorized as pseudo-first order kinetic with a constant rate of 0.6935 min−1 for CuO-nanoleaf/g-Al2O3 catalyst. The loading catalyst and temperature reaction effect on PNP conversion were also investigated. The results showed that 94.18% PNP conversion was obtained within only 2.5 min under the optimized conditions. Copyright © 2022 by Authors, Published by BCREC Group. This is an open access article under the CC BY-SA License (https://creativecommons.org/licenses/by-sa/4.0). 
Catalyst Deactivation Simulation Through Carbon Deposition in Carbon Dioxide Reforming over Ni/CaO-Al2O3 Catalyst Istadi Istadi; Didi D. Anggoro; Nor Aishah Saidina Amin; Dorothy Hoo Wei Ling
Bulletin of Chemical Reaction Engineering & Catalysis 2011: BCREC Volume 6 Issue 2 Year 2011 (December 2011)
Publisher : Masyarakat Katalis Indonesia - Indonesian Catalyst Society (MKICS)

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.9767/bcrec.6.2.1213.129-136

Abstract

Major problem in CO2 reforming of methane (CORM) process is coke formation which is a carbonaceous residue that can physically cover active sites of a catalyst surface and leads to catalyst deactivation. A key to develop a more coke-resistant catalyst lies in a better understanding of the methane reforming mechanism at a molecular level. Therefore, this paper is aimed to simulate a micro-kinetic approach in order to calculate coking rate in CORM reaction. Rates of encapsulating and filamentous carbon formation are also included. The simulation results show that the studied catalyst has a high activity, and the rate of carbon formation is relatively low. This micro-kinetic modeling approach can be used as a tool to better understand the catalyst deactivation phenomena in reaction via carbon deposition. © 2011 by Authors, Published by BCREC Group. This is an open access article under the CC BY-SA License (https://creativecommons.org/licenses/by-sa/4.0)
Synthesis, Structural Characterization, Hirschfeld Surface Analysis and Photocatalytic CO2 Reduction of Yb(III) Complex with 4-Aacetylphenoxyacetic Acid and 1,10-Phenanthroline Ligands Xi-Shi Tai; Yuan-Fang Wang; Li-Hua Wang; Xi-Hai Yan
Bulletin of Chemical Reaction Engineering & Catalysis 2023: BCREC Volume 18 Issue 2 Year 2023 (August 2023)
Publisher : Masyarakat Katalis Indonesia - Indonesian Catalyst Society (MKICS)

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.9767/bcrec.18471

Abstract

A new nine-coordinated Yb(III) complex [YbL3(Phen)] (1) (HL = 2-(4-acetylphenoxy)acetic acid (APA), Phen = 1,10-phenanthroline) was synthesized with 2-(4-acetylphenoxy)acetic acid, YbCl3.6H2O, NaOH and 1,10-phenanthroline as materials. Complex (1) was characterized by IR and X-ray single-crystal diffraction analysis. The results show that the Yb(III) ion is nine-coordinated with seven carboxylate oxygen atoms from five different deprotonated APA ligands and two nitrogen atoms from one Phen ligand. Complex (1) forms a 3D supramolecular framework through the - stacking interactions between the Phen aromatic rings. The hirschfeld surface analysis of complex (1) was also calculated. The CO2 photoconversion activity of complex (1) has been performed under UV-vis light irradiation. The complex (1) shows good photocatalytic activity with the yield of CO is closed to 146 mmol/g after three hours of UV-vis light irradiation, the CO selectivity has reached to 97.9%. Copyright © 2023 by Authors, Published by BCREC Group. This is an open access article under the CC BY-SA License (https://creativecommons.org/licenses/by-sa/4.0).
New Dynamic Analysis and System Identification of Biodiesel Production Process from Palm Oil Ahmmed S. Ibrehem; Hikmat S. Al-Salim
Bulletin of Chemical Reaction Engineering & Catalysis 2009: BCREC Volume 4 Issue 2 Year 2009 (December 2009)
Publisher : Masyarakat Katalis Indonesia - Indonesian Catalyst Society (MKICS)

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.9767/bcrec.4.2.7111.61-68

Abstract

In this study we present advanced mathematical model was used to capture the batch reactor characteristics of reacting compounds new parameters and new a prerequisite average slope analysis (PASA) method for the system dynamic behaviour under different operational conditions is a prerequisite to the good selection for these parameters. The model was applied to batch reactor for the production of bio-diesel from palm and kapok oils. Results of the model were compared with experimental data in terms of conversion of transesterification reaction for the production of bio-diesel under unsteady state. A good agreement was obtained between our model predictions and the experimental data. Both experimental and modeling results showed that the conversion of triglycerides to methyl ester was affected by the process conditions and by using PASA that could be achieved by making some deterministic tests either in real data plant or in the physical model that properly and adequately fits the actual process. The input-output relationships are studied using the open-loop dynamic response of the process, which can be determined from the process model by stepping different inputs and recording output responses. Starting from steady state conditions, each input is perturbed with certain magnitude that is enough to show the effect on the system dynamics. The transesterficition process with temperature of about 70 oC, and methanol ratio to the triglyceride of about 5 times its stoichiometry and the NAOH catalyst of wt 0.4%, appear to be acceptable process conditions. PASA shows methanol ratio to the triglyceride has big effect on the system. PASA method can be applied for different processes. © 2009 by Authors, Published by BCREC Group. This is an open access article under the CC BY-SA License (https://creativecommons.org/licenses/by-sa/4.0)
Evaluation of Low Cost-Activated Carbon Produced from Waste Tyres Pyrolysis for Removal of 2-Chlorophenol Kanchana Manirajah; Sheela V. Sukumaran; Nor Nasuha Abdullah; Hazirah A. Razak; Nurul Ainirazali
Bulletin of Chemical Reaction Engineering & Catalysis 2019: BCREC Volume 14 Issue 2 Year 2019 (August 2019)
Publisher : Masyarakat Katalis Indonesia - Indonesian Catalyst Society (MKICS)

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.9767/bcrec.14.2.3617.443-449

Abstract

A low cost Activated Carbon (AC) was prepared by using waste tyres as raw material for the removal of 2-chlorophenol (2-CP). The AC adsorbent was prepared and activated by pyrolysis process at 900 ºC under constant nitrogen flow. The physical properties of the AC produced was characterized using X-ray Diffraction (XRD), Brunauer-Emmett-Teller (BET), Field Emission Scanning Electron Microscopy (FESEM), and Fourier Transform Infra Red (FTIR). The influence of initial adsorbate concentration, pH and adsorbent dosage on the removal of 2-CP in the batch-operational mode at ambient temperature were also investigated. The results obtained showed the AC presence of an amorphous carbon with high BET surface area and a total pore volume of 208 m2.g-1 and 0.5817 cm3, respectively. The highest adsorption capacity of 2-CP by the AC absorbent was achieved at an initial concentration of 10 mg.L-1, pH 5, and adsorbent dosage of 0.5 g in the first 10 min of contact time. This finding proves that the low cost-AC produced from waste tyres can be utilized for an effective removal of chemical plant wastewater containing toxic chlorine substances. Copyright © 2019 BCREC Group. All rights reserved 
Kinetic Model of LiFePO4 Formation Using Non-Isothermal Thermogravimetric Analysis Abdul Halim Abdul Halim; Widiyastuti Widiyastuti; Heru Setyawan; Sugeng Winardi
Bulletin of Chemical Reaction Engineering & Catalysis 2014: BCREC Volume 9 Issue 1 Year 2014 (April 2014)
Publisher : Masyarakat Katalis Indonesia - Indonesian Catalyst Society (MKICS)

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.9767/bcrec.9.1.5508.60-65

Abstract

The formation reaction of LiFePO4 from decomposition of precursors LiOH, FeSO4.7H2O and (NH4)2HPO4 with mol ratio of Li:Fe:P=1:1:1 was investigated. The experiment was carried out by thermogravimetric differential thermal analysis (TG-DTA) method using nitrogen as atmosfer at a constant heating rate to obtain kinetic constant parameters. Several heating rates were selected, there are 5, 7, 10, 15, 17.5, 22.5 and 25 °C/min. Activation energy, pre-exponential factor and reaction order were taken using Kissinger method and obtained respectively 56.086 kJ/mol, 6.95×108 min-1, and 1.058. Based on fitting result between reaction model and experiment were obtained that reaction obeyed the three dimension diffusion model. © 2014 by Authors, Published by BCREC Group. This is an open access article under the CC BY-SA License (https://creativecommons.org/licenses/by-sa/4.0)

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